US20050193831A1 - Test method for assessing thermal mechanical fatigue performance of a test material - Google Patents
Test method for assessing thermal mechanical fatigue performance of a test material Download PDFInfo
- Publication number
- US20050193831A1 US20050193831A1 US10/792,158 US79215804A US2005193831A1 US 20050193831 A1 US20050193831 A1 US 20050193831A1 US 79215804 A US79215804 A US 79215804A US 2005193831 A1 US2005193831 A1 US 2005193831A1
- Authority
- US
- United States
- Prior art keywords
- rib
- test
- base
- preparing
- test method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000012360 testing method Methods 0.000 title claims abstract description 123
- 239000000463 material Substances 0.000 title claims abstract description 37
- 238000010998 test method Methods 0.000 title claims abstract description 32
- 230000001351 cycling effect Effects 0.000 claims description 21
- 238000001816 cooling Methods 0.000 claims description 19
- 238000010438 heat treatment Methods 0.000 claims description 17
- 229910000601 superalloy Inorganic materials 0.000 claims description 8
- 230000006835 compression Effects 0.000 claims description 6
- 238000007906 compression Methods 0.000 claims description 6
- 238000013459 approach Methods 0.000 description 12
- 230000035882 stress Effects 0.000 description 9
- 239000007789 gas Substances 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 238000011068 loading method Methods 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 238000005382 thermal cycling Methods 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011253 protective coating Substances 0.000 description 3
- 229910000951 Aluminide Inorganic materials 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 239000000567 combustion gas Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000002028 premature Effects 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 238000005050 thermomechanical fatigue Methods 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005094 computer simulation Methods 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 229910001173 rene N5 Inorganic materials 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004154 testing of material Methods 0.000 description 1
- 238000012956 testing procedure Methods 0.000 description 1
- 238000002076 thermal analysis method Methods 0.000 description 1
- 239000012720 thermal barrier coating Substances 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/32—Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0001—Type of application of the stress
- G01N2203/0005—Repeated or cyclic
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/003—Generation of the force
- G01N2203/0057—Generation of the force using stresses due to heating, e.g. conductive heating, radiative heating
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0058—Kind of property studied
- G01N2203/0069—Fatigue, creep, strain-stress relations or elastic constants
- G01N2203/0073—Fatigue
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/022—Environment of the test
- G01N2203/0222—Temperature
- G01N2203/0224—Thermal cycling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/026—Specifications of the specimen
- G01N2203/0262—Shape of the specimen
Definitions
- This invention relates to the testing of materials and, more particularly, to evaluating the thermal mechanical fatigue performance of materials used in aircraft gas turbine engines.
- air is drawn into the front of the engine, compressed by a shaft-mounted compressor, and mixed with fuel.
- the mixture is combusted, and the resulting hot combustion gases are passed through a turbine mounted on the same shaft.
- the flow of gas turns the turbine by contacting an airfoil portion of the turbine blade, which turns the shaft and provides power to the compressor.
- the hot exhaust gases flow from the back of the engine, driving it and the aircraft forward.
- There may additionally be a bypass fan that forces air around the center core of the engine, driven by a shaft extending from the turbine section.
- the components of the turbine section of the engine are repeatedly thermally cycled between lower and higher temperatures.
- the thermal cycles may be between room temperature and the operating temperature when the engine is started, operated, and shut down, or between an intermediate temperature and a higher operating temperature when the engine power output is changed between lower and higher power settings.
- Some of the components are mechanically loaded during the thermal cycling.
- the turbine blade has a complex shape, including an attachment section, an airfoil with a thin tip portion, and a platform.
- the airfoil is in the direct flow of the hot combustion gases.
- the turbine blade is typically made of an alloy that has good high temperature mechanical properties.
- thermo mechanical fatigue TMF
- the combination of thermally induced stresses, mechanically induced stresses, and the temperature extremes can combine to cause the formation and propagation of cracks in the airfoil of the turbine blade, particularly in its airfoil tip, that lead to premature failure of the turbine blade. Because the turbine blade rotates at up to 20,000 rpm, such a premature failure may lead to an unplanned removal from service or major damage of the engine.
- the present invention fulfills this need, and further provides related advantages.
- the present invention provides a technique for evaluating the thermal mechanical fatigue performance of materials and articles that are used in conditions of temperature variations and mechanical loading. This approach particularly provides a good indicator of the thermal mechanical fatigue performance of materials such as nickel-base superalloys that form turbine blades.
- the present approach is simple and inexpensive to implement.
- the test method for testing the thermal mechanical fatigue performance of a test material comprises the steps of preparing a test specimen of the test material, wherein the test specimen comprises a base, and one or more ribs extending outwardly from the base, and thermally cycling the test specimen through at least one test cycle, and preferably to a plurality of test cycles.
- the rib is heated to a higher rib temperature and thereafter cooled to a lower rib temperature.
- Higher and “lower” are used relative to each other in this context, and do not denote any specific temperatures.
- the rib may be held at the higher rib temperature for a period of time before cooling.
- the test cycle may be complex, with several stages of heating, cooling, and holding at temperature.
- the test specimen may be heated generally, or only the rib may be heated locally.
- the test specimen, and particularly the rib is evaluated for thermal mechanical fatigue damage, such as the presence of fatigue cracks. With this type of evaluation, no instrumentation of the test specimen is required during the thermal cycling.
- the test material may be of any operable type, but is typically a nickel-base superalloy test material. Such nickel-base superalloys are used in most turbine blades for aircraft gas turbine engines.
