US20100276142A1 - Method of treating proppants and fractures in-situ with fluorinated silane - Google Patents

Method of treating proppants and fractures in-situ with fluorinated silane Download PDF

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Publication number
US20100276142A1
US20100276142A1 US12/745,936 US74593608A US2010276142A1 US 20100276142 A1 US20100276142 A1 US 20100276142A1 US 74593608 A US74593608 A US 74593608A US 2010276142 A1 US2010276142 A1 US 2010276142A1
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US
United States
Prior art keywords
group
formula
fracture
fluorinated
independently selected
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US12/745,936
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English (en)
Inventor
John D. Skildum
Jimmie R. Baran, Jr.
Wayne W. Fan
Madeline P. Shinbach
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3M Innovative Properties Co
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3M Innovative Properties Co
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Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Priority to US12/745,936 priority Critical patent/US20100276142A1/en
Assigned to 3M INNOVATIVE PROPERTIES COMPANY reassignment 3M INNOVATIVE PROPERTIES COMPANY ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: FAN, WAYNE W., SHINBACH, MADELINE P., SKILDUM, JOHN D., BARAN, JIMMIE R., JR.
Publication of US20100276142A1 publication Critical patent/US20100276142A1/en
Abandoned legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60Compositions for stimulating production by acting on the underground formation
    • C09K8/62Compositions for forming crevices or fractures
    • C09K8/66Compositions based on water or polar solvents
    • C09K8/68Compositions based on water or polar solvents containing organic compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805Compounds having only one group containing active hydrogen
    • C08G18/288Compounds containing at least one heteroatom other than oxygen or nitrogen
    • C08G18/2885Compounds containing at least one heteroatom other than oxygen or nitrogen containing halogen atoms
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805Compounds having only one group containing active hydrogen
    • C08G18/288Compounds containing at least one heteroatom other than oxygen or nitrogen
    • C08G18/289Compounds containing at least one heteroatom other than oxygen or nitrogen containing silicon
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60Compositions for stimulating production by acting on the underground formation
    • C09K8/80Compositions for reinforcing fractures, e.g. compositions of proppants used to keep the fractures open
US12/745,936 2007-12-05 2008-12-01 Method of treating proppants and fractures in-situ with fluorinated silane Abandoned US20100276142A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US12/745,936 US20100276142A1 (en) 2007-12-05 2008-12-01 Method of treating proppants and fractures in-situ with fluorinated silane

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US99244207P 2007-12-05 2007-12-05
US12/745,936 US20100276142A1 (en) 2007-12-05 2008-12-01 Method of treating proppants and fractures in-situ with fluorinated silane
PCT/US2008/085116 WO2009076080A1 (en) 2007-12-05 2008-12-01 Method of treating proppants and fractures in-situ with fluorinated silane

Publications (1)

Publication Number Publication Date
US20100276142A1 true US20100276142A1 (en) 2010-11-04

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ID=40429802

Family Applications (1)

Application Number Title Priority Date Filing Date
US12/745,936 Abandoned US20100276142A1 (en) 2007-12-05 2008-12-01 Method of treating proppants and fractures in-situ with fluorinated silane

Country Status (6)

Country Link
US (1) US20100276142A1 (de)
EP (1) EP2225344B1 (de)
CN (1) CN101889066A (de)
AT (1) ATE547498T1 (de)
CA (1) CA2708144A1 (de)
WO (1) WO2009076080A1 (de)

