US189504A - Improvement in processes for clarifying sugar - Google Patents

Improvement in processes for clarifying sugar Download PDF

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US189504A
US189504A US189504DA US189504A US 189504 A US189504 A US 189504A US 189504D A US189504D A US 189504DA US 189504 A US189504 A US 189504A
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sugar
water
improvement
processes
liquor
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    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/04Separating crystals from mother liquor
    • C13B30/08Washing residual mother liquor from crystals

Definitions

  • My invention is based on the fact that in proportion as the temperature of the water or sugar-liquor used in the centrifugal machine for liquoring the sugar is reduced, so will the tendency of the crystals to dissolve during the clarifying process be diminished.
  • raw sugars contain acertain proportion of coloring matter, salts, and uncrystallizable sugar
  • the machine when charged with the raw sugar, is to be set rotating, and when the necessary speed is attained for insuring the adherence of the sugar to the perforated copper drum, I remove the inner circular drum, and liquor the dry sugar with a spray of water, or of refined sugarliquor, reduced to a temperature of 32 Fahrenheit, or as near the freezing-point as possible, by the means described under the second head of the invention.- This liquoring operation I continue (keeping the machine in action) until the coloring matters are washed out of the sugar.
  • the sugar when sufficiently boiled,is discharged into a suitable vessel, and from thence into centrifugal machines, in the ordi nary manner.
  • a spray of water or liquor at a temperature as near freezing-point as possible, taking care that the water he brought into close contact with the sugar, so as not to be heated by coming in contact with the surrounding atmosphere.
  • the duration of the process will vary according to the material under operation, and the Water being in either case perfectly under the control of the attendant, he will only have to turn a tap on and off. I find a ton of ice daily yields sufficient iced water to liquor a daily out-turn of one hundred tons of sugar even in the summer-time.
  • sugar-liquor be used in preference to water, it will be most conveniently cooled down to the required temperature of 32 Fahrenheit, or thereabout, by being passed through copper coils embedded in ice or surrounded by iced water.
  • I connect the nozzles of the molds with a vacuum-pump, and thereby facilitate the passage of the cold sugar-liquor through the sugar in the molds.
  • the fine liquor may easily be re dueed to 32 Fahrenheit, 0r thereabout, by passing it through a series of copper pipes embedded in ice immediately before being used for the liquoring process.

Description

UNITED STATES PATENT JOHN SCHWARTZ, OF PELHAM STREET, MILE END, NEW TOWN, ENGLAND.
IMPROVEMENT IN PROCESSES FOR CLARIFVING SUGAR.
Specification forming part of Letters Patent No. 189,504, dated April 10, 1877 application filed December 12, 1876.
monly experienced.
My invention is based on the fact that in proportion as the temperature of the water or sugar-liquor used in the centrifugal machine for liquoring the sugar is reduced, so will the tendency of the crystals to dissolve during the clarifying process be diminished.
As raw sugars contain acertain proportion of coloring matter, salts, and uncrystallizable sugar, I propose to subject raw sugar to the following treatment, in order to remove all such matters therefrom prior to the sugar being melted in the refinery.
Thus I use an ordinary centrifugal machine, with the simple addition of a movable inner drum or cylinder, which will form, with the perforated copper drum of the machine, an annular chamber for the reception of the sugar to be clarified, which sugar is to be placed in the annular chamber in a powdered or crushed condition. The machine, when charged with the raw sugar, is to be set rotating, and when the necessary speed is attained for insuring the adherence of the sugar to the perforated copper drum, I remove the inner circular drum, and liquor the dry sugar with a spray of water, or of refined sugarliquor, reduced to a temperature of 32 Fahrenheit, or as near the freezing-point as possible, by the means described under the second head of the invention.- This liquoring operation I continue (keeping the machine in action) until the coloring matters are washed out of the sugar.
Having described my mode of dealing with raw sugars so as to cleanse them from their impurities prior to melting them in the refinery, or to fit them for use for domestic or household purposes, without subjecting them to any other process of refining, I now proceed to describe my plan of dealing with sugar as it leaves the vacuum-pan or other evaporating-panin a concrete state, before undergo ing the process of drying in the centrifugal machine.
The sugar, when sufficiently boiled,is discharged into a suitable vessel, and from thence into centrifugal machines, in the ordi nary manner. When the sirup has been partially or wholly driven out by the centrifugal action, I apply to the face of the sugar, while in motion, a spray of water or liquor at a temperature as near freezing-point as possible, taking care that the water he brought into close contact with the sugar, so as not to be heated by coming in contact with the surrounding atmosphere. 0f various modes of proceeding I prefer the following plan I place a ton of block-ice in a tank carefully felted, and about ten feet above the machinefloor, and add from time to time as much water through a perforated pipe (to spread it over the surface of the ice) as will be found requisite to supplement the water due to the melting of the ice. The iced water I convey, through pipes carefully felted, to the machine, wherein is fixed a vertical pipe finely perforated on the side facing the sugar that is revolving in the centrifugal machine or Iuse a finely-perforated rose at the end of an indiarubber pipe, to be held by the attendant close to the sugar while in motion.
The duration of the process will vary according to the material under operation, and the Water being in either case perfectly under the control of the attendant, he will only have to turn a tap on and off. I find a ton of ice daily yields sufficient iced water to liquor a daily out-turn of one hundred tons of sugar even in the summer-time.
If sugar-liquor be used in preference to water, it will be most conveniently cooled down to the required temperature of 32 Fahrenheit, or thereabout, by being passed through copper coils embedded in ice or surrounded by iced water.
Hitherto it has been found that however carefully the sugar, after leaving the centrifugal machine, was spread out in the coolingfloors or sugar-bins, it was impossible to sufficiently cool it to prevent its loss of bloom, and its becoming darker in color, which result from the packing of the sugar while hot in casks or bags. I claim for my invention the advantage of reducing the temperature of the sugar, while in the centrifugal machine, to that of the atmosphere, and even below it, during the summer months, thus insuring its retaining its bloom and not deteriorating in value.
In the manufacture of loaf-sugar, instead of liquoring the loaves of sugar, in the usual way, with fine liquor of suitable density, I find that by first reducing the temperature of the fine liquor to as nearly 32 Fahrenheit as possible, a very much less percentage of sugar is dissolved out of the sugar molds, and hence results in a greater weight of loaf-sugar than that usually obtained, the crystals being as efi'ectually cleansed, but not melted by this new liquoring process.
With the view of expediting the process, I connect the nozzles of the molds with a vacuum-pump, and thereby facilitate the passage of the cold sugar-liquor through the sugar in the molds. The fine liquor may easily be re dueed to 32 Fahrenheit, 0r thereabout, by passing it through a series of copper pipes embedded in ice immediately before being used for the liquoring process.
Having now set forth the nature of my invention, and the manner of carrying it into effect, I wish it to be understood that I claim- The process of clarifying raw and refined sugar, which consistsin submitting it to the action of a spray of water or sugar-liquor reduced to a temperature of 32 Fahrenheit, or thereabout, the same being evenly diffused through the sugar mass by centrifugal force, substantially as and for the purpose specified.
Dated this 23d day of November, 1876.
JOHN SCHWARTZ.
Witnesses:
WILMER M. HARRIS, Jno. DEAN, Both of No. 17 Graceahwch Street, London.
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