- the present approach allows such test materials to be evaluated and comparatively tested before going to the expense of fabricating the actual gas turbine components for testing.
- the present approach may also be used to evaluate the effects of different thermal and mechanical loading cycles.
- the rib of the test specimen may be solid. There may instead be one or more slots through the rib and extending parallel to the long direction of the rib. In the slotted configuration of a single slot, the rib is supported from the base at a first end of the rib and at a second end of the rib, but does not contact the base in a central portion of the rib. Where there is more than one slot, the rib is supported from its ends and also from intermediate locations along its length.
- the slots may be of the same lengths or of different lengths.
- the rib may have hollow cavities therein.
- the rib may be coated with protective coatings or may be made of an alternate material.
- the base must have a relatively large size and mass as compared with the rib, in order to properly constrain the expansion and contraction of the rib.
- a mass of the base is at least 25 times larger than a mass of the rib.
- the test specimen has a width of the base at least 5 times larger than a width of the rib, and/or a height of the base at least 3 times larger than a height of the rib.
- the rib should be maintained in compression while the rib is heated toward the higher rib temperature during the heating part of the cycle. However, the rib may go into tension if the rib compressively yields or creeps. Likewise, the rib goes into tension during cooling. This stress state is achieved by having the average rib temperature higher than the average base temperature during heating and lower during cooling, and by having the base sufficiently stiff to resisting bending loads imposed by the ribs. At least a portion of the base may be insulated, such as by packing it in insulation, to aid the thermal control and to ensure that the rib is in compression at the higher rib temperature.
- FIG. 1 is a block diagram of a method in accordance with an embodiment of the invention
- FIGS. 2-4 are a set of elevational views of a first embodiment of a test specimen, with FIG. 2 a side view, FIG. 3 a top view, and FIG. 4 an end view;
- FIG. 5 is a side view of a second embodiment of the test specimen
- FIG. 6 is a side view of a third embodiment of the test specimen
- FIG. 7 is a side view of a fourth embodiment of the test specimen.
- FIG. 8 is a perspective view of a fifth embodiment of the test specimen.
- FIG. 9 is a graph of temperature versus time for the rib and the base during heating and cooling.
- FIG. 1 depicts an embodiment of a test method for testing the thermal mechanical fatigue performance of a test material.
- the test method first includes preparing a test specimen 30 of the test material, step 20 .
- the test material is preferably a nickel-base superalloy.
- nickel-base means that the composition has more nickel present than any other element.
- the nickel-base superalloys are typically of a composition that is strengthened by the precipitation of gamma-prime phase or a related phase.
- the test material may instead be other metallic materials, a ceramic, or a combination of materials.
- FIGS. 2-4 illustrate an embodiment of the test specimen 30 .
- the test specimen 30 comprises a base 32 , and at least one rib 34 extending outwardly from the base 32 .
- the base 32 is a rectangular prism with two parallel ends 36 and four lateral faces 38 .
- the rib 34 extends outwardly from one of the lateral faces 38 .
- the base 32 must have a much larger mass than the rib 34 .
- the test specimen 30 has a mass of the base 32 at least 25 times larger than a mass of the rib 34 .
- a width WB of the base 32 is at least 5 (and often more) times larger than a width WR of the rib 34 .
- a height HB of the base 32 is at least 3 (and often more) times larger than a height HR of the rib 34 . The combination of heights and widths is selected so that the mass ratio is at least 25.
- FIGS. 5-8 depict other embodiments of the test specimen 30 .
- the embodiments are similar to that of FIGS. 2-4 , whose discussion is incorporated as appropriate, except as noted next.
- FIG. 5 there is a slot 40 through the rib 34 , extending parallel to a lengthwise direction 48 of the rib 34 . That is, the rib 34 is supported from the base 32 at a first end 42 of the rib 34 and at a second end 44 of the rib 34 .
- the rib 34 does not contact the base 32 in a central portion 46 of the rib 34 .
- the central portion 46 of the rib 34 is thereby thermally isolated from the base 32 .
- FIG. 6 is similar to that of FIG.
- a top 50 of the rib 34 comprises a strip 52 of a strip material joined to the remainder of the rib 34 , extending parallel to the lengthwise direction 48 .
- the joint of the strip 52 to the remainder of the rib 34 may be a weld, a diffusion bond, a mechanical joint, or other type of joint.
- the strip material that forms the strip 52 may be the same material as the rib material that forms the remainder of the rib 34 , or a different material.
- the approach of FIG. 7 is particularly useful in testing the performance of weldments or other types of attachments at the tip of a turbine blade.
- the embodiment of FIG. 7 having the strip 52 is illustrated in relation to the single-slot embodiment otherwise shown in FIG. 5 , but it may be used in relation to the multiple-slot embodiment of FIG. 6 , the unslotted embodiment of FIGS. 2-4 , or other operable embodiment.
- the embodiment of FIG. 8 has two ribs 34 on opposing faces 38 of the base 32 . Any of the compatible features discussed in relation to the other embodiments may be used with the embodiment of FIG. 8 .
- test specimen 30 is illustrated as rectilinear in its general shape. It may instead have other shapes, such as a cylinder or a disk.
- the rib 34 may be coated with a coating 54 such as a protective coating so that the performance of the coating on the test specimen may be evaluated.
- the coating may be, for example, an environmental coating (e.g., an aluminide or platinum aluminide coating) or a thermal barrier coating (e.g., a bond coat with an overlying ceramic thermal barrier).