Cited By (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100018706A1 (en) * 2006-12-07 2010-01-28 Fan Wayne W Particles comprising a fluorinated siloxane and methods of making and using the same
US20100167965A1 (en) * 2008-12-26 2010-07-01 Bp Corporation North America Inc. Amphiphobic Proppant
US20100270021A1 (en) * 2007-12-21 2010-10-28 Baran Jr Jimmie R Methods for treating hydrocarbon-bearing formations with fluorinated polymer compositions
US20100288498A1 (en) * 2007-12-21 2010-11-18 Moore George G I Fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US20110177983A1 (en) * 2008-07-18 2011-07-21 Baran Jr Jimmie R Cationic fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US20130292118A1 (en) * 2012-05-03 2013-11-07 Halliburton Energy Services, Inc. Particulates Having Hydrophobic and Oleophobic Surfaces and Methods Relating Thereto
US8629089B2 (en) 2008-12-18 2014-01-14 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated ether compositions
US8701763B2 (en) 2008-05-05 2014-04-22 3M Innovative Properties Company Methods for treating hydrocarbon-bearing formations having brine
US8833449B2 (en) 2009-07-09 2014-09-16 3M Innovative Properties Company Methods for treating carbonate hydrocarbon-bearing formations with fluorinated amphoteric compounds
US9057012B2 (en) 2008-12-18 2015-06-16 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated phosphate and phosphonate compositions
WO2016025004A1 (en) * 2014-08-15 2016-02-18 Halliburton Energy Services, Inc. Hydrophobic surface treatment for use in subterranean formation operations
US9499737B2 (en) 2010-12-21 2016-11-22 3M Innovative Properties Company Method for treating hydrocarbon-bearing formations with fluorinated amine
US9624422B2 (en) 2010-12-20 2017-04-18 3M Innovative Properties Company Methods for treating carbonate hydrocarbon-bearing formations with fluorinated amine oxides
US9701889B2 (en) 2011-01-13 2017-07-11 3M Innovative Properties Company Methods for treating siliciclastic hydrocarbon-bearing formations with fluorinated amine oxides
US9890294B2 (en) 2012-11-19 2018-02-13 3M Innovative Properties Company Composition including a fluorinated polymer and a non-fluorinated polymer and methods of making and using the same
US10106724B2 (en) 2012-11-19 2018-10-23 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated ionic polymers
US10385261B2 (en) 2017-08-22 2019-08-20 Covestro Llc Coated particles, methods for their manufacture and for their use as proppants
US10435617B2 (en) 2015-09-03 2019-10-08 Saudi Arabian Oil Company Treatment of kerogen in subterranean formations
US10519406B2 (en) 2016-09-01 2019-12-31 Saudi Arabian Oil Company Treatment of sulfide scales
US10753190B1 (en) 2019-04-29 2020-08-25 Saudi Arabian Oil Company Forming mineral in fractures in a geological formation
US10900339B2 (en) 2019-04-23 2021-01-26 Saudi Arabian Oil Company Forming mineral in fractures in a geological formation
CN112680205A (zh) * 2019-10-17 2021-04-20 中国石油化工股份有限公司 一种表面活性剂驱油体系及制备方法
CN112680209A (zh) * 2019-10-17 2021-04-20 中国石油化工股份有限公司 一种支撑剂及制备方法
US11268373B2 (en) 2020-01-17 2022-03-08 Saudi Arabian Oil Company Estimating natural fracture properties based on production from hydraulically fractured wells
US11319478B2 (en) 2019-07-24 2022-05-03 Saudi Arabian Oil Company Oxidizing gasses for carbon dioxide-based fracturing fluids
US11339321B2 (en) 2019-12-31 2022-05-24 Saudi Arabian Oil Company Reactive hydraulic fracturing fluid
US11352548B2 (en) 2019-12-31 2022-06-07 Saudi Arabian Oil Company Viscoelastic-surfactant treatment fluids having oxidizer
US11365344B2 (en) 2020-01-17 2022-06-21 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11390796B2 (en) 2019-12-31 2022-07-19 Saudi Arabian Oil Company Viscoelastic-surfactant fracturing fluids having oxidizer
US11396625B2 (en) 2019-09-17 2022-07-26 Saudi Arabian Oil Company Coated proppant and methods of making and use thereof
US11473001B2 (en) 2020-01-17 2022-10-18 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11473009B2 (en) 2020-01-17 2022-10-18 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11492541B2 (en) 2019-07-24 2022-11-08 Saudi Arabian Oil Company Organic salts of oxidizing anions as energetic materials
US11542815B2 (en) 2020-11-30 2023-01-03 Saudi Arabian Oil Company Determining effect of oxidative hydraulic fracturing
US11549894B2 (en) 2020-04-06 2023-01-10 Saudi Arabian Oil Company Determination of depositional environments
US11573159B2 (en) 2019-01-08 2023-02-07 Saudi Arabian Oil Company Identifying fracture barriers for hydraulic fracturing
US11578263B2 (en) 2020-05-12 2023-02-14 Saudi Arabian Oil Company Ceramic-coated proppant
US11584889B2 (en) 2021-01-04 2023-02-21 Saudi Arabian Oil Company Synthetic source rock with tea
US11885790B2 (en) 2021-12-13 2024-01-30 Saudi Arabian Oil Company Source productivity assay integrating pyrolysis data and X-ray diffraction data

