US1923896A - Mining soluble salt - Google Patents

Mining soluble salt Download PDF

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US1923896A
US1923896A US574149A US57414931A US1923896A US 1923896 A US1923896 A US 1923896A US 574149 A US574149 A US 574149A US 57414931 A US57414931 A US 57414931A US 1923896 A US1923896 A US 1923896A
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solvent
air
tube
salt
level
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Edward N Trump
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    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/28Dissolving minerals other than hydrocarbons, e.g. by an alkaline or acid leaching agent

Definitions

  • the object is to provide a new and useful 5 method of operation and arrangement of well casings which will control the level of water or other liquid, while it is dissolving salts or other soluble minerals to produce brine or other solutions.
  • I am enabled to dissolve out a section of the bottom layers of the bed of minerals such asrock salt, sulphur or potash salts and am thus able to afterwards attack succeeding upper layers of the salts from below.
  • the object of my invention is to provide a method of dissolving a section of the lower part of the bed by attacking it radially from the well for a very limited height.
  • My invention consists of the maintenance of a layer of air, gas or other fluid medium which will float on the liquid protecting the roof of the cavity and preventing the liquid from coming in contact with it.
  • This layer is formed by introducing the medium so as to force the liquid down to the desired level and to'provide a surplus over the volume of medium so required which will be absorbed by the liquid so that the escape of the surplus will automatically control the level.
  • Fig. 1 is a diagrammatic vertical section showing one form of embodiment.
  • Fig. 2 is a similar view of another form.
  • Fig. 3 is a similar view of another form.
  • Fig. 4 is a similar. view of another form.
  • Fig. 1 The well is cased 'with 10" tube 7 through gravel into rock. An 8" casing 8 cemented into lower part of shale roof and upper part of salt bed. 'A 6" casing 9 to the top of the undercutand a 3' tube 10 to bottom of' the salt,
  • the water at pressure of about 200 pounds tothe square inch, is pumped into the 3" tube or casing 10, passing into the cavity where it circulates and dissolves salt off of the circumference of the cavity and flows upwards through the annular space between the tubes 9 and 10, as partially saturated brine.
  • red, blue, green and yellow in accordance with the oflicial chart.
  • the color red indicates air or other fluid medium for separating the solvent from the soluble; blue indicates water or other solvent; green represents sulphur water, and yellow indicates brine or solution.
  • the well is piped with a 3" tube 11 to bottom of the salt and a 6" tube 12 is packed off in the 8" tube 13 which is cemented in the rock.
  • the 6" tube 12 may be stopped at the top of the salt or extended down intoit to top of the undercut.
  • the well is operated by forcing water down annular space between tubes 11 and 12 and brine out of tube 11. Air is forced in with the water-and entrained in the form of bubbles which reduce in size by ab- 1 sorption and increase of pressure. The air is therefore compressed to the pressure of the water at the bottom of the well and holds back the liquid to required level.
  • the 3" tube 14 reaching to the bottom of the salt is provided with a bell 15 which is either part of the 6" tube 16 or will slide down through it. This bell receives the surplus air at the level of the top of the undercut and transfers it through small holes or passages 17 to the inside of the 3" tube 14.
  • the water is forced down through the annular space between the tubes 14 and 16 and out through holes or space 18 above the bell 15.
  • Air is forced through the crown of small tube 19 into the water and is carried down entrained as small bubbles increasing in pressure.
  • the 8" casing 20 is cemented into the rock and the top of the rock salt bed.
  • a 6 casing 21 is extended down nearly to the level of the undercut.
  • a 3" tube 22 extends to the bottom of the salt.
  • the connections of water and brine and air pipe are arranged so that the well can be operated either way, with brine or water in the 3" tube 22.
  • a 1" pipe 23 is suspended inside the 3" tube 22, with its bottom end at the top of desired undercut.
  • This 1" tube 23 may be very readily moved up or down or changed in position, to
  • a reducing valve 28 shown in the air pipe is set to obstruct the air, the level of the air cushion will be lowered the amount of the differential pressure measured in feet of water.
  • Fig. 4 In Fig. 4 are shown air gages 25 and 26, the mercury gage 27 and a reducingvalve 28, the hand pump 29 and also a number of valves in the air line, the water line and the brine line, whereby the several flows and the direction of flow may be controlled. Also the center air pipe may be arranged for change of vertical position.
  • the level of the solvent may be regulated during the several stages as required.
  • This arrangement of well eliminates all packers, uses simple tubing without any connection between them at the bottom, and the regulation is all accomplished at the top of the well.
  • the level can be varied at will.
  • the air indicator 30, is suspended in the space betwe n pipes 20 and 21. .
  • the bottom end being below the top of the undercut.
  • the hand air pump 29 is operated to force air into the tube 30 until it bubbles under the bottom end.
  • the difference in pressure indicated between gage 25 and gage 26, shows the distance between the water level and the bottom of the air indicator-pipe 30.
  • soluble salt or other mineral capable of being dissolved.
  • solvent any fluid medium capable of dissolving the soluble.
  • non-solvent any fluid medium which will not dissolve the soluble.
  • the method of mining a soluble which consists in introducing into the mine cavity a supply of, solvent, and a supply of gaseous medium in excess'of the amount that wouldbe taken up by the solvent so that the surplus gaseous medium will be discharged from the cavity, discharging the solution from the cavity together with the surplus gaseous medium, and controlling as required the level of the solvent in the cavity by controlling the point of discharge of the surplus gaseous medium.

