US20180050389A1 - Unit Cell Titanium Casting - Google Patents
Unit Cell Titanium Casting Download PDFInfo
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- US20180050389A1 US20180050389A1 US15/676,683 US201715676683A US2018050389A1 US 20180050389 A1 US20180050389 A1 US 20180050389A1 US 201715676683 A US201715676683 A US 201715676683A US 2018050389 A1 US2018050389 A1 US 2018050389A1
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- chamber
- internal chamber
- pressure
- external chamber
- external
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D18/00—Pressure casting; Vacuum casting
- B22D18/06—Vacuum casting, i.e. making use of vacuum to fill the mould
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D18/00—Pressure casting; Vacuum casting
- B22D18/04—Low pressure casting, i.e. making use of pressures up to a few bars to fill the mould
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D21/00—Casting non-ferrous metals or metallic compounds so far as their metallurgical properties are of importance for the casting procedure; Selection of compositions therefor
- B22D21/002—Castings of light metals
- B22D21/005—Castings of light metals with high melting point, e.g. Be 1280 degrees C, Ti 1725 degrees C
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D23/00—Casting processes not provided for in groups B22D1/00 - B22D21/00
- B22D23/06—Melting-down metal, e.g. metal particles, in the mould
Definitions
- the present invention relates to precision titanium casting. More specifically, the present invention relates to an apparatus and method for precision titanium casting utilizing induction heating.
- Vacuum electric arc smelting is another method in which a titanium ingot is melted by substantial heat generated by mutual discharging in a high current state by respectively using a titanium ingot crucible and a water-cooled copper crucible as a positive electrode and a negative electrode, thereby forming a molten liquid metal in the crucible and completing the casting of the titanium.
- Another method is vacuum induction smelting in which an induction coil is wrapped outside a split-type water-cooled copper crucible.
- the electromagnetic force generated by the induction coil passes through a nonmetal isolation portion between splits of the copper crucible and then acts on a titanium ingot placed inside the crucible. Then the molten metal forms a molten metal liquid inside the crucible and the casting of the titanium is completed.
- Vacuum induction smelting and vacuum electric arc smelting require the use of a water-cooled copper crucible which results in the loss of substantial heat.
- the actual power consumed is very little (only 20% to 30% of the power actually acts on the titanium).
- the preparation of the molding shell is very complex and time consuming, which adds to the costs.
- the operation time of a single furnace is usually 60 to 80 minutes, and the loading and discharge process requires the coordination of many people.
- the process from the preparation of the wax pattern to the clearing of the molding shell can take ten days.
- Titanium is an extremely reactive metal. During melting via traditional casting processes, a water cooling environment is required. The molten titanium liquid will come into direct contact with water if the crucible cracks, resulting in a fierce reaction, or even explosion, which poses a great threat to production safety.
- a new kind of titanium alloy induction melting vacuum suction casting device is urgently needed, to solve the problems with existing titanium alloy casting, such as low efficiency, high cost, complicated technology, heavy workload, difficulty with preparing high-quality molding shells, long cycle and potential hazard.
- one of the primary tenets is the use of a pressure differential in order to assist the evacuation of material from the crucible into the pattern mold.
- a pressure differential In order to truly optimize the filling of complex geometries, the physical properties of resulting parts, and the efficiency of the equipment, it is beneficial to vary the pressure differential utilized during the casting sequence.
- the beginning of the cycle will have a minimal pressure differential between the outer chamber (containing the crucible) and the inner chamber (containing the pattern mold). This pressure differential is achieved through the use of a vacuum (to remove Oxygen and reduce pressure) and Argon (to replace any remaining Oxygen and increase pressure).
- One aspect of the present invention is a method for unit cell casting of titanium or titanium-alloys.
- the method includes positioning a mold within an internal chamber, wherein a pressure differential between the internal chamber and an external chamber is at a minimum.
- the method also includes evacuating an external chamber to create an evacuated external chamber wherein a ceramic crucible containing a titanium alloy ingot is positioned therein.
- the method also includes evacuating the internal chamber to create an evacuated internal chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere, wherein a pressure differential between the external chamber and the internal chamber is at minimum.
- the method also includes injecting a pressurized gas into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atm, wherein the pressure differential between the external chamber and the internal chamber is maximized.
- the method also includes melting the titanium alloy ingot within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible.
- the method also includes generating an electromagnetic field during the melting step, the electromagnetic field holding the molten titanium within the ceramic crucible.
- the method also includes ceasing the electromagnetic field.
- the method also includes transferring the completely melted titanium alloy material into the mold from the crucible using a pressure differential created between the external chamber and the internal chamber.
- the PLC controls the generation of the electromagnetic field to correspond to the complete melting of the titanium alloy ingot in the ceramic crucible.
- the pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber.
- Another aspect of the present invention is a system method for unit cell casting of titanium or titanium-alloys.
- the system includes an external chamber, a ceramic crucible positioned within the external chamber, an electromagnetic field generator centered about an opening of the ceramic crucible, an induction coil positioned around a bottom section of the ceramic crucible, an internal chamber positioned within the external chamber, a mold positioned within the internal chamber, a first vacuum gauge positioned within the internal chamber, a second vacuum gauge positioned within the external chamber, and a PLC in communication with the first vacuum gauge, the second vacuum gauge, and the induction coil.