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US9714371B2 (en) 2005-05-02 2017-07-25 Trican Well Service Ltd. Method for making particulate slurries and particulate slurry compositions
CA2848264C (en) 2007-04-26 2015-11-10 Trican Well Service Ltd. Control of particulate entrainment by fluids
US7921911B2 (en) * 2008-12-30 2011-04-12 Schlumberger Technology Corporation Surface-modifying agents for wettability modification
CA2690768A1 (en) * 2010-01-21 2011-07-21 Trican Well Services Ltd. Compositions and methods for enhancing fluid recovery for hydraulic fracturing treatments
US9234415B2 (en) * 2010-08-25 2016-01-12 Schlumberger Technology Corporation Delivery of particulate material below ground
US8459353B2 (en) 2010-08-25 2013-06-11 Schlumberger Technology Corporation Delivery of particulate material below ground
US8448706B2 (en) 2010-08-25 2013-05-28 Schlumberger Technology Corporation Delivery of particulate material below ground
US8714248B2 (en) 2010-08-25 2014-05-06 Schlumberger Technology Corporation Method of gravel packing
CN103848955B (zh) * 2012-11-30 2015-12-09 亿利资源集团有限公司 一种疏水性树脂组合物及其制备方法和应用
US9932514B2 (en) 2014-04-25 2018-04-03 Trican Well Service Ltd. Compositions and methods for making aqueous slurry
CA2856942A1 (en) 2014-07-16 2016-01-16 Trican Well Service Ltd. Aqueous slurry for particulates transportation
CA2880646A1 (en) 2015-01-30 2016-07-30 Trican Well Service Ltd. Composition and method of using polymerizable natural oils to treat proppants

Citations (1)

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WO2006116868A1 (en) * 2005-05-02 2006-11-09 Trican Well Service Ltd. Method for making transportable aqueous slurries by particulate hydrophobicization

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US4564456A (en) * 1984-06-01 1986-01-14 Dow Corning Corporation Method of treating water to inhibit corrosion and diminish mineral deposition
US5209775A (en) * 1992-01-23 1993-05-11 Dow Corning Corporation Water repellents containing organosilicon compounds
US20070029085A1 (en) * 2005-08-05 2007-02-08 Panga Mohan K Prevention of Water and Condensate Blocks in Wells
US20070225176A1 (en) * 2006-03-27 2007-09-27 Pope Gary A Use of fluorocarbon surfactants to improve the productivity of gas and gas condensate wells
US20080051300A1 (en) * 2006-08-23 2008-02-28 Pope Gary A Compositions and method for improving the productivity of hydrocarbon producing wells
BRPI0719929A2 (pt) * 2006-12-07 2014-03-11 3M Innovative Properties Co Partículas que compreendem um siloxano fluorado e métodos de preparo e uso das mesmas

Patent Citations (1)

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Publication number Priority date Publication date Assignee Title
WO2006116868A1 (en) * 2005-05-02 2006-11-09 Trican Well Service Ltd. Method for making transportable aqueous slurries by particulate hydrophobicization

