US1997919A - Centrifuge - Google Patents

Centrifuge Download PDF

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Publication number
US1997919A
US1997919A US635997A US63599732A US1997919A US 1997919 A US1997919 A US 1997919A US 635997 A US635997 A US 635997A US 63599732 A US63599732 A US 63599732A US 1997919 A US1997919 A US 1997919A
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Prior art keywords
cup
head
support
centrifuge
bottle
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Expired - Lifetime
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US635997A
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George J Strezynski
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De Laval Separator Co
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De Laval Separator Co
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Priority to US635997A priority Critical patent/US1997919A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B5/00Other centrifuges
    • B04B5/04Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers
    • B04B5/0407Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers for liquids contained in receptacles
    • B04B5/0414Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers for liquids contained in receptacles comprising test tubes
    • B04B5/0421Radial chamber apparatus for separating predominantly liquid mixtures, e.g. butyrometers for liquids contained in receptacles comprising test tubes pivotably mounted

Definitions

  • My invention is an improvement in centrifuges of the type, often called bottle centrifuges, in which small samples, in some machinessmaller than 10 cc. and in others as large as ,100 00., are
  • each of these glass bottles is generally placed in a metal cup which has, near its upper end, -a pair of trunnions supported by recesses in a revolving central head. These trunnions, because they concentrate great forces at two points, must be connectedto a strongring to distribute these forces around the circumference of the cup. This ring increases the weight of the cup and necessitates greater strength in the head. With speeds of 1500-2000 B. P. M. these forces are not excessive, but when speeds of 6000 R. P. M. and higher are attempted, they become quite serious.
  • the object of my invention is the provision of a cup which is much lighter, for equal strength,
  • Fig. l is a top view and Fig. 2 a side view, partly in section, of one of my improved centrifuge heads with two tubes in the position assumed when rotating.
  • Fig. 3 is a similar view showing the position assumed by the cups when at rest.
  • Fig. 4 is a section taken through a cup and the head in the plane A@ of Fig. l, and showing particularly the area of support of the flange on the cup by the head of themachine.
  • a cup-carrying head a is supported and driven by a spindle b.
  • the upper part c of the head is of smaller diameter than the lower part and has across its center a semi-circular bottomed groove (1 with smaller semi-circular bottomed ends e
  • I have counterbored at f to receive flanges g around the 1932, seria No. 635,997 (01. 233-26) large ends of frustro-conical cups h adapted to support and carry bottles 2'.
  • the lower part of the head is made of great mass in accordance with the principle of my copending application, Serial Number 634,674, filed September 24, 1932.
  • the outside diameter ofthe wide end of the body of the cup is mm. and of the flange mm.,' and the contact between the flange and its support extends approximately 240 ofthe circumference.
  • a centrifuge comprising a rotatable head having a central body portion and a disk portion extending horizontally beyond the central body,
  • the central body being provided with a groove extending radially of the head and having a semicircular bottom which is abruptly contracted near its outer end, the smaller bottomed end being counterbored throughout its semi-circular portion to afford a support for the flange of a bottle-supporting cup, said support being operative, when said head is rotating, to support a cup in a position at right angles to the axis of rotation of the head, the head having clearance to permit a cup to tilt and, while said head is not rotating, to rest upon the disk portion of the body.
  • a bottle centrifuge the combination, with a bottle-supporting cup having a'flange around one end, of a rotatable head having a central body portion and a disk portion extending horizontally beyond the central body,'the body beingprovided with an open top socket adapted to support more than half the annular area of the cup flange and, during rotation. support the cup at its inner end in a horizontal position with its outer end unsupported and overlying said disk portion, the socket having, below the level of the body of the socket, clearance to allow a cup to tilt, said disk portion of the head then affording a support for the cup.
  • a bottle centrifuge the combination with a frustro-conical bottle supporting cup having a flange around its large end, of a rotatable cupcarrying head provided with a socket rigid therewith adapted to support more than half and less than three-quarters of the annular area of the flange and having, below the level of the bottom of the socket, clearance to allow a cup to drop substantially below a horizontal position.
  • a centrifuge comprising a one-piece rotatable head provided with a groove extending radially of the head, said groove having a spuricir- 'c-ular bottom which is abruptly contracted near its outer end, the smaller bottomed end being counterbored throughout its semi eiroul-ar portion to afford a cup flange support that is operative, when said head is rotating, to support a cup in a position at right angles to the axis of rotation of the head, the head having clearance to permit a cup to drop substantially below a horizontal position.
  • a bottle centrifuge the combination with a flanged bottle-supporting cup, of a rotatable head provided with a diametric groove, having opposing side Walls and a semi-circumferential bottom and an open top, the head having inwardly extending shoulders extending along the opposite oute'r ends of the grooves, said shoulders being counterbored along their inner faces line with the semi-circular parts of the grooves to form cup flange supports adapted to support cups in an angular position while at rest and in a radial position during rapid rotation GEORGE J. 'ST-REZYNSKI.