- a minimal pressure differential is maintained between the external chamber and the internal chamber prior to the melting of the titanium alloy ingot.
- the pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber.
- the external chamber is evacuated to create an evacuated external chamber wherein the ceramic crucible contains a titanium alloy ingot positioned therein.
- a pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber.
- the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by the induction coil positioned around the ceramic crucible.
- the internal chamber is evacuated to create an evacuated internal chamber.
- the PLC controls the generating of the electromagnetic field to correspond to the complete melting of the titanium alloy ingot in the ceramic crucible.
- the titanium alloy material is completely transferred into the mold from the crucible using a maximum pressure differential created between the external chamber and the internal chamber.
- the pressurized gas is preferably argon.
- the mold is preferably covered in a kaolin wool insulating material.
- the mold is preferably for a thin-walled golf club head.
- the mold is alternatively for an article having a wall thickness less than 0.250 inch.
- the induction melting time preferably ranges from 30 seconds to 90 seconds.
- the ceramic crucible is preferably composed of two yttria-based primary crucible layers, wherein a first primary crucible layer has a thickness ranging from 0.010 inch to 0.060 inch, and a second primary crucible layer has a thickness ranging from 0.001 inch to 0.020 inch.
- the ceramic crucible further comprises a silica based backup layer.
- the induction coil is preferably positioned around a bottom section of the ceramic crucible.
- the induction coil is alternatively positioned around an upper section of the ceramic crucible.
- FIG. 1 is an illustration of a unit-cell casting system.
- FIG. 2 is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing placement of the induction coils at a lower section of the crucible.
- FIG. 2A is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing placement of the induction coils at an upper section of the crucible.
- FIG. 2B is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing an insulation material wrapped around the mold.
- FIG. 3A is an illustration of a technician pre-heating a mold in an oven.
- FIG. 3B is an illustration of a technician attaching the pre-heated mold to a lid of the internal container.
- FIG. 3C is an illustration of a technician attaching the lid to the internal container.
- FIG. 3D is an isolated view of the internal container.
- FIG. 3E is an isolated view of the lid of the internal container.
- FIG. 3F is an isolated view of the internal chamber of the internal container showing infrared heaters.
- FIG. 4 is an illustration of a unit-cell casting system during an external chamber evacuation step.
- FIG. 4A is an illustration of a unit-cell casting system during an external chamber pressurization step.
- FIG. 4B is an illustration of a unit-cell casting system during an ingot melting step.
- FIG. 5 is an illustration of a PLC unit and computer for a unit cell casting system.
- FIG. 6 is a block diagram of a unit cell casting method.
- FIG. 7 is an isolated view of a crucible for a unit cell casting system.
- FIG. 8 is a flow chart of a method for unit cell titanium casting.
- FIG. 9 is a flow chart of a method for unit cell titanium casting.
- FIG. 10 is a flow chart of a method for unit cell titanium casting.
- FIG. 11 is an illustration of a PLC unit, an operator's computer for a unit cell casting system, an internal chamber with monitoring connections.
- FIG. 12 is an illustration of a PLC unit, an operator's computer for a unit cell casting system, an internal chamber with monitoring connections.
- FIG. 13 illustrates an electromagnetic field generator around the crucible.
- a chill plate should be utilized which would help to definitively control the time that the molten material would transition to the pattern mold.
- the chill plate would be in the shape of a ring, with an opening centered on the opening of the ceramic crucible where the material is being melted.
- the plate itself would be cooled during melting and then at the optimal pour time, the cooling would be turned off. With the cooling, the seal melts through and the material is evacuated into the pattern mold. The use of this feature will allow for precise evacuation times providing consistent and optimum part quality.
- a unit cell titanium casting system 5 comprises an external container 44 , an internal container 39 , a vacuum mechanism 60 , a crucible 10 , an induction coil 15 , a coil electrical generation mechanism 25 , and a mold 30 .
- the external container 44 defines an external chamber 45 .
- the internal container 39 defines an internal chamber 40 .
- the vacuum mechanism 60 includes a vacuum line 71 , a vacuum connector 70 and pressure gauges 75 a and 75 b. The vacuum mechanism 60 is utilized to evacuate and pressurize the external chamber 45 and the internal chamber 40 in order to create a pressure differential between the internal chamber 40 and the external chamber 45 .
- the crucible 10 is preferably composed of a ceramic material.
- the crucible 10 is composed of a first layer 11 a, a second layer 11 b and a silica based third layer 11 c, as shown in FIG. 7 .
- a metal ingot 20 is placed within the interior of the crucible 10 .
- the metal ingot 20 is preferably a titanium alloy material.
- the volume of the crucible 10 preferably corresponds to the amount of metal necessary for forming the article.
- the interior of the crucible 10 preferably has a diameter ranging from 15 centimeters (“cm”) to 90 cm, more preferably from 35 cm to 60 cm.