Cited By (58)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100018706A1 (en) * 2006-12-07 2010-01-28 Fan Wayne W Particles comprising a fluorinated siloxane and methods of making and using the same
US8236737B2 (en) * 2006-12-07 2012-08-07 3M Innovative Properties Company Particles comprising a fluorinated siloxane and methods of making and using the same
US8678090B2 (en) 2007-12-21 2014-03-25 3M Innovative Properties Company Methods for treating hydrocarbon-bearing formations with fluorinated polymer compositions
US20100270021A1 (en) * 2007-12-21 2010-10-28 Baran Jr Jimmie R Methods for treating hydrocarbon-bearing formations with fluorinated polymer compositions
US20100288498A1 (en) * 2007-12-21 2010-11-18 Moore George G I Fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US8418759B2 (en) 2007-12-21 2013-04-16 3M Innovative Properties Company Fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US8701763B2 (en) 2008-05-05 2014-04-22 3M Innovative Properties Company Methods for treating hydrocarbon-bearing formations having brine
US20110177983A1 (en) * 2008-07-18 2011-07-21 Baran Jr Jimmie R Cationic fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US9200102B2 (en) 2008-07-18 2015-12-01 3M Innovative Properties Company Cationic fluorinated polymer compositions and methods for treating hydrocarbon-bearing formations using the same
US9057012B2 (en) 2008-12-18 2015-06-16 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated phosphate and phosphonate compositions
US8629089B2 (en) 2008-12-18 2014-01-14 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated ether compositions
US20100167965A1 (en) * 2008-12-26 2010-07-01 Bp Corporation North America Inc. Amphiphobic Proppant
US8833449B2 (en) 2009-07-09 2014-09-16 3M Innovative Properties Company Methods for treating carbonate hydrocarbon-bearing formations with fluorinated amphoteric compounds
US9624422B2 (en) 2010-12-20 2017-04-18 3M Innovative Properties Company Methods for treating carbonate hydrocarbon-bearing formations with fluorinated amine oxides
US9499737B2 (en) 2010-12-21 2016-11-22 3M Innovative Properties Company Method for treating hydrocarbon-bearing formations with fluorinated amine
US9701889B2 (en) 2011-01-13 2017-07-11 3M Innovative Properties Company Methods for treating siliciclastic hydrocarbon-bearing formations with fluorinated amine oxides
US20130292118A1 (en) * 2012-05-03 2013-11-07 Halliburton Energy Services, Inc. Particulates Having Hydrophobic and Oleophobic Surfaces and Methods Relating Thereto
US9708527B2 (en) * 2012-05-03 2017-07-18 Halliburton Energy Services, Inc. Particulates having hydrophobic and oleophobic surfaces and methods relating thereto
US10106724B2 (en) 2012-11-19 2018-10-23 3M Innovative Properties Company Method of contacting hydrocarbon-bearing formations with fluorinated ionic polymers
US9890294B2 (en) 2012-11-19 2018-02-13 3M Innovative Properties Company Composition including a fluorinated polymer and a non-fluorinated polymer and methods of making and using the same
WO2016025004A1 (en) * 2014-08-15 2016-02-18 Halliburton Energy Services, Inc. Hydrophobic surface treatment for use in subterranean formation operations
US10012065B2 (en) 2014-08-15 2018-07-03 Halliburton Energy Services, Inc. Hydrophobic surface treatment for use in subterranean formation operations
US10435617B2 (en) 2015-09-03 2019-10-08 Saudi Arabian Oil Company Treatment of kerogen in subterranean formations
US10479927B2 (en) 2015-09-03 2019-11-19 Saudi Arabian Oil Company Treatment of kerogen in subterranean formations
US10781360B2 (en) 2015-09-03 2020-09-22 Saudi Arabian Oil Company Kerogen and organic matter degrading additive for hydraulic fracturing fluids
US11186806B2 (en) 2016-09-01 2021-11-30 Saudi Arabian Oil Company Treatment of sulfide scales
US10519406B2 (en) 2016-09-01 2019-12-31 Saudi Arabian Oil Company Treatment of sulfide scales
US10851291B2 (en) 2017-08-22 2020-12-01 Covestro Llc Coated particles, methods for their manufacture and for their use as proppants