Description

April 16, 1935. G. J. STREZYNSKI CENTRIFUGE Fi led Oct. 5, 1932 a fi m; M R WWW g 6 7 w e d m F Patented Apr. 16, 1935 PATENT OFFICE CENTRIFUGE George J. Strczynski, Poughkeepsie, N. Y., as-
signor to The De Laval Separator Company, New York; N. Y., a corporation of New Jersey Application October 3,
7 Claims.
My invention is an improvement in centrifuges of the type, often called bottle centrifuges, in which small samples, in some machinessmaller than 10 cc. and in others as large as ,100 00., are
' placed in special shaped glass bottles and rotated at high speed to generate a centrifugal force which separatesthe ingredients of different specific gravity, the proportions of which are then read from ascale marked on the bottle. Each of these glass bottles is generally placed in a metal cup which has, near its upper end, -a pair of trunnions supported by recesses in a revolving central head. These trunnions, because they concentrate great forces at two points, must be connectedto a strongring to distribute these forces around the circumference of the cup. This ring increases the weight of the cup and necessitates greater strength in the head. With speeds of 1500-2000 B. P. M. these forces are not excessive, but when speeds of 6000 R. P. M. and higher are attempted, they become quite serious.
The object of my invention is the provision of a cup which is much lighter, for equal strength,
than prior cups and the provision of a head especially adapted to support such a cup.
application, Serial Number1626,037, filed July 29, 1932, of A. E. Flowers,- it is not necessary that the bottles shall turn, as the machine approaches rest, until their axes are vertical. They need turn only until their axes are to from the horizontal. found it practicable to support the cups, not from trunnions, but by a relatively small flange encircling the large end of the cup and resting in a recess in a comparatively simple and massive supporting head.
In the accompanying drawing, which illustrates a preferred embodiment of my invention:
Fig. l is a top view and Fig. 2 a side view, partly in section, of one of my improved centrifuge heads with two tubes in the position assumed when rotating. Fig. 3 is a similar view showing the position assumed by the cups when at rest. Fig. 4 is a section taken through a cup and the head in the plane A@ of Fig. l, and showing particularly the area of support of the flange on the cup by the head of themachine.
A cup-carrying head a is supported and driven by a spindle b. The upper part c of the head is of smaller diameter than the lower part and has across its center a semi-circular bottomed groove (1 with smaller semi-circular bottomed ends e With one type of bottle shown in a co-pending Using bottles of this character, I have counterbored at f to receive flanges g around the 1932, seria No. 635,997 (01. 233-26) large ends of frustro-conical cups h adapted to support and carry bottles 2'.
When at rest, the cups h and bottles i assume the position shown in Fig. 3.. When revolving, centrifugal force causes the cups and bottles to assume the position shown in Fig. 2, in which position the flanges g fit closely in the counterbores j and are supported on more than half the area of the annular surface adjacent to the conical part of the cup.
The lower part of the head is made of great mass in accordance with the principle of my copending application, Serial Number 634,674, filed September 24, 1932.
As an example of suitable dimensions, in one size of machine carrying 10 cc. bottles, the outside diameter ofthe wide end of the body of the cup is mm. and of the flange mm.,' and the contact between the flange and its support extends approximately 240 ofthe circumference.
In a centrifuge and cup embodying the invention, it has been found possible to rotate the centrifuge at 18000 R. P. M. without the production of excessive forces.
What I claim and desire to protect by Letters Patent is:
1. A centrifuge comprising a rotatable head having a central body portion and a disk portion extending horizontally beyond the central body,
the central body being provided with a groove extending radially of the head and having a semicircular bottom which is abruptly contracted near its outer end, the smaller bottomed end being counterbored throughout its semi-circular portion to afford a support for the flange of a bottle-supporting cup, said support being operative, when said head is rotating, to support a cup in a position at right angles to the axis of rotation of the head, the head having clearance to permit a cup to tilt and, while said head is not rotating, to rest upon the disk portion of the body.