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Drilling And Exploitation, And Mining Machines And Methods (AREA)

Description

Aug. 22, 1933. TRUMP I 1,923,896
MINING SOLUBLE SALT I I Filed Nov. 1051951 2 Sheets-Sheet 1 Inderzlor: Zdzdardik'fiump, g7 M flfibrng.
Aug. 22, 1933. TRUMP 1,923,896-
MINING SOLUBLE SALT Filed Nov. 10, 1931 2 Sheets-Sheet 2 P 1P W I WE g a I" .3 11' .4.
y j Indemnmardmflm Patented Aug. 22, 1933 IVHNING SOLUBLE SALT Edward N. Trump, Syracuse, N. 'Y.
Application November 10, 1931 Serial No. 574,149
6 Claims. (Cl. 262-3) The invention relates to improvements in' method and means for mining soluble salts or similar materials.
The object is to provide a new and useful 5 method of operation and arrangement of well casings which will control the level of water or other liquid, while it is dissolving salts or other soluble minerals to produce brine or other solutions.
By means of the control of level, I am enabled to dissolve out a section of the bottom layers of the bed of minerals such asrock salt, sulphur or potash salts and am thus able to afterwards attack succeeding upper layers of the salts from below.
While the following description is .given by way of example as applied to operation upon salt beds, it will be understood that it will equally apply to other soluble materials.
2 The method now in use for dissolving -these salts by means of wells drilled through the bed requires the circulation of liquid through casings either to the top or bottom of the bed by superior pressure. If the liquid is introduced at the top of the bed it creeps out under the insoluble roof until it comes in contact with the salt and, becoming heavy with the salt dissolved, falls and is forced back to the center circulating tube and up to the top of the well. v
Because the fresliliquid dissolves faster than more saturated brine, the shape of the cavity becomes an inverted cone.
.As the top increases in diameter the support of the shale or rock roof is removed and caving takes place which cuts off the tubes and covers the surface of the salt below hindering further dissolving and requiring expensive cleaning and drilling to put back the tubing at the full depth.
With a very thick bed of .salt, 200 ft., it is possible to introduce the liquid at the bottom forcing it out the annular space around the center tube, making a ball shaped cavity-which will support the roof a longer time.
With a thin bed of salt the liquid rises to the top before it is saturated andthe first method must be followed. If there is considerable insoluble material in the bed, the sides of the cone or ball are covered and protected from the liquid and the well gradually loses capacity and is finally abandoned. I
Even if the salt is pure, the saturated brine protects the salt below and it is dissolved Very slowly if attacked from above.
'to undercut a rock salt bed as an example in a If the salt is attacked from below, the saturated brine falls away and fresh liquid reaches the salt so that solution takes place much more rapidly. The object of my invention is to provide a method of dissolving a section of the lower part of the bed by attacking it radially from the well for a very limited height.
.crease about .5 ft. per day, or in one year it will have a diameter of nearly 360 ft. This is about the limit of rock salt roof without caving.
My invention consists of the maintenance of a layer of air, gas or other fluid medium which will float on the liquid protecting the roof of the cavity and preventing the liquid from coming in contact with it. This layer is formed by introducing the medium so as to force the liquid down to the desired level and to'provide a surplus over the volume of medium so required which will be absorbed by the liquid so that the escape of the surplus will automatically control the level. The level'can also be controlled by the pressure of medium in the cavity.
Referring to the drawings, which illustrate merely by way of example preferred means for efiecting the invention:--
Fig. 1 .is a diagrammatic vertical section showing one form of embodiment.
Fig. 2 is a similar view of another form.
Fig. 3 is a similar view of another form.
Fig. 4 is a similar. view of another form.
Similar numerals) refer to similar parts throughout the several views. Fig. 1. The well is cased 'with 10" tube 7 through gravel into rock. An 8" casing 8 cemented into lower part of shale roof and upper part of salt bed. 'A 6" casing 9 to the top of the undercutand a 3' tube 10 to bottom of' the salt,
1500 ft. well with ft. of salt.
With the arrangement shown in Fig. 1, the water, at pressure of about 200 pounds tothe square inch, is pumped into the 3" tube or casing 10, passing into the cavity where it circulates and dissolves salt off of the circumference of the cavity and flows upwards through the annular space between the tubes 9 and 10, as partially saturated brine.
To prevent attack of thesalt above the end of the tube 9, air, of about 700 pounds per square inch pressure, is pumped into the annular space between tubes 8 and 9, forcing the water down until the air bubbles under the end of tube 9. This will maintain the water level at this level and an air cushion will fill the space between the ripples on top of the brine as long as there is a.
surplus of air kept moving into the tube 9.
I have indicated in the drawings the colors red, blue, green and yellow, in accordance with the oflicial chart. The color red indicates air or other fluid medium for separating the solvent from the soluble; blue indicates water or other solvent; green represents sulphur water, and yellow indicates brine or solution.
In the modification shown in Fig. 2, the well is piped with a 3" tube 11 to bottom of the salt and a 6" tube 12 is packed off in the 8" tube 13 which is cemented in the rock. The 6" tube 12 may be stopped at the top of the salt or extended down intoit to top of the undercut. The well is operated by forcing water down annular space between tubes 11 and 12 and brine out of tube 11. Air is forced in with the water-and entrained in the form of bubbles which reduce in size by ab- 1 sorption and increase of pressure. The air is therefore compressed to the pressure of the water at the bottom of the well and holds back the liquid to required level.
Small holes 13 in tube 11 at level of top of undercut allow surplus air to escape into the brine regulating the level of air which fills space around tubes to underside of packer. This arrangement reduces the pressure of air needed to the pressure of the water at top of well instead of the bottom as in Fig. 1.
