US2144785A - Apparatus for the production of artificial silk - Google Patents
Apparatus for the production of artificial silk Download PDFInfo
- Publication number
- US2144785A US2144785A US48907A US4890735A US2144785A US 2144785 A US2144785 A US 2144785A US 48907 A US48907 A US 48907A US 4890735 A US4890735 A US 4890735A US 2144785 A US2144785 A US 2144785A
- Authority
- US
- United States
- Prior art keywords
- precipitant
- spinning
- filament
- filaments
- bowl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title description 10
- 229920002955 Art silk Polymers 0.000 title description 5
- 238000009987 spinning Methods 0.000 description 31
- 208000012886 Vertigo Diseases 0.000 description 30
- 238000000034 method Methods 0.000 description 13
- 239000007788 liquid Substances 0.000 description 11
- 239000000835 fiber Substances 0.000 description 9
- 229920002678 cellulose Polymers 0.000 description 6
- 239000001913 cellulose Substances 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 4
- 238000004804 winding Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000001464 adherent effect Effects 0.000 description 2
- 229960000510 ammonia Drugs 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- JJLJMEJHUUYSSY-UHFFFAOYSA-L Copper hydroxide Chemical compound [OH-].[OH-].[Cu+2] JJLJMEJHUUYSSY-UHFFFAOYSA-L 0.000 description 1
- 239000005750 Copper hydroxide Substances 0.000 description 1
- 241000347389 Serranus cabrilla Species 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 230000004308 accommodation Effects 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 229910001956 copper hydroxide Inorganic materials 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16F—SPRINGS; SHOCK-ABSORBERS; MEANS FOR DAMPING VIBRATION
- F16F7/00—Vibration-dampers; Shock-absorbers
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
- D01D5/14—Stretch-spinning methods with flowing liquid or gaseous stretching media, e.g. solution-blowing
Definitions
- the present invention relates to a process and apparatus for the production of artificial fibres by a new stretch-spinning method.
- the elemental filaments remain more or less adherent after stretching.
- the finished and stretched soft elemental filaments which are still plastic, readily stick together, and the subsequent acid treatment does not effect the separation of this undesirable union, but rather tends to accentuate it.
- the invention is chiefly concerned with the formation and subsequent treatment of soft and woolly filaments without mechanical means.
- the exclusive treatment in the precipitant liquid during the formation of the filaments enables the operation to be carried on at a high velocity (about 100 metres per minute) in such a manner that the filament is not drawn oil, but descends with the current of precipitant, owing to the velocity of the latter.
- An object of the invention is to provide apparatus for the production of cuprammonium silk fibre by the stretch-spinning method comprising in combina- 40 tion with a spinning bowl, a spinning nozzle having a group of jets downwardly directed into the upper end of the bowl, a discharge nozzle at the lower end of the bowl, means causing precipitant liquid to descend continuously, without negative pressure, through said bowl and its discharge nozzle, and means expressing the filamentary jets of cellulose solution through the spinning nozzle into the descending precipitant, of a downwardly tapering vessel disposed below said discharge nozzle, a discharge orifice at the bottom of said vessel, and means causing the precipitant to descend continuously, also without negative pressure, through said vessel wherein it serves to stretch the bundle of filaments 56 emerging fro-m said discharge nozzle, a precipitant collecting bath disposed below said discharge orifice, and an endless band passing through said bath for transporting the stretched filament bundle at reduced speed whereby said bath and band serve to relax the tension of the filament bundle.
- the stretch-spinning treatment afforded by said apparatus which is far more protective than the known methods in that it entirely avoids mechanical drawing, has the advantage that the bundle of filaments is finally rendered softer and wool-like in character, though remaining satisfactorily firm.
- the filaments After passing over the heated, cylindrical screen, the filaments are wound in hank form alternately on round winding drums, over which they run without kinking.
- the raw fibres which have been wound in parallel arrangement on the large drum may be cut up, the length of the staple depending on the existing conditions in the spinning works, and being usually about 30-40 mm.
- the staple fibres are then put through an opener, in which they are loosened, either alone or in admixture with cotton or wool. They are next put through an opener combined with a beater, to furnish a compact fleece which, after several passages through the beater, is converted into a second lap, finer and more uniform than the first. This lap is then put through the cotton carder, for example, and passed repeatedly through the coarse, medium and fine drawing frames.