2. In a bottle centrifuge, the combination, with a bottle-supporting cup having a'flange around one end, of a rotatable head having a central body portion and a disk portion extending horizontally beyond the central body,'the body beingprovided with an open top socket adapted to support more than half the annular area of the cup flange and, during rotation. support the cup at its inner end in a horizontal position with its outer end unsupported and overlying said disk portion, the socket having, below the level of the body of the socket, clearance to allow a cup to tilt, said disk portion of the head then affording a support for the cup.
3. In a bottle centrifuge, the combination, with a flanged frustro-conical bottle supporting cup, of a rotatable head provided with a groove extending radially of the head, said groove having a semi-circular bottom which is abruptly contracted near its outer end, the smaller bottomed end being counterbored throughout its semi-circular portion to afford a cup flange support that is operative, when said head is rotating, to support a cup in a position at right angles to the axis of rotation of the head, the head having clearance to permit a cup to drop substantially below a horizontal position.
4. In a bottle centrifuge, the combination with a frustro-conical bottle supporting cup having a flange around its large end, of a rotatable cupcarrying head provided with a socket rigid therewith adapted to support more than half and less than three-quarters of the annular area of the flange and having, below the level of the bottom of the socket, clearance to allow a cup to drop substantially below a horizontal position.
5. A centrifuge comprising a one-piece rotatable head provided with a groove extending radially of the head, said groove having a seinicir- 'c-ular bottom which is abruptly contracted near its outer end, the smaller bottomed end being counterbored throughout its semi eiroul-ar portion to afford a cup flange support that is operative, when said head is rotating, to support a cup in a position at right angles to the axis of rotation of the head, the head having clearance to permit a cup to drop substantially below a horizontal position.
6. In a bottle centrifuge, the combination with a flanged bottle-supporting cup, of a rotatable head provided with a groove arcuate in cross section with its axis at right angles to the axis of rotation of the head and having its outer end contracted to form a shoulder which is arcuately counterbored throughout more than 180 and less than 270 to support said flanged cup in a radial position whilerotating-and in an inclined position when at rest. 7
'7. In a bottle centrifuge, the combination with a flanged bottle-supporting cup, of a rotatable head provided with a diametric groove, having opposing side Walls and a semi-circumferential bottom and an open top, the head having inwardly extending shoulders extending along the opposite oute'r ends of the grooves, said shoulders being counterbored along their inner faces line with the semi-circular parts of the grooves to form cup flange supports adapted to support cups in an angular position while at rest and in a radial position during rapid rotation GEORGE J. 'ST-REZYNSKI.
US635997A 1932-10-03 1932-10-03 Centrifuge Expired - Lifetime US1997919A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3377021A (en) * 1965-05-17 1968-04-09 Internat Equipment Company Centrifuge rotors, buckets and combinations of such buckets and rotors
US3687359A (en) * 1971-01-07 1972-08-29 Damon Corp Centrifuge rotor
EP0177849A2 (en) * 1984-10-01 1986-04-16 E.I. Du Pont De Nemours And Company Top loading swinging bucket centrifuge rotor having knife edge pivots
US4585433A (en) * 1984-10-01 1986-04-29 E. I. Du Pont De Nemours And Company Sample container for a top loading swinging bucket centrifuge rotor
US4585434A (en) * 1984-10-01 1986-04-29 E. I. Du Pont De Nemours And Company Top loading swinging bucket centrifuge rotor having knife edge pivots
US4718885A (en) * 1986-12-18 1988-01-12 E. I. Du Pont De Nemours And Company Swinging bucket centrifuge rotor having an uninterrupted knife edge pivot

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3377021A (en) * 1965-05-17 1968-04-09 Internat Equipment Company Centrifuge rotors, buckets and combinations of such buckets and rotors
US3687359A (en) * 1971-01-07 1972-08-29 Damon Corp Centrifuge rotor
EP0177849A2 (en) * 1984-10-01 1986-04-16 E.I. Du Pont De Nemours And Company Top loading swinging bucket centrifuge rotor having knife edge pivots
US4585433A (en) * 1984-10-01 1986-04-29 E. I. Du Pont De Nemours And Company Sample container for a top loading swinging bucket centrifuge rotor
US4585434A (en) * 1984-10-01 1986-04-29 E. I. Du Pont De Nemours And Company Top loading swinging bucket centrifuge rotor having knife edge pivots
EP0177849A3 (en) * 1984-10-01 1987-05-06 E.I. Du Pont De Nemours And Company Top loading swinging bucket centrifuge rotor having knife edge pivots
US4718885A (en) * 1986-12-18 1988-01-12 E. I. Du Pont De Nemours And Company Swinging bucket centrifuge rotor having an uninterrupted knife edge pivot

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