In accordance with the modification shown in Fig. 3, the 3" tube 14, reaching to the bottom of the salt, is provided with a bell 15 which is either part of the 6" tube 16 or will slide down through it. This bell receives the surplus air at the level of the top of the undercut and transfers it through small holes or passages 17 to the inside of the 3" tube 14.
The water is forced down through the annular space between the tubes 14 and 16 and out through holes or space 18 above the bell 15.
Air is forced through the crown of small tube 19 into the water and is carried down entrained as small bubbles increasing in pressure.
The amout of air absorbed increases with the depth and pressure of the water. As the salt dissolves it drives out a portion of the air which has been dissolved. If a surplus of air over the amount absorbed, any leakage and the volume required to fill the space around the tube up to the packer is forced in, the surplus escapes under the bell and entering the tube 14, helps elevate the brine passing up this tube.
, In accordance with the modification shown in Fig. 4, the 8" casing 20 is cemented into the rock and the top of the rock salt bed.
A 6 casing 21 is extended down nearly to the level of the undercut.
A 3" tube 22 extends to the bottom of the salt. The connections of water and brine and air pipe are arranged so that the well can be operated either way, with brine or water in the 3" tube 22.
A 1" pipe 23 is suspended inside the 3" tube 22, with its bottom end at the top of desired undercut. This 1" tube 23 may be very readily moved up or down or changed in position, to
regulate the level of the air cushion and consequently the top level of the solvent outside of the 3" tube 22.
If this pipe 23 is wide open, the level of thetop of the water outside the 3" tube 22 will be enough below the end of the 1" pipe 23 to overcome the friction of the air passing up the annular space, through the piping and valve and down the 1" center pipe 23.
If a reducing valve 28 shown in the air pipe is set to obstruct the air, the level of the air cushion will be lowered the amount of the differential pressure measured in feet of water.
With a 1500 it. well with weak brine, 18 cu. ft. of air per minute will maintain the level with very little surplus. When the brine is saturated only 6 cu. ft. are required.
With this amount of air the friction in the tubing will be negligible and the level will be very little below the end of the 1" pipe 23 when the reducing valve is wide open.
The above amounts are when using 20 cu. ft. of water=200 gal. per min.
In Fig. 4 are shown air gages 25 and 26, the mercury gage 27 and a reducingvalve 28, the hand pump 29 and also a number of valves in the air line, the water line and the brine line, whereby the several flows and the direction of flow may be controlled. Also the center air pipe may be arranged for change of vertical position.
By the proper manipulation of these several instrumentalities, the level of the solvent may be regulated during the several stages as required.
This arrangement of well eliminates all packers, uses simple tubing without any connection between them at the bottom, and the regulation is all accomplished at the top of the well. The level can be varied at will.
The air indicator 30, is suspended in the space betwe n pipes 20 and 21. .The bottom end being below the top of the undercut. The hand air pump 29 is operated to force air into the tube 30 until it bubbles under the bottom end. The difference in pressure indicated between gage 25 and gage 26, shows the distance between the water level and the bottom of the air indicator-pipe 30.
By soluble is meant salt or other mineral capable of being dissolved. I
By solvent is meant any fluid medium capable of dissolving the soluble.
By non-solvent is meant any fluid medium which will not dissolve the soluble.
What I claim is:
1. In the operation of mining a soluble, wherein a solvent is introduced into the mine, and a non-solvent is introduced into the mine to form a separating layer between the solvent and the soluble above it, and wherein the solution is discharged from the mine, the method which consists in introducingthe solvent admixed with the non-solvent and utilizing the said separating layer of non-solvent for controlling the level of the solvent in the mine cavity.
2. In the operation of mining a soluble, wherein a solvent is introduced into the mine, and a non-solvent is introduced into the mine to form a separating layerbetwcen the solvent and the soluble above it, and wherein the solution is discharged from the mine, the method which consists in introducing the solvent and non-solvent continuously and in utilizing the said separating layer of non-solvent for controlling and changing as required the level of the solvent in the mine cavity.
3. In the operation of mining a soluble, wherein a continuous supply of a solvent is introduced into the mine and also a continuous supply of non-solvent which will form a protecting layer between the-solvent and the soluble above it, and which will also provide a continuously discharging surplus, and wherein the solution isdischarged from the mine, the method which consists in utilizing the discharging surplus of nonsolvent to cooperate in the discharge of solution, whereby the required pressures of the introto lighten the ascending column of solution, so that the energy derived from the upward movement of said ascending column may be utilized in connection with the introduction of the solvent.
5. In the operation of mining a'soluble, wherein an admixture of a solvent and a non-solvent is introduced into the mine, the non-solvent separating from the solvent to form a protecting layer between the soluble and the solvent, the method which consists in controlling the level of the solvent by the difierence in pressure of the non-solvent at a point approximate the level of the solvent and at the point of discharge of a surplus of the non-solvent which escapes into the discharging solution.
6. The method of mining a soluble, which consists in introducing into the mine cavity a supply of, solvent, and a supply of gaseous medium in excess'of the amount that wouldbe taken up by the solvent so that the surplus gaseous medium will be discharged from the cavity, discharging the solution from the cavity together with the surplus gaseous medium, and controlling as required the level of the solvent in the cavity by controlling the point of discharge of the surplus gaseous medium.
EDWARD N. TRUMP
US574149A 1931-11-10 1931-11-10 Mining soluble salt Expired - Lifetime US1923896A (en)