- an environmental coating e.g., an aluminide or platinum aluminide coating
- a thermal barrier coating e.g., a bond coat with an overlying ceramic thermal barrier
- the rib 34 may include hollow cavities 56 therein, to simulate internal cooling passages.
- the presence of a hollow cavity 56 is illustrated in FIG. 5 , but it may be used in relation to the embodiments of FIGS. 2-4 and 6 - 8 as well.
- the test specimen 30 is thermally cycled through at least one test cycle, and typically a plurality of test cycles, step 22 .
- the test specimen 30 is heated to a higher rib temperature and thereafter cooled to a lower rib temperature.
- the test specimen 30 may also be held at the higher rib temperature and/or at the lower rib temperature for a period of time.
- FIG. 9 depicts the average temperature of the rib 34 and the base 32 during a typical test cycle including heating and cooling. Because of its smaller dimensions and thermal mass, and relatively larger surface area, the average temperature of the rib 34 leads that of the base 32 . That is, the rib 34 reaches the higher temperatures faster than does the base 32 during heating.
- the rib 34 is initially at a higher temperature than the base 32 , and then falls to the lower temperature faster than does the base 32 during the latter portion of the cooling period. The result is that the rib 34 is in compression at the higher temperatures, the desired stress state. Insulating the base 32 accentuates this temperature-difference behavior of the rib 34 relative to the base 32 .
- the test cycles may be simple in their form of temperature as a function of time, with a heating and cooling, and optional hold period.
- the test cycles may instead be more complex in their temperature-time form, with several patterns of heating, cooling, and intermediate holds during the heating or cooling.
- the heating and cooling may be accomplished generally, with the entire test specimen 30 heated and cooled as a single piece, or heating and cooling may be accomplished locally, as by preferentially heating and cooling the rib 34 .
- One virtue of the present approach is that there is no use of complex, expensive force-applying machinery or the like that would constrain the selection of the form of the temperature-time test cycle, or with the selection of the mode of heating and cooling.
- the test approach naturally accounts for the temperature-dependent effects of the material on the induced stress.
- the rib 34 is maintained in compression while the rib 34 is heated toward the higher rib temperature and is at the higher rib temperature. This result may be achieved by maintaining the base 32 at a lower temperature than the rib 34 when the rib is at the higher rib temperature.
- the base 32 may be packed in an insulation, such as a fiber or foam ceramic insulation, to further aid in controlling the rates of heat input into and heat removal from the base 32 .
- the test specimen is evaluated, step 24 , for thermal mechanical fatigue damage.
- the evaluation 24 may be of any type.
- the test specimen may be evaluated optically for the presence of fatigue cracks in the rib 34 .
- the evaluation 24 may be performed either after step 22 is complete, or at an intermediate stage of the test cycling of step 22 .
- the present approach has been reduced to practice, both with thermal analysis of the operability of the test specimen 30 and with actual testing.
- Thermal and stress analysis using computer modeling was employed to design the geometry of the test specimen and the nature of the thermal cycle to which it should be thermally cycled in order to duplicate the temperature and strain cycle of the tip of a turbine blade. This modeling ensures that the results for the test specimen simulates the turbine blade tip thermal fatigue cracking.
- the simulation included modeling the heatup of the test specimen in the heatup furnace subject to the appropriate thermal boundary conditions. In the model, the furnace and the test specimen were brought up to a specified temperature, held at that temperature, and cooled. The base was insulated on all of the four vertical faces. The faces were exposed to the furnace ambient temperature. During heating, the rib was heated by radiation and convection from the furnace. Subsequent to heatup and hold, the cooling of the test specimen was modeled.
- the rib During cooling, the rib cooled by radiation and convection to air. The temperature predictions were validated with measured thermocouple data. Stress analysis was performed by modeling the test specimen using a three-dimensional thermal-elastic-plastic analysis. The thermal exposure of the specimen caused thermal strains in the specimen and the resulting stress-strain behavior was computed using coupled thermal-stress analysis.
- a test sample according to the present design of Rene N5 nickel-base superalloy was prepared according to the present approach and tested by cycling an air furnace set at 2450° F. and room temperature. Thermal-fatigue failure was observed after 48 cycles when a 0.500 inch slot was used, and after 142 cycles when a 0.250 inch slot was used.
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
Abstract
A test method for testing the thermal mechanical fatigue performance of a test material includes preparing a test specimen of the test material, wherein the test specimen has a base, and a rib extending outwardly from the base. The test specimen is thermally cycled through at least one test cycle. In each test cycle the rib is heated to a higher rib temperature and thereafter cooled to a lower rib temperature. The test specimen is evaluated for thermal mechanical fatigue damage.
Description
- This invention relates to the testing of materials and, more particularly, to evaluating the thermal mechanical fatigue performance of materials used in aircraft gas turbine engines.
- In an aircraft gas turbine (jet) engine, air is drawn into the front of the engine, compressed by a shaft-mounted compressor, and mixed with fuel. The mixture is combusted, and the resulting hot combustion gases are passed through a turbine mounted on the same shaft. The flow of gas turns the turbine by contacting an airfoil portion of the turbine blade, which turns the shaft and provides power to the compressor. The hot exhaust gases flow from the back of the engine, driving it and the aircraft forward. There may additionally be a bypass fan that forces air around the center core of the engine, driven by a shaft extending from the turbine section.
- In service, the components of the turbine section of the engine are repeatedly thermally cycled between lower and higher temperatures. The thermal cycles may be between room temperature and the operating temperature when the engine is started, operated, and shut down, or between an intermediate temperature and a higher operating temperature when the engine power output is changed between lower and higher power settings. Some of the components are mechanically loaded during the thermal cycling.
