US1850181A - Magnet core - Google Patents

Magnet core Download PDF

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Publication number
US1850181A
US1850181A US424738A US42473830A US1850181A US 1850181 A US1850181 A US 1850181A US 424738 A US424738 A US 424738A US 42473830 A US42473830 A US 42473830A US 1850181 A US1850181 A US 1850181A
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US
United States
Prior art keywords
iron
nickel
phosphoric acid
treated
magnet core
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US424738A
Inventor
Roseby Philip Norton
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Automatic Telephone Manufacturing Co Ltd
Original Assignee
Automatic Telephone Manufacturing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Automatic Telephone Manufacturing Co Ltd filed Critical Automatic Telephone Manufacturing Co Ltd
Application granted granted Critical
Publication of US1850181A publication Critical patent/US1850181A/en
Anticipated expiration legal-status Critical
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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/12Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
    • H01F1/14Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
    • H01F1/16Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of sheets
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49002Electrical device making
    • Y10T29/4902Electromagnet, transformer or inductor
    • Y10T29/49075Electromagnet, transformer or inductor including permanent magnet or core
    • Y10T29/49076From comminuted material

Description

pressure.
Patented Mar. 22,1932v UNIT D} STATES "1 'r |m'1' orrlcs PHILIP NOBTON ROSEBY, OI LIVEBQOOL, -E NGLA.ND, ASSIQNOR 'I'O AUTOMATIC TELE- PHONE- MANUFACTURING COMPANY LIKI'IED, OI LIVERPOOL, ENGLAND, A. BRITISH comm IAGNE'I COBB No Drawing: Application and January so, mo, Serial No. mass, and in Grumman mm... a, 1929.
The present invention relates-to the con; struction of magnet cores and is particularly concerned with cores which are made from powdered material by the application of high Such cores find considerable application for loading coils of the type used on telephone lines where their special magnetic properties are 'particularly advantageous.
= t has generally been considered necessary in the manufacture of loading coils of this nature to employ magnetic material in as finely divided a state as; possible in order that the particles may form a compact and substantially homogeneous mass and also so that with the'insulation of individual particles there a may not be 'a conducting path of ap reciable other m aterial,
advantage however, t at after the loading 39 coils have em pressed it is necessary to sub-i ject them to further heat treatment to restore their. magnetic pro rties to the maximum value, or alternative y if such heat treatment is not undertaken loss of magnetic properties of thecoil will necessitate the use of a v coil larger than would otherwise be necessary.
Moreover the heat treatment is liable to afiect adversely the mechanical properties of the pressed core.
, The. hief object of the present invention is the provision of .a method for reducing the magnetic material-to a'suflici'entl fine state without the necessity for first ren ering it brittle. According tothe invention this is'accomplished in that the material is drawn out into wire o f'very small diameter, for in-' stance as small as 4 mils, and is then fed throu h a small hole inja steel plate to a cutter w ich will preferably be of a'rotarly 1 type by which it is cut up}v into very sma lengths. The pieces so produced may then be annealed, coslettised, coated with insulatproportion, say up to 20%, of powdered iron which tends to fill up the interstices and thus produce a more compact core. As an alternative to the use of the coslettising process, a somewhat similar result may be-obtained by treating the chopped up parti cles with phosphorimacid. If hard drawn nickel-iron wire is used the'acid treatment is preferably effected at about 300 F. and results in the production of a deposit of nickel and iron phosphates on each article. The powdered iron for mixing wlth the nickel 11'011 particles is also treated with phosphoric acid ut without heat. The insulating varnish used as a binder preferably comprises a suitable solution of the synthetic resin known under the trade name bakelite. Where the alternative rocess described above is employed it is esirable to use somewhat higher magnetic material prepared as above described are more satisfactory as regards their magnetic properties and after the core has been pressed to the required shape do not need any further treatment to bring these properties back to their original value.
I claim:
1. A magnet core forloadingcoils and the nickel-iron wires treated with phosphoric acid at approximately 300" F. and subset quently sub1ected to high pressure.
3. A process for making magnet cores for use in loading coils and the like in which finely-drawn nickel-iron wire is cut into small lengths, annealed, treated with phosphoric acid and mixed with powdered iron which has been similarly treated with ph'osphoric acid after which the mixture is coated with synthetic resin varnish and then subjected to pressure in a heated mould to cause the particles to agglome'rate.
4. A process as claimed in claim 3 in which the nickel-iron particles are treated with phosphoric acid at approximately 300 F.
while the iron powder is treated with phosphoric acid at ordinary temperatures.
5. A magnet core comprising fourparts of short lengths of nickel-iron wire mixed with one part of powdered iron, a coating of nickel-iron phosphates on said powdered iron and wiresto insulate the same, and insulating material separating said phosphate coated particles and binding the same into a solid mass.
6. A process for making magnet cores which consists in annealing short lengths of nickel-iron wire, treating the same with phos phoric acid and mixing it with powdered iron, then coating the mixture with an insulating compound after which it is subjected late the same and insulating material separating the phosphoric coated powder and wires. I
,In testimony whereof I afiixrmy si ature.
PHILIP NORTON ROS BY.
to heat and pressure to. bind the whole into ,iron wire into small lengths, annealing the Wires, treating them with phosphoric acid at a temperature of 300 F., mixing the treated wires. with powdered iron which has been A l which consists in treating a mixture of powderediron' and short lengths of annealed treated with phosphoric acid, coating the mixture with a binder of insulating material, and then binding the same into a homogene-- ous mass under heatiand pressure.
9. The method of making magnet cores nickel-ironwire with phosphoric acid to insnlate the particles from each other, then coating theparticles with an insulating 'material, and then subjecting the mass to heat and pressure to bind the same into a solid mass. 7
t 10. .A ,inagiiet, core composed of short lengths of nickel-iron wire mixed with pow dered iron, a coating of phosphoric acid on said wires and'said powdered iron to insuiao
US424738A 1929-02-08 1930-01-30 Magnet core Expired - Lifetime US1850181A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1850181X 1929-02-08