- a height of the crucible 10 preferably ranges 30 cm to 200 cm, and more preferably from 60 cm to 100 cm.
- connection nozzle 27 is connected between a bottom opening (not shown) of the crucible 10 and an opening to the mold 30 .
- the connection nozzle 27 allows the melted metal material from the ingot 20 to flow into the mold 30 for casting of the article.
- the size of connection nozzle 27 is determined based on the size and shape of the cavity of the mold 30 , and is preferably from 5 cm to 100 cm, and more preferably from 15 cm to 50 cm.
- the induction coil 15 is wrapped around the crucible 10 .
- the induction coil 15 is energized to generate an electromagnetic force to melt the metal ingot 20 (e.g., titanium alloy ingot) within the crucible 10 .
- the coil electrical generation mechanism 25 provides the electricity to the induction coil 15 .
- the induction coil 15 is wrapped around a bottom section 10 b of the crucible 10 . This melts the bottom of the ingot 20 first.
- the induction coil 15 is wrapped around an upper section 10 a of the crucible 10 . This melts the top of the ingot 20 first.
- the induction coil 15 is preferably centered on the upper third of the ingot 20 . This positioning allows the induction coil 15 to first act on the upper portion of the ingot 20 (melting the material from the top down), causing molten material to cascade around the still-solid ingot 20 and forming a seal before the electromagnetic forces of the induction coil 15 affect the remaining material.
- the induction coil 15 is positioned towards the bottom 10 b of the ceramic crucible 10 . This positioning allows for a uniform melt as molten material cascades onto itself and also increased homogeneity of the pour as the electromagnetic forces can better act on the molten material prior to it being evacuated from the crucible 10 .
- Melting of the ingot 20 of titanium alloy is carried out in a vacuum condition for induction melting.
- the induction coil 15 is connected to the coil electrical generation mechanism 25 .
- the ceramic crucible 10 is utilized for vacuum induction melting of the titanium alloy.
- the ceramic material does not interfere with the fielding effect of the electromagnetic force, and the electro-magnetic induction energy generated by the induction coil 15 is fully focused on melting the ingot of titanium alloy.
- an insulating material 31 is wrapped around the mold 30 .
- pattern molds are preheated prior to use in order to improve the flow of material into the mold itself and to better allow the mold 30 to fill completely. Due to the nature of titanium materials, and the melting process itself, the more that heat loss is minimized, the greater time the material has to flow and fill the mold 30 prior to solidification. To this end, pattern mold heat is retained through the use of an insulating material 31 (e.g.: Kaolin wool) thereby extending the useful period of the mold 30 prior to the pour and allowing for better fill, including filling of more difficult molds (e.g., thin walled castings).
- an insulating material 31 e.g.: Kaolin wool
- the mold 30 is preheated in an oven 80 .
- pattern molds 30 are preheated prior to use in order to improve the flow of material into the mold 30 itself and to better allow the mold 30 to fill completely. Due to the nature of titanium materials, and the melting process itself, there is a likely correlation between the temperature of the mold 30 and the ability to fill complex and/or thin walled pattern molds 30 . Temperatures testing include 1050° C., 1060° C., 1100° C., 1150° C., 1200° C., 1250° C. and 1260° C. The pre-heated mold is removed from the 80 and attached to a lid 35 of the internal container 39 .
- infrared heaters 50 a and 50 b are used to maintain the heat of the mold 30 within the internal chamber 40 . Due to the nature of titanium materials, and the melting process itself, the more that heat loss is minimized, the greater time the material can flow and fill the mold 30 prior to solidification. To this end, pattern mold heat is retained through the use of infrared heaters 50 a and 50 b placed within the internal walls of the internal chamber 40 of the internal container 39 in order to minimize pattern mold cool down and improve the ability to cast complex and/or thin-walled parts.
- FIGS. 4, 4A and 4B illustrate the casting process using a pressure differential between the external chamber 45 and the internal chamber 40 to assist in the flow of melted titanium alloy materials into a mold 30 .
- FIG. 5 illustrates a programmable logic computer (“PLC”) and operator computer 91 utilized with the unit cell casting system 5 .
- PLC programmable logic computer
- FIG. 6 is a block diagram of a unit cell casting method 600 .
- an ingot 20 is prepared for casting.
- the single ingot 20 is utilized to manufacture a single article such as a golf club head 29 .
- the present invention manufactures only a single article in each process.
- the mold 30 is preheated in an oven.
- the external chamber 45 is evacuated.
- the external chamber 45 is pressurized with an argon gas.
- the internal chamber 40 is evacuated.
- the induction coil 15 is energized and at step 607 the ingot 20 is melted within the crucible 10 .
- the melted material flows into mold 30 .
- the de-molding process occurs.
- the article (golf club head) 29 is finished.
- a frequency generated in the induction coil ranges from 1 kilo-Hertz to 50 kilo-Hertz, and a power ranges from 15 kilo-Watts to 50 kilo-Watts.
- An atmospheric pressure of the evacuated internal chamber ranges from 3 ⁇ 10 ⁇ 2 atmosphere to 9.87 ⁇ 10 ⁇ 7 atmosphere.