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2732334A (en) * 1956-01-24 pollock
US2772868A (en) * 1954-01-18 1956-12-04 Phillips Petroleum Co Apparatus for control of roof location in the formation of underground caverns by solution mining
US2901403A (en) * 1954-02-15 1959-08-25 Phillips Petroleum Co Underground storage of ammonia and its recovery
US2943026A (en) * 1953-12-14 1960-06-28 Phillips Petroleum Co Removal of salt from solutions
US2986007A (en) * 1952-08-29 1961-05-30 Texaco Inc Underground storage
US2994200A (en) * 1957-01-28 1961-08-01 Phillips Petroleum Co Making underground storage caverns
US3632171A (en) * 1970-02-04 1972-01-04 Allied Chem Method of controlling growth of brine wells
DE2642296A1 (en) * 1975-09-23 1977-03-24 Ppg Ind Canada Ltd SOLUTION DEGRADATION PROCEDURE
US5669734A (en) * 1995-11-29 1997-09-23 Texas Brine Corporation Process for making underground storage caverns
US9365349B1 (en) 2015-11-17 2016-06-14 Air Liquide Large Industries U.S. Lp Use of multiple storage caverns for product impurity control
US9399810B2 (en) 2014-11-18 2016-07-26 Air Liquide Large Industries U.S. Lp Materials of construction for use in high pressure hydrogen storage in a salt cavern
US9482654B1 (en) 2015-11-17 2016-11-01 Air Liquide Large Industries U.S. Lp Use of multiple storage caverns for product impurity control
US9573762B2 (en) 2015-06-05 2017-02-21 Air Liquide Large Industries U.S. Lp Cavern pressure management
US9656807B2 (en) 2014-05-08 2017-05-23 Air Liquide Large Industries U.S. Lp Hydrogen cavern pad gas management