- One of the components that is subjected to the greatest temperature extremes and the greatest mechanical loadings during thermal cycling is the turbine blade. The turbine blade has a complex shape, including an attachment section, an airfoil with a thin tip portion, and a platform. The airfoil is in the direct flow of the hot combustion gases. The turbine blade is typically made of an alloy that has good high temperature mechanical properties.
- As a result of its material of construction and the nature of its thermal and mechanical loadings during service, the turbine blade, particularly the airfoil and airfoil tip, are subject to thermo mechanical fatigue (TMF). The combination of thermally induced stresses, mechanically induced stresses, and the temperature extremes can combine to cause the formation and propagation of cracks in the airfoil of the turbine blade, particularly in its airfoil tip, that lead to premature failure of the turbine blade. Because the turbine blade rotates at up to 20,000 rpm, such a premature failure may lead to an unplanned removal from service or major damage of the engine.
- It is therefore important to evaluate the performance of the turbine blade with regard to its material of construction and the loading conditions to ensure that the turbine blade can withstand the thermal mechanical fatigue and will not fail prematurely. There are a variety of testing procedures used, including full scale tests of the turbine blades, tests of proxy specimens such as cylindrical test bars which are used in the hope that their performance will reflect the performance of the turbine blades, and accelerated tests using special test equipment. All of the available testing approaches have shortcomings. The full-scale tests are expensive, the tests of proxy specimens do not necessarily reflect the performance of the turbine blade, and accelerated tests are not a good indicators of actual service performance and do not permit a realistic evaluation of the materials and conditions. Stresses imposed in other simulative tests fail to accurately account for the complex effects of the test material in determining the stress that results due to a number of factors such as thermal expansion coefficient, elastic modulus, emissivity, thermal conductivity, and yield strength, all of which vary with temperature.
- There remains a need for an improved approach to evaluating components of gas turbine engines, as well as articles subjected to similar conditions, to evaluate their thermal mechanical fatigue performance. The present invention fulfills this need, and further provides related advantages.
- The present invention provides a technique for evaluating the thermal mechanical fatigue performance of materials and articles that are used in conditions of temperature variations and mechanical loading. This approach particularly provides a good indicator of the thermal mechanical fatigue performance of materials such as nickel-base superalloys that form turbine blades. The present approach is simple and inexpensive to implement.
- The test method for testing the thermal mechanical fatigue performance of a test material comprises the steps of preparing a test specimen of the test material, wherein the test specimen comprises a base, and one or more ribs extending outwardly from the base, and thermally cycling the test specimen through at least one test cycle, and preferably to a plurality of test cycles. In each test cycle the rib is heated to a higher rib temperature and thereafter cooled to a lower rib temperature. (“Higher” and “lower” are used relative to each other in this context, and do not denote any specific temperatures.) The rib may be held at the higher rib temperature for a period of time before cooling. The test cycle may be complex, with several stages of heating, cooling, and holding at temperature. In the thermal cycling, the test specimen may be heated generally, or only the rib may be heated locally. The test specimen, and particularly the rib, is evaluated for thermal mechanical fatigue damage, such as the presence of fatigue cracks. With this type of evaluation, no instrumentation of the test specimen is required during the thermal cycling.
- The test material may be of any operable type, but is typically a nickel-base superalloy test material. Such nickel-base superalloys are used in most turbine blades for aircraft gas turbine engines. The present approach allows such test materials to be evaluated and comparatively tested before going to the expense of fabricating the actual gas turbine components for testing. The present approach may also be used to evaluate the effects of different thermal and mechanical loading cycles.
- The rib of the test specimen may be solid. There may instead be one or more slots through the rib and extending parallel to the long direction of the rib. In the slotted configuration of a single slot, the rib is supported from the base at a first end of the rib and at a second end of the rib, but does not contact the base in a central portion of the rib. Where there is more than one slot, the rib is supported from its ends and also from intermediate locations along its length. The slots may be of the same lengths or of different lengths. The rib may have hollow cavities therein. The rib may be coated with protective coatings or may be made of an alternate material.
- The base must have a relatively large size and mass as compared with the rib, in order to properly constrain the expansion and contraction of the rib. In one embodiment, a mass of the base is at least 25 times larger than a mass of the rib. Desirably, the test specimen has a width of the base at least 5 times larger than a width of the rib, and/or a height of the base at least 3 times larger than a height of the rib.
- The rib should be maintained in compression while the rib is heated toward the higher rib temperature during the heating part of the cycle. However, the rib may go into tension if the rib compressively yields or creeps. Likewise, the rib goes into tension during cooling. This stress state is achieved by having the average rib temperature higher than the average base temperature during heating and lower during cooling, and by having the base sufficiently stiff to resisting bending loads imposed by the ribs. At least a portion of the base may be insulated, such as by packing it in insulation, to aid the thermal control and to ensure that the rib is in compression at the higher rib temperature.
- Analysis of the heat flow of the test specimen during the test cycle, as well as preliminary test results, indicates that the present approach produces a good indicator of the susceptibility of the material to thermal mechanical fatigue.
- Other features and advantages of the present invention will be apparent from the following more detailed description of the preferred embodiment, taken in conjunction with the accompanying drawings, which illustrate, by way of example, the principles of the invention. The scope of the invention is not, however, limited to this preferred embodiment.