- An atmospheric pressure of the evacuated internal chamber ranges from 9.87 ⁇ 10 ⁇ 7 atmosphere to 9.87 ⁇ 10 ⁇ 13 atmosphere.
- the first layer 11 a and the second layer 11 b are preferably composed of yttrium oxide and other materials.
- Yttrium oxide is highly inert to titanium in a high-temperature environment resulting in no chemical reaction between the two materials.
- Yttrium oxide also isolates the ceramic material from the titanium during the melting process to prevent reaction between them to ensure the smooth melting of the titanium-alloy.
- the third layer 11 c of the crucible 10 is preferably composed of silicon dioxide and other materials. The silicon dioxide resists the metallic expansion and thermal stress during the melting process to ensure strength of the crucible.
- a preferred thickness of the first layer 11 a is from 0.5 mm to 1.5 mm and the preferred thickness range of the crucible 10 is from 5 mm to 15 mm.
- a method 800 for unit cell casting of titanium or titanium-alloys is shown in FIG. 8 .
- a pressure of an internal chamber is monitored utilizing a first vacuum gauge.
- a pressure of an external chamber is monitored utilizing a second vacuum gauge.
- the pressure of the internal chamber and the pressure of the external chamber are transmitted to a programmable logic controller (PLC).
- PLC programmable logic controller
- a mold is positioned within the internal chamber.
- an external chamber is evacuated to create an evacuated external chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere, wherein a ceramic crucible containing a titanium alloy ingot is positioned therein.
- the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere, wherein the external chamber and the internal chamber have an equal pressurization.
- the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible.
- the completely melted titanium alloy material is transferred into the mold from the crucible using a pressure equalization between the external chamber and the internal chamber.
- a pressure equalization is maintained between the external chamber and the internal chamber during the melting of the titanium alloy ingot.
- the pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber.
- a method 900 for unit cell casting of titanium or titanium-alloys is shown in FIG. 9 .
- a pressure of an internal chamber is monitored utilizing a first vacuum gauge.
- a pressure of an external chamber is monitored utilizing a second vacuum gauge.
- the pressure of the internal chamber and the pressure of the external chamber are transmitted to a programmable logic controller (PLC).
- PLC programmable logic controller
- a mold is positioned within the internal chamber.
- an external chamber is evacuated to create an evacuated external chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere, wherein a ceramic crucible containing a titanium alloy ingot is positioned therein.
- the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere, wherein the external chamber and the internal chamber have an equal pressurization.
- the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible.
- a pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atm, wherein the pressure differential between the external chamber and the internal chamber is maximized.
- the completely melted titanium alloy material is transferred into the mold from the crucible using a pressure equalization between the external chamber and the internal chamber.
- a high pressure differential in maintained between the external chamber and the internal chamber during the transfer of the melted titanium alloy material is monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber.
- a method 1000 for unit cell casting of titanium or titanium-alloys is shown in FIG. 10 .
- a mold is positioned within an internal chamber of a casting chamber.
- an external chamber is evacuated to create an evacuated external chamber wherein a ceramic crucible containing a titanium alloy ingot is positioned therein.
- the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3 ⁇ 10 ⁇ 2 atmosphere.
- the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible, wherein the external chamber and the internal chamber are at an equal pressurization.
- a pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atmosphere.
- a high pressure differential is utilized between the external chamber and the internal chamber to flow the completely melted titanium alloy material into the mold from the crucible.
- FIG. 11 illustrates a PLC 90 , an operator's computer 91 and an apparatus 5 for a system for unit cell titanium casting.
- FIG. 12 illustrates a PLC 90 , an operator's computer 91 and an internal chamber with an optical pyrometer for a system for unit cell titanium casting.
- the optical pyrometer monitors the temperature of the internal chamber.
- an electromagnetic field generator 199 is positioned around a bottom of the crucible.
- the electromagnetic field generator 199 is controlled by the PLC 90 .
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Abstract
Description
- The present application claims priority to U.S. Provisional Patent Application No. 62/375,804, filed on Aug. 16, 2016, which is hereby incorporated by reference in its entirety.
- Not Applicable
- The present invention relates to precision titanium casting. More specifically, the present invention relates to an apparatus and method for precision titanium casting utilizing induction heating.
- Various methods of titanium casting are well-known. One such method is investment casting which involves a lost wax procedure.
- Vacuum electric arc smelting is another method in which a titanium ingot is melted by substantial heat generated by mutual discharging in a high current state by respectively using a titanium ingot crucible and a water-cooled copper crucible as a positive electrode and a negative electrode, thereby forming a molten liquid metal in the crucible and completing the casting of the titanium.
- Another method is vacuum induction smelting in which an induction coil is wrapped outside a split-type water-cooled copper crucible. The electromagnetic force generated by the induction coil passes through a nonmetal isolation portion between splits of the copper crucible and then acts on a titanium ingot placed inside the crucible. Then the molten metal forms a molten metal liquid inside the crucible and the casting of the titanium is completed.