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2732334A (en) * 1956-01-24 pollock
US2986007A (en) * 1952-08-29 1961-05-30 Texaco Inc Underground storage
US2943026A (en) * 1953-12-14 1960-06-28 Phillips Petroleum Co Removal of salt from solutions
US2772868A (en) * 1954-01-18 1956-12-04 Phillips Petroleum Co Apparatus for control of roof location in the formation of underground caverns by solution mining
US2901403A (en) * 1954-02-15 1959-08-25 Phillips Petroleum Co Underground storage of ammonia and its recovery
US2994200A (en) * 1957-01-28 1961-08-01 Phillips Petroleum Co Making underground storage caverns
US3632171A (en) * 1970-02-04 1972-01-04 Allied Chem Method of controlling growth of brine wells
DE2642296A1 (en) * 1975-09-23 1977-03-24 Ppg Ind Canada Ltd SOLUTION DEGRADATION PROCEDURE
US5669734A (en) * 1995-11-29 1997-09-23 Texas Brine Corporation Process for making underground storage caverns
US9656807B2 (en) 2014-05-08 2017-05-23 Air Liquide Large Industries U.S. Lp Hydrogen cavern pad gas management
US9399810B2 (en) 2014-11-18 2016-07-26 Air Liquide Large Industries U.S. Lp Materials of construction for use in high pressure hydrogen storage in a salt cavern
US9573762B2 (en) 2015-06-05 2017-02-21 Air Liquide Large Industries U.S. Lp Cavern pressure management
US9365349B1 (en) 2015-11-17 2016-06-14 Air Liquide Large Industries U.S. Lp Use of multiple storage caverns for product impurity control
US9482654B1 (en) 2015-11-17 2016-11-01 Air Liquide Large Industries U.S. Lp Use of multiple storage caverns for product impurity control

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