-
FIG. 1 is a block diagram of a method in accordance with an embodiment of the invention; -
FIGS. 2-4 are a set of elevational views of a first embodiment of a test specimen, withFIG. 2 a side view,FIG. 3 a top view, andFIG. 4 an end view; -
FIG. 5 is a side view of a second embodiment of the test specimen; -
FIG. 6 is a side view of a third embodiment of the test specimen; -
FIG. 7 is a side view of a fourth embodiment of the test specimen; -
FIG. 8 is a perspective view of a fifth embodiment of the test specimen; and -
FIG. 9 is a graph of temperature versus time for the rib and the base during heating and cooling. -
FIG. 1 depicts an embodiment of a test method for testing the thermal mechanical fatigue performance of a test material. The test method first includes preparing atest specimen 30 of the test material,step 20. The test material is preferably a nickel-base superalloy. As used herein, “nickel-base” means that the composition has more nickel present than any other element. The nickel-base superalloys are typically of a composition that is strengthened by the precipitation of gamma-prime phase or a related phase. The test material may instead be other metallic materials, a ceramic, or a combination of materials. -
FIGS. 2-4 illustrate an embodiment of thetest specimen 30. Thetest specimen 30 comprises abase 32, and at least onerib 34 extending outwardly from thebase 32. As illustrated, thebase 32 is a rectangular prism with two parallel ends 36 and four lateral faces 38. Therib 34 extends outwardly from one of the lateral faces 38. - The base 32 must have a much larger mass than the
rib 34. Preferably, thetest specimen 30 has a mass of the base 32 at least 25 times larger than a mass of therib 34. In one design, a width WB of thebase 32 is at least 5 (and often more) times larger than a width WR of therib 34. In another embodiment, a height HB of thebase 32 is at least 3 (and often more) times larger than a height HR of therib 34. The combination of heights and widths is selected so that the mass ratio is at least 25. -
FIGS. 5-8 depict other embodiments of thetest specimen 30. The embodiments are similar to that ofFIGS. 2-4 , whose discussion is incorporated as appropriate, except as noted next. In the embodiment ofFIG. 5 , there is aslot 40 through therib 34, extending parallel to alengthwise direction 48 of therib 34. That is, therib 34 is supported from the base 32 at afirst end 42 of therib 34 and at asecond end 44 of therib 34. Therib 34 does not contact the base 32 in acentral portion 46 of therib 34. Thecentral portion 46 of therib 34 is thereby thermally isolated from thebase 32. The embodiment ofFIG. 6 is similar to that ofFIG. 5 , except that there are multiple (i.e., two or more)slots 40 in therib 34. Therib 34 is thereby supported from the base 32 at theends rib 34, and also at one or more additional locations along the length of therib 34. Themultiple slots 40 may be of the same length, as illustrated, or of different lengths to provide a range of sensitivities. In the embodiment ofFIG. 7 , a top 50 of therib 34 comprises astrip 52 of a strip material joined to the remainder of therib 34, extending parallel to thelengthwise direction 48. The joint of thestrip 52 to the remainder of therib 34 may be a weld, a diffusion bond, a mechanical joint, or other type of joint. The strip material that forms thestrip 52 may be the same material as the rib material that forms the remainder of therib 34, or a different material. The approach ofFIG. 7 is particularly useful in testing the performance of weldments or other types of attachments at the tip of a turbine blade. The embodiment ofFIG. 7 having thestrip 52 is illustrated in relation to the single-slot embodiment otherwise shown inFIG. 5 , but it may be used in relation to the multiple-slot embodiment ofFIG. 6 , the unslotted embodiment ofFIGS. 2-4 , or other operable embodiment. The embodiment ofFIG. 8 has tworibs 34 on opposingfaces 38 of thebase 32. Any of the compatible features discussed in relation to the other embodiments may be used with the embodiment ofFIG. 8 . - In these embodiments of
FIGS. 2-8 , thetest specimen 30 is illustrated as rectilinear in its general shape. It may instead have other shapes, such as a cylinder or a disk. - The
rib 34 may be coated with acoating 54 such as a protective coating so that the performance of the coating on the test specimen may be evaluated. The coating may be, for example, an environmental coating (e.g., an aluminide or platinum aluminide coating) or a thermal barrier coating (e.g., a bond coat with an overlying ceramic thermal barrier). The presence of theprotective coating 54 is illustrated inFIG. 7 , but it may be used in relation to the embodiments ofFIGS. 2-6 and 8 as well. - The
rib 34 may include hollow cavities 56 therein, to simulate internal cooling passages. The presence of a hollow cavity 56 is illustrated inFIG. 5 , but it may be used in relation to the embodiments ofFIGS. 2-4 and 6-8 as well. - Returning to the discussion of
FIG. 1 , thetest specimen 30 is thermally cycled through at least one test cycle, and typically a plurality of test cycles,step 22. In each test cycle, thetest specimen 30 is heated to a higher rib temperature and thereafter cooled to a lower rib temperature. Thetest specimen 30 may also be held at the higher rib temperature and/or at the lower rib temperature for a period of time.FIG. 9 depicts the average temperature of therib 34 and the base 32 during a typical test cycle including heating and cooling. Because of its smaller dimensions and thermal mass, and relatively larger surface area, the average temperature of therib 34 leads that of thebase 32. That is, therib 34 reaches the higher temperatures faster than does thebase 32 during heating. During cooling, therib 34 is initially at a higher temperature than the base 32, and then falls to the lower temperature faster than does thebase 32 during the latter portion of the cooling period. The result is that therib 34 is in compression at the higher temperatures, the desired stress state. Insulating thebase 32 accentuates this temperature-difference behavior of therib 34 relative to thebase 32. - The test cycles may be simple in their form of temperature as a function of time, with a heating and cooling, and optional hold period. The test cycles may instead be more complex in their temperature-time form, with several patterns of heating, cooling, and intermediate holds during the heating or cooling. There is no limitation on the types of cycles that may be used in
step 22. The heating and cooling may be accomplished generally, with theentire test specimen 30 heated and cooled as a single piece, or heating and cooling may be accomplished locally, as by preferentially heating and cooling therib 34. One virtue of the present approach is that there is no use of complex, expensive force-applying machinery or the like that would constrain the selection of the form of the temperature-time test cycle, or with the selection of the mode of heating and cooling. Another virtue is that the test approach naturally accounts for the temperature-dependent effects of the material on the induced stress. Desirably, therib 34 is maintained in compression while therib 34 is heated toward the higher rib temperature and is at the higher rib temperature. This result may be achieved by maintaining the base 32 at a lower temperature than therib 34 when the rib is at the higher rib temperature. The base 32 may be packed in an insulation, such as a fiber or foam ceramic insulation, to further aid in controlling the rates of heat input into and heat removal from thebase 32. - The test specimen is evaluated,
step 24, for thermal mechanical fatigue damage. Theevaluation 24 may be of any type. For example, the test specimen may be evaluated optically for the presence of fatigue cracks in therib 34. Theevaluation 24 may be performed either afterstep 22 is complete, or at an intermediate stage of the test cycling ofstep 22. - The present approach has been reduced to practice, both with thermal analysis of the operability of the
test specimen 30 and with actual testing. - Thermal and stress analysis using computer modeling was employed to design the geometry of the test specimen and the nature of the thermal cycle to which it should be thermally cycled in order to duplicate the temperature and strain cycle of the tip of a turbine blade. This modeling ensures that the results for the test specimen simulates the turbine blade tip thermal fatigue cracking. The simulation included modeling the heatup of the test specimen in the heatup furnace subject to the appropriate thermal boundary conditions. In the model, the furnace and the test specimen were brought up to a specified temperature, held at that temperature, and cooled. The base was insulated on all of the four vertical faces. The faces were exposed to the furnace ambient temperature. During heating, the rib was heated by radiation and convection from the furnace. Subsequent to heatup and hold, the cooling of the test specimen was modeled. During cooling, the rib cooled by radiation and convection to air. The temperature predictions were validated with measured thermocouple data. Stress analysis was performed by modeling the test specimen using a three-dimensional thermal-elastic-plastic analysis. The thermal exposure of the specimen caused thermal strains in the specimen and the resulting stress-strain behavior was computed using coupled thermal-stress analysis.
- A test sample according to the present design of Rene N5 nickel-base superalloy was prepared according to the present approach and tested by cycling an air furnace set at 2450° F. and room temperature. Thermal-fatigue failure was observed after 48 cycles when a 0.500 inch slot was used, and after 142 cycles when a 0.250 inch slot was used.
- Although a particular embodiment of the invention has been described in detail for purposes of illustration, various modifications and enhancements may be made without departing from the spirit and scope of the invention. Accordingly, the invention is not to be limited except as by the appended claims.
Claims (25)
1. A test method for testing the thermal mechanical fatigue performance of a test material, the test method comprising the steps of:
preparing a test specimen of the test material, wherein the test specimen comprises
a base, and
a rib extending outwardly from the base;
thermally cycling the test specimen through at least one test cycle, wherein in each test cycle the rib is heated to a higher rib temperature and thereafter cooled to a lower rib temperature: and
evaluating the test specimen for thermal mechanical fatigue damage.
2. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen of a nickel-base superalloy test material.
3. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen with two ribs extending outwardly from the base.
4. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen with at least one slot in the rib, wherein each slot extends parallel to a lengthwise direction of the rib.
5. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen with exactly one slot in the rib extending parallel to a lengthwise direction of the rib, so that the rib is supported from the base at a first end of the rib and at a second end of the rib, but does not contact the base in a central portion of the rib.
6. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen with more than one slot in the rib, wherein each slot extends parallel to a lengthwise direction of the rib.
7. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen having a strip material joined to a remainder of the rib and extending parallel to a lengthwise direction of the rib, wherein the strip material is different from a rib material that forms a remainder of the rib.
8. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen having a mass of the base at least 25 times larger than a mass of the rib.
9. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen having a width of the base at least 5 times larger than a width of the rib.
10. The test method of claim 1 , wherein the step of preparing includes the step of
preparing the test specimen having a height of the base at least 3 times larger than a height of the rib.
11. The test method of claim 1 , wherein the step of thermally cycling includes the step of
maintaining the rib in compression while the rib is at the higher rib temperature.
12. The test method of claim 1 , wherein the step of thermally cycling includes the step of
maintaining the base at a lower temperature than the rib when the rib is heated toward the higher rib temperature.
13. The test method of claim 1 , wherein the step of thermally cycling includes the step of
thermally cycling the test specimen in a plurality of test cycles.
14. The test method of claim 1 , wherein the step of thermally cycling includes the step of
thermally cycling the test specimen by general heating.
15. The test method of claim 1 , wherein the step of thermally cycling includes the step of
thermally cycling the test specimen by local heating of the rib.
16. The test method of claim 1 , wherein the step of thermally cycling includes the step of
heating the rib to the higher rib temperature, holding the rib at the higher rib temperature for a period of time, and thereafter cooling the rib to a lower rib temperature.
17. The test method of claim 1 , including an additional step, prior to the step of thermally cycling, of
insulating at least a portion of the base.