- Vacuum induction smelting and vacuum electric arc smelting require the use of a water-cooled copper crucible which results in the loss of substantial heat. The actual power consumed is very little (only 20% to 30% of the power actually acts on the titanium). Furthermore, the preparation of the molding shell is very complex and time consuming, which adds to the costs. In the traditional casting technology, the operation time of a single furnace is usually 60 to 80 minutes, and the loading and discharge process requires the coordination of many people. In the traditional casting technology, the process from the preparation of the wax pattern to the clearing of the molding shell can take ten days.
- Titanium is an extremely reactive metal. During melting via traditional casting processes, a water cooling environment is required. The molten titanium liquid will come into direct contact with water if the crucible cracks, resulting in a fierce reaction, or even explosion, which poses a great threat to production safety.
- To solve the above problems, a new kind of titanium alloy induction melting vacuum suction casting device is urgently needed, to solve the problems with existing titanium alloy casting, such as low efficiency, high cost, complicated technology, heavy workload, difficulty with preparing high-quality molding shells, long cycle and potential hazard.
- Utilizing the two chamber casting system, one of the primary tenets is the use of a pressure differential in order to assist the evacuation of material from the crucible into the pattern mold. In order to truly optimize the filling of complex geometries, the physical properties of resulting parts, and the efficiency of the equipment, it is beneficial to vary the pressure differential utilized during the casting sequence. Optimally, the beginning of the cycle will have a minimal pressure differential between the outer chamber (containing the crucible) and the inner chamber (containing the pattern mold). This pressure differential is achieved through the use of a vacuum (to remove Oxygen and reduce pressure) and Argon (to replace any remaining Oxygen and increase pressure). Immediately prior to crucible evacuation the pressure in the inner chamber would be decreased; this will allow for additional pressure-assisted transition in order to allow the filling of complex geometries, while minimizing turbulent flow of molten Titanium, and also minimizing overall equipment cycle times.
- One aspect of the present invention is a method for unit cell casting of titanium or titanium-alloys. The method includes positioning a mold within an internal chamber, wherein a pressure differential between the internal chamber and an external chamber is at a minimum. The method also includes evacuating an external chamber to create an evacuated external chamber wherein a ceramic crucible containing a titanium alloy ingot is positioned therein. The method also includes evacuating the internal chamber to create an evacuated internal chamber having a pressure no greater than 3×10−2 atmosphere, wherein a pressure differential between the external chamber and the internal chamber is at minimum. The method also includes injecting a pressurized gas into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atm, wherein the pressure differential between the external chamber and the internal chamber is maximized. The method also includes melting the titanium alloy ingot within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible. The method also includes generating an electromagnetic field during the melting step, the electromagnetic field holding the molten titanium within the ceramic crucible. The method also includes ceasing the electromagnetic field. The method also includes transferring the completely melted titanium alloy material into the mold from the crucible using a pressure differential created between the external chamber and the internal chamber. A high pressure differential in maintained between the external chamber and the internal chamber during the transfer of the melted titanium alloy material. The PLC controls the generation of the electromagnetic field to correspond to the complete melting of the titanium alloy ingot in the ceramic crucible. The pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber.
- Another aspect of the present invention is a system method for unit cell casting of titanium or titanium-alloys. The system includes an external chamber, a ceramic crucible positioned within the external chamber, an electromagnetic field generator centered about an opening of the ceramic crucible, an induction coil positioned around a bottom section of the ceramic crucible, an internal chamber positioned within the external chamber, a mold positioned within the internal chamber, a first vacuum gauge positioned within the internal chamber, a second vacuum gauge positioned within the external chamber, and a PLC in communication with the first vacuum gauge, the second vacuum gauge, and the induction coil. A minimal pressure differential is maintained between the external chamber and the internal chamber prior to the melting of the titanium alloy ingot. The pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber. The external chamber is evacuated to create an evacuated external chamber wherein the ceramic crucible contains a titanium alloy ingot positioned therein. A pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber. The titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by the induction coil positioned around the ceramic crucible. The internal chamber is evacuated to create an evacuated internal chamber. The PLC controls the generating of the electromagnetic field to correspond to the complete melting of the titanium alloy ingot in the ceramic crucible. The titanium alloy material is completely transferred into the mold from the crucible using a maximum pressure differential created between the external chamber and the internal chamber.
- The pressurized gas is preferably argon. The mold is preferably covered in a kaolin wool insulating material. The mold is preferably for a thin-walled golf club head. The mold is alternatively for an article having a wall thickness less than 0.250 inch. The induction melting time preferably ranges from 30 seconds to 90 seconds. The ceramic crucible is preferably composed of two yttria-based primary crucible layers, wherein a first primary crucible layer has a thickness ranging from 0.010 inch to 0.060 inch, and a second primary crucible layer has a thickness ranging from 0.001 inch to 0.020 inch. The ceramic crucible further comprises a silica based backup layer. The induction coil is preferably positioned around a bottom section of the ceramic crucible. The induction coil is alternatively positioned around an upper section of the ceramic crucible.
- Having briefly described the present invention, the above and further objects, features and advantages thereof will be recognized by those skilled in the pertinent art from the following detailed description of the invention when taken in conjunction with the accompanying drawings.