US10647911B2 (en) 2017-08-22 2020-05-12 Covestro Llc Coated particles, methods for their manufacture and for their use as proppants
US10385261B2 (en) 2017-08-22 2019-08-20 Covestro Llc Coated particles, methods for their manufacture and for their use as proppants
US11573159B2 (en) 2019-01-08 2023-02-07 Saudi Arabian Oil Company Identifying fracture barriers for hydraulic fracturing
US10900339B2 (en) 2019-04-23 2021-01-26 Saudi Arabian Oil Company Forming mineral in fractures in a geological formation
US11028680B2 (en) * 2019-04-29 2021-06-08 Saudi Arabian Oil Company Forming mineral in fractures in a geological formation
US10753190B1 (en) 2019-04-29 2020-08-25 Saudi Arabian Oil Company Forming mineral in fractures in a geological formation
US11499090B2 (en) 2019-07-24 2022-11-15 Saudi Arabian Oil Company Oxidizers for carbon dioxide-based fracturing fluids
US11713411B2 (en) 2019-07-24 2023-08-01 Saudi Arabian Oil Company Oxidizing gasses for carbon dioxide-based fracturing fluids
US11319478B2 (en) 2019-07-24 2022-05-03 Saudi Arabian Oil Company Oxidizing gasses for carbon dioxide-based fracturing fluids
US11492541B2 (en) 2019-07-24 2022-11-08 Saudi Arabian Oil Company Organic salts of oxidizing anions as energetic materials
US11396625B2 (en) 2019-09-17 2022-07-26 Saudi Arabian Oil Company Coated proppant and methods of making and use thereof
CN112680205A (zh) * 2019-10-17 2021-04-20 中国石油化工股份有限公司 一种表面活性剂驱油体系及制备方法
CN112680209B (zh) * 2019-10-17 2022-12-09 中国石油化工股份有限公司 一种支撑剂及制备方法
CN112680209A (zh) * 2019-10-17 2021-04-20 中国石油化工股份有限公司 一种支撑剂及制备方法
US11352548B2 (en) 2019-12-31 2022-06-07 Saudi Arabian Oil Company Viscoelastic-surfactant treatment fluids having oxidizer
US11713413B2 (en) 2019-12-31 2023-08-01 Saudi Arabian Oil Company Viscoelastic-surfactant fracturing fluids having oxidizer
US11390796B2 (en) 2019-12-31 2022-07-19 Saudi Arabian Oil Company Viscoelastic-surfactant fracturing fluids having oxidizer
US11718784B2 (en) 2019-12-31 2023-08-08 Saudi Arabian Oil Company Reactive hydraulic fracturing fluid
US11339321B2 (en) 2019-12-31 2022-05-24 Saudi Arabian Oil Company Reactive hydraulic fracturing fluid
US11597867B2 (en) 2019-12-31 2023-03-07 Saudi Arabian Oil Company Viscoelastic-surfactant treatment fluids having oxidizer
US11268373B2 (en) 2020-01-17 2022-03-08 Saudi Arabian Oil Company Estimating natural fracture properties based on production from hydraulically fractured wells
US11473009B2 (en) 2020-01-17 2022-10-18 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11473001B2 (en) 2020-01-17 2022-10-18 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11719091B2 (en) 2020-01-17 2023-08-08 Saudi Arabian Oil Company Estimating natural fracture properties based on production from hydraulically fractured wells
US11365344B2 (en) 2020-01-17 2022-06-21 Saudi Arabian Oil Company Delivery of halogens to a subterranean formation
US11549894B2 (en) 2020-04-06 2023-01-10 Saudi Arabian Oil Company Determination of depositional environments
US11578263B2 (en) 2020-05-12 2023-02-14 Saudi Arabian Oil Company Ceramic-coated proppant
US11542815B2 (en) 2020-11-30 2023-01-03 Saudi Arabian Oil Company Determining effect of oxidative hydraulic fracturing
US11584889B2 (en) 2021-01-04 2023-02-21 Saudi Arabian Oil Company Synthetic source rock with tea
US11885790B2 (en) 2021-12-13 2024-01-30 Saudi Arabian Oil Company Source productivity assay integrating pyrolysis data and X-ray diffraction data

Also Published As

Publication number Publication date
EP2225344A1 (de) 2010-09-08
CN101889066A (zh) 2010-11-17
ATE547498T1 (de) 2012-03-15
WO2009076080A1 (en) 2009-06-18
CA2708144A1 (en) 2009-06-18
EP2225344B1 (de) 2012-02-29

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AS Assignment

Owner name: 3M INNOVATIVE PROPERTIES COMPANY, MINNESOTA

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:SKILDUM, JOHN D.;BARAN, JIMMIE R., JR.;FAN, WAYNE W.;AND OTHERS;SIGNING DATES FROM 20100330 TO 20100525;REEL/FRAME:024477/0433

STCB Information on status: application discontinuation

Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION