US2042787A - Manufacture of artificial silk - Google Patents
Manufacture of artificial silk Download PDFInfo
- Publication number
- US2042787A US2042787A US714722A US71472234A US2042787A US 2042787 A US2042787 A US 2042787A US 714722 A US714722 A US 714722A US 71472234 A US71472234 A US 71472234A US 2042787 A US2042787 A US 2042787A
- Authority
- US
- United States
- Prior art keywords
- bobbins
- drying
- silk
- perforations
- artificial silk
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229920002955 Art silk Polymers 0.000 title abstract description 15
- 238000004519 manufacturing process Methods 0.000 title description 3
- 238000001035 drying Methods 0.000 abstract description 19
- 238000000034 method Methods 0.000 abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 6
- 230000008602 contraction Effects 0.000 abstract 1
- 238000004804 winding Methods 0.000 description 19
- 229920002678 cellulose Polymers 0.000 description 5
- 239000001913 cellulose Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 238000009987 spinning Methods 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 238000010981 drying operation Methods 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000003009 desulfurizing effect Effects 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 238000002166 wet spinning Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/04—Supporting filaments or the like during their treatment
- D01D10/0409—Supporting filaments or the like during their treatment on bobbins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/06—Washing or drying
Definitions
- Our present invention relates to the manufacture of artificial silk and more particularly to drying artificial silk.
- the same effect may be produced in a much simpler way by preventing the moisture from escaping through the perforations towards the interior of the bobbin and forcing it to escape exclusively through the outer surface of the winding.
- the bobbins may for instance be closed at their both ends, or a number of bobbins may be superposed in known manner to form a column of bobbins and the ends of the column may be closed, or the bobbins may be slid on a tube, the external diameter of which is approximately the inner diameter of the bobbin, or the inner surface of the bobbin may be covered by fitting an elastic sleeve; briefiy, there may be used any means by which the perforations are closed and a perforated bobbin is transformed in a certain degree into a nonperforated one.
- any means is used and lies within the scope of the invention which causes drying to be started at the outer layers of the Winding and to be progressively carried towards the interior layers, so that the outer layers of threads are dried first, whereas the layer of threads lying directly on the bobbin is dried last.
- the uniformity of the different portions of a hank of threads as to their dyeing properties may be still further improved and ensured by interrupting the drying operation prematurely, that is to say before the winding of thread is dried throughout.
- a silk is obtained which, when perfectly dry, contains 6 to '7 grams of water per grams of dry cellulose hydrate.
- drying is interrupted prior to obtaining this content of water, for instance at a content of water of say 15, 20 or 25 per cent.
- the essence of the invention therefore is the drying of a winding of threads only from the outer surface of the winding towards the support of the winding in such a manner that the innermost layers of the winding are less dried than the outer layers thereof.
- Example 1 A winding of wet viscose silk, spun in a so-called Muller II bath containing sulfuric acid and sodium sulfate, and wound on perforated bobbins, is washed free from acid by the suction or pressure method and then contains so much moisture that 315 grams of wet fibers correspond with 100 grams of dry cellulose.
- the bobbins are then dried with air having a relative content of moisture of 30 per cent at a temperature of between and C. while closing the perforations in one of the aforesaid manners until the winding contains 16 to 18 per cent of moisture and grams of dry cellulose weighing 116 to 118 grams.
- the silk After having been kept for some time in a moistening room, the silk is twisted at an atmosphere having a high content of moisture on twisting machines in which there are several rows of bobbins one above the other and further treated in the usual way.
- Example 2 Vinylse silk spun in a spinning bath containing sulfuric acid, sodium sulfate and magnesium sulfate, and wound on perforated bobbins, is washed free from acid by the suction or pressure method, and then has a wet weight of about 260 gramscalculated on 100 grams'of dry cellulose, and is dried, while closing the perforations, at a temperature of between 40 and 60 C. with air having a relative content of moisture of 60 per cent, until the winding contains 25 per cent of moisture or a weight of about grams per 100 grams of dry cellulose.
- the further treatment is as described in Example 1.
- the process may be applied with advantage in all cases where awet fiber is collected on a solid, unyielding and perforated support and where drying produces a considerable shrinking of the thread both in a longitudinal and a lateral direction.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Textile Engineering (AREA)
- Treatment Of Fiber Materials (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Artificial Filaments (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE417307X | 1933-03-14 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2042787A true US2042787A (en) | 1936-06-02 |
Family
ID=6448692
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US714722A Expired - Lifetime US2042787A (en) | 1933-03-14 | 1934-03-08 | Manufacture of artificial silk |
Country Status (5)
Country | Link |
---|---|
US (1) | US2042787A (enrdf_load_stackoverflow) |
BE (1) | BE401900A (enrdf_load_stackoverflow) |
FR (1) | FR769850A (enrdf_load_stackoverflow) |
GB (1) | GB417307A (enrdf_load_stackoverflow) |
NL (1) | NL37713C (enrdf_load_stackoverflow) |
-
1934
- 1934-03-08 FR FR769850D patent/FR769850A/fr not_active Expired
- 1934-03-08 US US714722A patent/US2042787A/en not_active Expired - Lifetime
- 1934-03-09 BE BE401900D patent/BE401900A/xx unknown
- 1934-03-09 NL NL68698A patent/NL37713C/xx active
- 1934-03-14 GB GB8060/34A patent/GB417307A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
NL37713C (enrdf_load_stackoverflow) | 1936-03-16 |
BE401900A (enrdf_load_stackoverflow) | 1934-04-30 |
GB417307A (en) | 1934-10-02 |
FR769850A (fr) | 1934-09-03 |
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