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FIG. 1 is an illustration of a unit-cell casting system. -
FIG. 2 is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing placement of the induction coils at a lower section of the crucible. -
FIG. 2A is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing placement of the induction coils at an upper section of the crucible. -
FIG. 2B is an isolated view of an interior chamber, crucible, induction coils and mold of the unit-cell casting system, showing an insulation material wrapped around the mold. -
FIG. 3A is an illustration of a technician pre-heating a mold in an oven. -
FIG. 3B is an illustration of a technician attaching the pre-heated mold to a lid of the internal container. -
FIG. 3C is an illustration of a technician attaching the lid to the internal container. -
FIG. 3D is an isolated view of the internal container. -
FIG. 3E is an isolated view of the lid of the internal container. -
FIG. 3F is an isolated view of the internal chamber of the internal container showing infrared heaters. -
FIG. 4 is an illustration of a unit-cell casting system during an external chamber evacuation step. -
FIG. 4A is an illustration of a unit-cell casting system during an external chamber pressurization step. -
FIG. 4B is an illustration of a unit-cell casting system during an ingot melting step. -
FIG. 5 is an illustration of a PLC unit and computer for a unit cell casting system. -
FIG. 6 is a block diagram of a unit cell casting method. -
FIG. 7 is an isolated view of a crucible for a unit cell casting system. -
FIG. 8 is a flow chart of a method for unit cell titanium casting. -
FIG. 9 is a flow chart of a method for unit cell titanium casting. -
FIG. 10 is a flow chart of a method for unit cell titanium casting. -
FIG. 11 is an illustration of a PLC unit, an operator's computer for a unit cell casting system, an internal chamber with monitoring connections. -
FIG. 12 is an illustration of a PLC unit, an operator's computer for a unit cell casting system, an internal chamber with monitoring connections. -
FIG. 13 illustrates an electromagnetic field generator around the crucible. - During the casting process it is critical to ensure that the material be heated sufficiently and consistently in order to ensure proper flow into the pattern mold. Especially with the use of a bottom-fed/gravity flow system, having the ability to precisely control the pour time will allow for optimum material heating ensuring desired material properties in the finished part. In order to achieve this a chill plate should be utilized which would help to definitively control the time that the molten material would transition to the pattern mold. The chill plate would be in the shape of a ring, with an opening centered on the opening of the ceramic crucible where the material is being melted. The plate itself would be cooled during melting and then at the optimal pour time, the cooling would be turned off. With the cooling, the seal melts through and the material is evacuated into the pattern mold. The use of this feature will allow for precise evacuation times providing consistent and optimum part quality.
- As shown in
FIG. 1 , a unit celltitanium casting system 5 comprises anexternal container 44, aninternal container 39, avacuum mechanism 60, acrucible 10, aninduction coil 15, a coilelectrical generation mechanism 25, and amold 30. Theexternal container 44 defines anexternal chamber 45. Theinternal container 39 defines aninternal chamber 40. Thevacuum mechanism 60 includes avacuum line 71, avacuum connector 70 andpressure gauges vacuum mechanism 60 is utilized to evacuate and pressurize theexternal chamber 45 and theinternal chamber 40 in order to create a pressure differential between theinternal chamber 40 and theexternal chamber 45. - The
crucible 10 is preferably composed of a ceramic material. In a most preferred embodiment, thecrucible 10 is composed of afirst layer 11 a, asecond layer 11 b and a silica basedthird layer 11 c, as shown inFIG. 7 . Ametal ingot 20 is placed within the interior of thecrucible 10. Themetal ingot 20 is preferably a titanium alloy material. The volume of thecrucible 10 preferably corresponds to the amount of metal necessary for forming the article. The interior of thecrucible 10 preferably has a diameter ranging from 15 centimeters (“cm”) to 90 cm, more preferably from 35 cm to 60 cm. A height of thecrucible 10 preferably ranges 30 cm to 200 cm, and more preferably from 60 cm to 100 cm. - A
connection nozzle 27 is connected between a bottom opening (not shown) of thecrucible 10 and an opening to themold 30. Theconnection nozzle 27 allows the melted metal material from theingot 20 to flow into themold 30 for casting of the article. Specifically, the size ofconnection nozzle 27 is determined based on the size and shape of the cavity of themold 30, and is preferably from 5 cm to 100 cm, and more preferably from 15 cm to 50 cm. - The
induction coil 15 is wrapped around thecrucible 10. Theinduction coil 15 is energized to generate an electromagnetic force to melt the metal ingot 20 (e.g., titanium alloy ingot) within thecrucible 10. The coilelectrical generation mechanism 25 provides the electricity to theinduction coil 15. As shown inFIG. 2 , theinduction coil 15 is wrapped around abottom section 10 b of thecrucible 10. This melts the bottom of theingot 20 first. As shown inFIG. 2A , theinduction coil 15 is wrapped around anupper section 10 a of thecrucible 10. This melts the top of theingot 20 first. - In order to optimize the ability of the target material to seal around the port of a
ceramic crucible 10, theinduction coil 15 is preferably centered on the upper third of theingot 20. This positioning allows theinduction coil 15 to first act on the upper portion of the ingot 20 (melting the material from the top down), causing molten material to cascade around the still-solid ingot 20 and forming a seal before the electromagnetic forces of theinduction coil 15 affect the remaining material. - Alternatively, in order to fully utilize the electromagnetic forces of the