- the sliver is then simply put through the slubbing, intermediate and roving frames and finally taken to the spinning frame which turns out the finished yarn.
- the fibres wound in parallel on the drum may also be transferred directly to the comber or cotton drawing frame, without being out, the machine delivering a completely straightened rove.
- the aforesaid working stages may be eliminated, the fibre coming direct from the reel being formed, on the doubling frame, into a yarn which complies with the most stringent requirements in respect of quality.
- the fibre may be worked up as a cotton substitute, which is produced cheaply in the manner last described, eliminating the first cutting and deforming of the fibre and employing the exceedingly soft fibres, formed in accordance with the above process, and having a handsome dull sheen and fluffy character, directly for further manufacturing treatment.
- the open filament being present in the strand, the latter acquires the woolly character that is imparted to cut goods by protruding fibrils.
- Fig. l is a cross-section of apparatus for spinning and subsequently treating fibres according to the invention
- Fig. 2 is a front elevation, partly in section, of the spinning portion of the apparatus.
- Fig. 3 illustrates a detail
- the apparatus for the first mentioned process, comprises a pipe 1 containing the cellulose solution, and furnished with a plurality of discharge nozzles 2 adapted to be swung for filling and cleaning, which is advisable in a multiple-nozzle arrangement as shown.
- the bowl head it is so designed as to provide accommodation for any convenient large number of juxtaposed spinning bowls 3.
- the precipitant liquid flows in a uniform and quiet manner into all the spinning bowls 3 inserted in said head.
- the height of the precipitant in the head determines the rate of discharge of the filaments.
- the cellulose solution flows, under pressure, into the nozzle heads 2 and thence through groups of jets into the precipitant-filled spinning bowls 3.
- the delivery outlet 1 of the trough 6 is adjustable
- the precipitant is caused to flow therethrough at a velocity that is substantially higher than its velocity of descent in the spinning bowls 3, in consequence of which the filaments 4 are subjected to additional stretching, the degree of elongation depending on the setting of the outlet 1.
- the filaments and precipitant pass into a collector bath 9 underneath, in which the filaments are received on an endless belt conveyor 8.
- the strands l9 of filament are relaxed by the precipitant present in the collector, and conveyed, in that condition, over a guide roller 22 to a suction screening cylinder H, by means of which the precipitant (and its contained ammonia) adhering to the filaments is removed as completely as possible.
- Gas drawn into the cylinder I I by the vacuum is recovered in known manner. This purpose is substantially favoured by a heating coil 20 provided in the vessel.
- has a conical bottom, to enable the collected copper hydroxide to be drawn oif and returned tothe dissolving process. It carries a guide 2! which directs the filaments on to cylindrical drums l2 and I3 alternately, on which the strands of filament are wound, either crosswise or parallel, until a certain depth of layer has been attained, whilst, at the same time, the filaments are washed in sulphuric acid, sprayed upon them through nozzles l4.
- the filaments are cut away from the winding drums.
- the resulting cakes 15 are then superimposed in several layers in a washing vessel l 6, as shown in Fig. 3, on perforated plates I1 and treated with liquids in succession.
- the treatment may be performed under the usual conditions, though preferably in a vacuum trough. Two soapings are given.
- the cakes are dried and mangled, either at ordinary or higher temperature, and with smooth or fluted rollers.
- a perfectly soft and open, smooth or undulating (woolly) fibrous material is obtained, which can be cut into any convenient known lengths of staple.
- Apparatus for the production of cuprammonium silk fibre by the stretch-spinning method comprising the combination with a spinning bowl, a spinning nozzle having a group of jets downwardly directed into the upper end of the bowl, a discharge nozzle at the lower end of the bowl, means causing precipitant liquid to descend continuously, without negative pressure, through said bowl and its discharge nozzle, and means expressing filamentary jets of cellulose solution through the spinning nozzle into the descending precipitant, of a downwardly-tapering vessel disposed below said discharge nozzle, a discharge orifice at the bottom of said vessel, means causing the same precipitant to descend continuously, also without negative pressure, through said vessel wherein it serves to stretch the bundle of filaments emerging from said discharge nozzle, a precipitant-collecting bath disposed below said discharge orifice, and an endless band passing through said bath for transporting the stretched filament bundle at reduced speed whereby said bath and band serve to relax the tension of the filament bundle.