18. The test method of claim 1 , wherein the step of evaluating includes the step of
evaluating the test specimen optically for a presence of fatigue cracks in the rib.
19. A test method for testing the thermal mechanical fatigue performance of a test material, the test method comprising the steps of:
preparing a test specimen of the test material, wherein the test specimen comprises
a base, and
a rib extending outwardly from the base, wherein the rib includes a slot therein, so that the rib is supported from the base at a first end of the rib and at a second end of the rib, but does not contact the base in a central portion of the rib;
thermally cycling the test specimen in at least one test cycle, wherein in each test cycle the rib is heated to a higher rib temperature and thereafter cooled to a lower rib temperature, and wherein the rib is maintained in compression while the rib is heated toward the higher rib temperature; and
evaluating the test specimen for thermal mechanical fatigue damage.
20. The test method of claim 19 , wherein the step of preparing includes the step of
preparing the test specimen of a nickel-base superalloy test material.
21. The test method of claim 19 , wherein the step of preparing includes the step of
preparing the test specimen having a mass of the base at least 25 times larger than a mass of the rib.
22. The test method of claim 19 , including an additional step, prior to the step of thermally cycling, of
insulating at least a portion of the base.
23. The test method of claim 19 , wherein the step of thermally cycling includes the step of
maintaining the base at a lower temperature than the rib when the rib is at the higher rib temperature.
24. The test method of claim 19 , wherein the step of thermally cycling includes the step of
thermally cycling the test specimen in a plurality of test cycles.
25. The test method of claim 1 , wherein the step of thermally cycling includes the step of
thermally cycling without the use of force-applying machinery.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/792,158 US6935187B1 (en) | 2004-03-03 | 2004-03-03 | Test method for assessing thermal mechanical fatigue performance of a test material |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/792,158 US6935187B1 (en) | 2004-03-03 | 2004-03-03 | Test method for assessing thermal mechanical fatigue performance of a test material |
Publications (2)
Publication Number | Publication Date |
---|---|
US6935187B1 US6935187B1 (en) | 2005-08-30 |
US20050193831A1 true US20050193831A1 (en) | 2005-09-08 |
Family
ID=34861982
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/792,158 Expired - Fee Related US6935187B1 (en) | 2004-03-03 | 2004-03-03 | Test method for assessing thermal mechanical fatigue performance of a test material |
Country Status (1)
Country | Link |
---|---|
US (1) | US6935187B1 (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070042310A1 (en) * | 2005-06-15 | 2007-02-22 | Daniel Clark | Method and apparatus for the treatment of a component |
US8215181B1 (en) | 2008-09-04 | 2012-07-10 | Rolls-Royce North American Technologies, Inc. | Evaluation technique for bonded, dual wall static and rotating airfoil materials |
EP2662682A3 (en) * | 2012-05-10 | 2018-01-10 | Rolls-Royce plc | A method of fatigue testing a component |
WO2023192585A1 (en) * | 2022-03-31 | 2023-10-05 | University Of Tennessee Research Foundation | Systems and methods for measuring thermal characteristics of an object |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7658588B1 (en) * | 2006-01-27 | 2010-02-09 | Florida Turbine Technologies, Inc. | Optimized blade tip clearance process for a rub tolerant design |
US8005655B2 (en) * | 2008-02-26 | 2011-08-23 | Kimberly-Clark Worldwide, Inc. | Thermal comfort model having multiple fabric layers |
US7516674B1 (en) * | 2008-08-26 | 2009-04-14 | International Business Machines Corporation | Method and apparatus for thermally induced testing of materials under transient temperature |
EP2187005B1 (en) * | 2008-11-14 | 2015-04-01 | Siemens Aktiengesellschaft | Method of making a turbine blade holder for a device to determine flow quantities |
US9632046B2 (en) | 2014-02-05 | 2017-04-25 | Fracturelab Llc | Apparatus and method for assessing thermo-mechanical fatigue related phenomena within a test material |
CN110579419B (en) * | 2019-08-28 | 2021-07-13 | 安徽江淮汽车集团股份有限公司 | Low cycle fatigue reliability test method and device |
CN111060408B (en) * | 2019-12-24 | 2022-04-22 | 合肥通用机械研究院有限公司 | Strain-controlled thermo-mechanical fatigue performance testing method |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3795134A (en) * | 1972-03-30 | 1974-03-05 | Nasa | Anti-buckling fatigue test assembly |
US4748854A (en) * | 1986-06-10 | 1988-06-07 | Systran Corporation | Fatigue test apparatus |
US4933239A (en) * | 1989-03-06 | 1990-06-12 | United Technologies Corporation | Aluminide coating for superalloys |
US5967660A (en) * | 1997-06-06 | 1999-10-19 | Ford Global Technologies, Inc. | Accelerated thermal fatigue testing of engine combustion chambers |
US5980206A (en) * | 1996-05-31 | 1999-11-09 | Sikorsky Aircraft Corporation | Monolithic structure having improved flaw tolerance |
US5980103A (en) * | 1995-10-24 | 1999-11-09 | Kabushiki Kaisha Toyota Chuo Kenkyusho | Apparatus and method for testing thermal fatigue resistance |
US6595068B2 (en) * | 2000-02-25 | 2003-07-22 | Thomas E. Brovold | Compact hollow cylinder tensile tester |
US6761073B2 (en) * | 1999-04-13 | 2004-07-13 | Matsushita Electric Industrial Co., Ltd. | Strain detector having water-protective layer |
-
2004
- 2004-03-03 US US10/792,158 patent/US6935187B1/en not_active Expired - Fee Related
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3795134A (en) * | 1972-03-30 | 1974-03-05 | Nasa | Anti-buckling fatigue test assembly |
US4748854A (en) * | 1986-06-10 | 1988-06-07 | Systran Corporation | Fatigue test apparatus |
US4933239A (en) * | 1989-03-06 | 1990-06-12 | United Technologies Corporation | Aluminide coating for superalloys |
US5980103A (en) * | 1995-10-24 | 1999-11-09 | Kabushiki Kaisha Toyota Chuo Kenkyusho | Apparatus and method for testing thermal fatigue resistance |
US5980206A (en) * | 1996-05-31 | 1999-11-09 | Sikorsky Aircraft Corporation | Monolithic structure having improved flaw tolerance |
US5967660A (en) * | 1997-06-06 | 1999-10-19 | Ford Global Technologies, Inc. | Accelerated thermal fatigue testing of engine combustion chambers |
US6761073B2 (en) * | 1999-04-13 | 2004-07-13 | Matsushita Electric Industrial Co., Ltd. | Strain detector having water-protective layer |
US6595068B2 (en) * | 2000-02-25 | 2003-07-22 | Thomas E. Brovold | Compact hollow cylinder tensile tester |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070042310A1 (en) * | 2005-06-15 | 2007-02-22 | Daniel Clark | Method and apparatus for the treatment of a component |
US7759614B2 (en) * | 2005-06-15 | 2010-07-20 | Rolls-Royce Plc | Method and apparatus for the treatment of a component |
US8215181B1 (en) | 2008-09-04 | 2012-07-10 | Rolls-Royce North American Technologies, Inc. | Evaluation technique for bonded, dual wall static and rotating airfoil materials |
EP2662682A3 (en) * | 2012-05-10 | 2018-01-10 | Rolls-Royce plc | A method of fatigue testing a component |
WO2023192585A1 (en) * | 2022-03-31 | 2023-10-05 | University Of Tennessee Research Foundation | Systems and methods for measuring thermal characteristics of an object |
Also Published As
Publication number | Publication date |
---|---|
US6935187B1 (en) | 2005-08-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US8419270B2 (en) | Systems and methods for producing thermal mechanical fatigue on gas turbine rotors in a spin test environment | |
US6935187B1 (en) | Test method for assessing thermal mechanical fatigue performance of a test material | |
US7204153B2 (en) | Apparatus and a method for testing attachment features of components | |
CN111795901B (en) | Test method for simulating service damage of turbine blade material | |
CN110032795A (en) | Crystal Nickel-based Superalloy heat fatigue cracking initiating life prediction technique | |
Weser et al. | Advanced experimental and analytical investigations on combined cycle fatigue (CCF) of conventional cast and single-crystal gas turbine blades | |
Mauget et al. | Development and use of a new burner rig facility to mimic service loading conditions of Ni-based single crystal superalloys | |
McKnight et al. | Turbine blade tip durability analysis | |
Kupkovits | Thermomechanical fatigue behavior of the directionally-solidified nickel-base superalloy CM247LC | |
CN110096769A (en) | A kind of engine single crystal blade Thermomechanical Fatigue Life fast evaluation method | |
Manetti et al. | The dynamic influence of crystal orientation on a second generation single crystal material for turbine buckets | |
Bonnand et al. | Complex thermo-mechanical approaches to study the behavior of high-temperature alloys | |
Busse et al. | A finite element study of the effect of crystal orientation and misalignment on the crack driving force in a single-crystal superalloy | |
RU2724356C1 (en) | Turbo-machine disc locking assembly strength test device | |
Haubert et al. | High pressure turbine blade life sensitivity | |
Spera et al. | Thermal Fatigue Testing of Simulated Turbine Blades | |
Nurse et al. | Experimental determination of stress intensity factors for cracks in turbine discs | |
Lai et al. | Development of a thermal fatigue test bench for cylinder head materials | |
RU2726137C1 (en) | Turbomachine disc locking assembly strength test method | |
Bizon et al. | Thermal fatigue testing of simulated turbine blades | |
Filippini et al. | Coating Pre-Cracking Effect in Combined Cycle Fatigue Tests of Superalloys for Gas Turbine Blades | |
CN118173208A (en) | Prediction method capable of realizing reverse thrust of creep life of blade material of gas turbine | |
Kaufman | Elastic-plastic finite-element analyses of thermally cycled single-edge wedge specimens | |
SOECHTING et al. | Turbine airfoil LCF life prediction verification | |
Mabru et al. | Influence of coating on the thermal fatigue resistance of a Ni-based superalloy |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
AS | Assignment |
Owner name: GENERAL ELECTRIC COMPANY, NEW YORK Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:GORMAN, MARK DANIEL;SRIVATSA, SHESH KRISHNA;WRIGHT, PHLLEMON KENNARD, III;AND OTHERS;REEL/FRAME:015049/0393;SIGNING DATES FROM 20040224 TO 20040301 |
|
FEPP | Fee payment procedure |
Free format text: PAYOR NUMBER ASSIGNED (ORIGINAL EVENT CODE: ASPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY |
|
REMI | Maintenance fee reminder mailed | ||
LAPS | Lapse for failure to pay maintenance fees | ||
STCH | Information on status: patent discontinuation |
Free format text: PATENT EXPIRED DUE TO NONPAYMENT OF MAINTENANCE FEES UNDER 37 CFR 1.362 |
|
FP | Lapsed due to failure to pay maintenance fee |
Effective date: 20090830 |