induction coil 15, to include the electromagnetic stirring of the melt, theinduction coil 15 is positioned towards the bottom 10 b of theceramic crucible 10. This positioning allows for a uniform melt as molten material cascades onto itself and also increased homogeneity of the pour as the electromagnetic forces can better act on the molten material prior to it being evacuated from thecrucible 10. - Melting of the
ingot 20 of titanium alloy is carried out in a vacuum condition for induction melting. Theinduction coil 15 is connected to the coilelectrical generation mechanism 25. - The
ceramic crucible 10 is utilized for vacuum induction melting of the titanium alloy. The ceramic material does not interfere with the fielding effect of the electromagnetic force, and the electro-magnetic induction energy generated by theinduction coil 15 is fully focused on melting the ingot of titanium alloy. - In an embodiment shown in
FIG. 2B , an insulatingmaterial 31 is wrapped around themold 30. During casting pattern molds are preheated prior to use in order to improve the flow of material into the mold itself and to better allow themold 30 to fill completely. Due to the nature of titanium materials, and the melting process itself, the more that heat loss is minimized, the greater time the material has to flow and fill themold 30 prior to solidification. To this end, pattern mold heat is retained through the use of an insulating material 31 (e.g.: Kaolin wool) thereby extending the useful period of themold 30 prior to the pour and allowing for better fill, including filling of more difficult molds (e.g., thin walled castings). - As shown in
FIGS. 3A, 3B, 3C, 3D and 3E , themold 30 is preheated in anoven 80. During unit cell casting,pattern molds 30 are preheated prior to use in order to improve the flow of material into themold 30 itself and to better allow themold 30 to fill completely. Due to the nature of titanium materials, and the melting process itself, there is a likely correlation between the temperature of themold 30 and the ability to fill complex and/or thinwalled pattern molds 30. Temperatures testing include 1050° C., 1060° C., 1100° C., 1150° C., 1200° C., 1250° C. and 1260° C. The pre-heated mold is removed from the 80 and attached to alid 35 of theinternal container 39. - In an alternative embodiment shown in
FIG. 3F ,infrared heaters mold 30 within theinternal chamber 40. Due to the nature of titanium materials, and the melting process itself, the more that heat loss is minimized, the greater time the material can flow and fill themold 30 prior to solidification. To this end, pattern mold heat is retained through the use ofinfrared heaters internal chamber 40 of theinternal container 39 in order to minimize pattern mold cool down and improve the ability to cast complex and/or thin-walled parts. -
FIGS. 4, 4A and 4B illustrate the casting process using a pressure differential between theexternal chamber 45 and theinternal chamber 40 to assist in the flow of melted titanium alloy materials into amold 30. -
FIG. 5 illustrates a programmable logic computer (“PLC”) andoperator computer 91 utilized with the unitcell casting system 5. -
FIG. 6 is a block diagram of a unitcell casting method 600. Atstep 601, aningot 20 is prepared for casting. Thesingle ingot 20 is utilized to manufacture a single article such as agolf club head 29. As opposed to manufacturing multiple articles in a single process, which results in the loss of material, the present invention manufactures only a single article in each process. Atstep 602, themold 30 is preheated in an oven. Atstep 603, theexternal chamber 45 is evacuated. Atstep 604, theexternal chamber 45 is pressurized with an argon gas. Atstep 605, theinternal chamber 40 is evacuated. Atstep 606, theinduction coil 15 is energized and atstep 607 theingot 20 is melted within thecrucible 10. At thestep 608, the melted material flows intomold 30. Atstep 609, the de-molding process occurs. Atstep 610, the article (golf club head) 29 is finished. A frequency generated in the induction coil ranges from 1 kilo-Hertz to 50 kilo-Hertz, and a power ranges from 15 kilo-Watts to 50 kilo-Watts. An atmospheric pressure of the evacuated internal chamber ranges from 3×10−2 atmosphere to 9.87×10−7 atmosphere. An atmospheric pressure of the evacuated internal chamber ranges from 9.87×10−7 atmosphere to 9.87×10−13 atmosphere. - As shown in
FIG. 7 , thefirst layer 11 a and thesecond layer 11 b are preferably composed of yttrium oxide and other materials. Yttrium oxide is highly inert to titanium in a high-temperature environment resulting in no chemical reaction between the two materials. Yttrium oxide also isolates the ceramic material from the titanium during the melting process to prevent reaction between them to ensure the smooth melting of the titanium-alloy. Thethird layer 11 c of thecrucible 10 is preferably composed of silicon dioxide and other materials. The silicon dioxide resists the metallic expansion and thermal stress during the melting process to ensure strength of the crucible. - A preferred thickness of the
first layer 11 a is from 0.5 mm to 1.5 mm and the preferred thickness range of thecrucible 10 is from 5 mm to 15 mm. - A
method 800 for unit cell casting of titanium or titanium-alloys is shown inFIG. 8 . Atblock 801, a pressure of an internal chamber is monitored utilizing a first vacuum gauge. Atblock 802, a pressure of an external chamber is monitored utilizing a second vacuum gauge. Atblock 803, the pressure of the internal chamber and the pressure of the external chamber are transmitted to a programmable logic controller (PLC). Atblock 804, a mold is positioned within the internal chamber. Atblock 805, an external chamber is evacuated to create an evacuated external chamber having a pressure no greater than 3×10−2 atmosphere, wherein a ceramic crucible containing a titanium alloy ingot is positioned therein. Atblock 806, the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3×10−2 atmosphere, wherein the external chamber and the internal chamber have an equal pressurization. Atblock 807, the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible. Atblock 808, the completely melted titanium alloy material is transferred into the mold from the crucible using a pressure equalization between the external chamber and the internal chamber. A pressure equalization is maintained between the external chamber and the internal chamber during the melting of the titanium alloy ingot. The pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber. - A
method 900 for unit cell casting of titanium or titanium-alloys is shown inFIG. 9 . Atblock 901, a pressure of an internal chamber is monitored utilizing a first vacuum gauge. Atblock 902, a pressure of an external chamber is monitored utilizing a second vacuum gauge. Atblock 903, the pressure of the internal chamber and the pressure of the external chamber are transmitted to a programmable logic controller (PLC). Atblock 904, a mold is positioned within the internal chamber. Atblock 905, an external chamber is evacuated to create an evacuated external chamber having a pressure no greater than 3×10−2 atmosphere, wherein a ceramic crucible containing a titanium alloy ingot is positioned therein. Atblock 906, the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3×10−2 atmosphere, wherein the external chamber and the internal chamber have an equal pressurization. Atblock 907, the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible. Atblock 908, a pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atm, wherein the pressure differential between the external chamber and the internal chamber is maximized. Atblock 909, the completely melted titanium alloy material is transferred into the mold from the crucible using a pressure equalization between the external chamber and the internal chamber. A high pressure differential in maintained between the external chamber and the internal chamber during the transfer of the melted titanium alloy material. The pressure of the internal chamber and the pressure of the external chamber are monitored and communicated to the PLC during the casting process, and wherein the PLC controls the casting process based on the pressure of the internal chamber and the pressure of the external chamber. - A
method 1000 for unit cell casting of titanium or titanium-alloys is shown inFIG. 10 . Atblock 1001, a mold is positioned within an internal chamber of a casting chamber. Atblock 1002, an external chamber is evacuated to create an evacuated external chamber wherein a ceramic crucible containing a titanium alloy ingot is positioned therein. Atblock 1003, the internal chamber is evacuated to create an evacuated internal chamber having a pressure no greater than 3×10−2 atmosphere. Atblock 1004, the titanium alloy ingot is melted within the ceramic crucible utilizing induction heating generated by an induction coil positioned around the ceramic crucible, wherein the external chamber and the internal chamber are at an equal pressurization. Atblock 1005, a pressurized gas is injected into the evacuated external chamber to create a pressurized external chamber with a pressure in excess of 1 atmosphere. Atblock 1006, a high pressure differential is utilized between the external chamber and the internal chamber to flow the completely melted titanium alloy material into the mold from the crucible. -
FIG. 11 illustrates aPLC 90, an operator'scomputer 91 and anapparatus 5 for a system for unit cell titanium casting. -
FIG. 12 illustrates aPLC 90, an operator'scomputer 91 and an internal chamber with an optical pyrometer for a system for unit cell titanium casting. The optical pyrometer monitors the temperature of the internal chamber. - As shown in
FIG. 13 , anelectromagnetic field generator 199 is positioned around a bottom of the crucible. Theelectromagnetic field generator 199 is controlled by thePLC 90. - Those skilled in the pertinent art will recognize that materials other than titanium and titanium alloy may be cast in the unit cell casting system without departing from the scope and spirit of the present invention.
- From the foregoing it is believed that those skilled in the pertinent art will recognize the meritorious advancement of this invention and will readily understand that while the present invention has been described in association with a preferred embodiment thereof, and other embodiments illustrated in the accompanying drawings, numerous changes, modifications and substitutions of equivalents may be made therein without departing from the spirit and scope of this invention which is intended to be unlimited by the foregoing except as may appear in the following appended claims. Therefore, the embodiments of the invention in which an exclusive property or privilege is claimed are defined in the following appended claims.
Claims (19)
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US15/676,683 US20180050389A1 (en) | 2016-08-16 | 2017-08-14 | Unit Cell Titanium Casting |
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US15/676,683 US20180050389A1 (en) | 2016-08-16 | 2017-08-14 | Unit Cell Titanium Casting |
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CN108465800A (en) * | 2018-03-27 | 2018-08-31 | 南京宝泰特种材料股份有限公司 | The casting method of the irregular thin-section casting of titanium |
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CN108465800A (en) * | 2018-03-27 | 2018-08-31 | 南京宝泰特种材料股份有限公司 | The casting method of the irregular thin-section casting of titanium |
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