- Apparatus for the production of cuprammonium silk fibre by the stretch-spinning method comprising the combination with a spinning bowl, a spinning nozzle having a group of jets downwardly directed into the upper end of the bowl, a discharge nozzle at the lower end of the bowl, means causing precipitant liquid to descend continuously, without negative pressure, through said bowl and its discharge nozzle, and means expressing filamentary jets of cellulose solution through the spinning nozzle into the descending precipitant, of a downwardly-tapering vessel disposed below said discharge nozzle, a discharge orifice at the bottom of said vessel, means causing the same precipitant to descend continuously,
- Apparatus for the production of cuprammonium silk fibre by the stretch-spinning method comprising the combination with a spinning bowl, a spinning nozzle having a group of jets downwardly directed into the upper end of the bowl, a discharge nozzle at the lower end of the bowl, means causing precipitant liquid to descend continuously, without negative pressure, through said bowl and its discharge nozzle, and means expressing filamentary jets of cellulose solution through the spinning nozzle into the descending precipitant, of a downwardly-tapering vessel disposed below said discharge nozzle, means causing the same precipitant to descend continuously, also without negative pressure, through said vessel in the upper part of which it serves to stretch the bundle of filaments emerging from said discharge nozzle, a discharge tube at the bottom of said vessel and bent through approximately a right angle to retard the precipitant in the lower part of said vessel and thereby relax the tension of the previously stretched filament in said lower part, a precipitant-collecting bath disposed about said discharge tube, a drying chest, a heating coil in said chest, a perforated su
Landscapes
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Textile Engineering (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Artificial Filaments (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE131134X | 1934-11-13 | ||
DE2144785X | 1934-11-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2144785A true US2144785A (en) | 1939-01-24 |
Family
ID=32043823
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US48907A Expired - Lifetime US2144785A (en) | 1934-11-13 | 1935-11-08 | Apparatus for the production of artificial silk |
Country Status (6)
Country | Link |
---|---|
US (1) | US2144785A (enMihai) |
BE (1) | BE412229A (enMihai) |
CH (1) | CH226670A (enMihai) |
FR (1) | FR799482A (enMihai) |
GB (1) | GB455534A (enMihai) |
NL (1) | NL45229C (enMihai) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2431695A (en) * | 1944-07-03 | 1947-12-02 | American Bemberg Corp | Thread guide |
US2467541A (en) * | 1943-07-03 | 1949-04-19 | American Viscose Corp | Method and apparatus for spinning artificial filamentous products |
US2885729A (en) * | 1955-05-03 | 1959-05-12 | Bayer Ag | Stretch-spinning device for the manufacture of rayon |
US3066007A (en) * | 1955-07-11 | 1962-11-27 | British Celanese | Manufacture of artificial filamentary materials |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR847145A (enMihai) * | 1938-09-13 | 1939-10-03 | ||
GB1130497A (en) * | 1966-10-21 | 1968-10-16 | Asahi Chemical Ind | Process for the high-speed funnel spinning of viscose filaments |
-
0
- BE BE412229D patent/BE412229A/xx unknown
- NL NL45229D patent/NL45229C/xx active
-
1935
- 1935-11-08 US US48907A patent/US2144785A/en not_active Expired - Lifetime
- 1935-11-09 CH CH226670D patent/CH226670A/de unknown
- 1935-11-13 FR FR799482D patent/FR799482A/fr not_active Expired
- 1935-11-13 GB GB31417/35A patent/GB455534A/en not_active Expired
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2467541A (en) * | 1943-07-03 | 1949-04-19 | American Viscose Corp | Method and apparatus for spinning artificial filamentous products |
US2431695A (en) * | 1944-07-03 | 1947-12-02 | American Bemberg Corp | Thread guide |
US2885729A (en) * | 1955-05-03 | 1959-05-12 | Bayer Ag | Stretch-spinning device for the manufacture of rayon |
US3066007A (en) * | 1955-07-11 | 1962-11-27 | British Celanese | Manufacture of artificial filamentary materials |
Also Published As
Publication number | Publication date |
---|---|
BE412229A (enMihai) | |
GB455534A (en) | 1936-10-22 |
NL45229C (enMihai) | |
FR799482A (fr) | 1936-06-13 |
CH226670A (de) | 1943-04-30 |
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