Publications (1)

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US1850181A true US1850181A (en) 1932-03-22

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2601212A (en) * 1948-11-09 1952-06-17 Gen Aniline & Film Corp Heat resistant magnetic cores and method of making
US2689398A (en) * 1948-03-24 1954-09-21 Plessey Co Ltd Method of making magnetizable compacts
US2718049A (en) * 1948-01-16 1955-09-20 Lignes Telegraph Telephon Method of manufacturing bundles of very thin magnetic wires
US3245841A (en) * 1961-08-31 1966-04-12 Clarke Sydney George Production of iron powder having high electrical resistivity
DE2443192A1 (en) * 1973-09-11 1975-07-24 Westinghouse Electric Corp METHOD FOR MANUFACTURING MAGNETIC CORE BODIES
US5063011A (en) * 1989-06-12 1991-11-05 Hoeganaes Corporation Doubly-coated iron particles
US5198137A (en) * 1989-06-12 1993-03-30 Hoeganaes Corporation Thermoplastic coated magnetic powder compositions and methods of making same
US5306524A (en) * 1989-06-12 1994-04-26 Hoeganaes Corporation Thermoplastic coated magnetic powder compositions and methods of making same
US5536985A (en) * 1994-05-09 1996-07-16 General Motors Corporation Composite armature assembly
US5982073A (en) * 1997-12-16 1999-11-09 Materials Innovation, Inc. Low core loss, well-bonded soft magnetic parts
US6372348B1 (en) 1998-11-23 2002-04-16 Hoeganaes Corporation Annealable insulated metal-based powder particles
US7510766B2 (en) 2003-02-05 2009-03-31 Corporation Imfine Inc. High performance magnetic composite for AC applications and a process for manufacturing the same
EP2722118A1 (en) * 2011-06-17 2014-04-23 Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.) Iron-base soft magnetic powder for dust cores, manufacturing method thereof, and dust core
EP4075461A1 (en) * 2021-03-31 2022-10-19 Universität Stuttgart Method of manufacturing an electric component

Cited By (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2718049A (en) * 1948-01-16 1955-09-20 Lignes Telegraph Telephon Method of manufacturing bundles of very thin magnetic wires
US2689398A (en) * 1948-03-24 1954-09-21 Plessey Co Ltd Method of making magnetizable compacts
US2601212A (en) * 1948-11-09 1952-06-17 Gen Aniline & Film Corp Heat resistant magnetic cores and method of making
US3245841A (en) * 1961-08-31 1966-04-12 Clarke Sydney George Production of iron powder having high electrical resistivity
DE2443192A1 (en) * 1973-09-11 1975-07-24 Westinghouse Electric Corp METHOD FOR MANUFACTURING MAGNETIC CORE BODIES
US5063011A (en) * 1989-06-12 1991-11-05 Hoeganaes Corporation Doubly-coated iron particles
US5198137A (en) * 1989-06-12 1993-03-30 Hoeganaes Corporation Thermoplastic coated magnetic powder compositions and methods of making same
US5306524A (en) * 1989-06-12 1994-04-26 Hoeganaes Corporation Thermoplastic coated magnetic powder compositions and methods of making same
US5543174A (en) * 1989-06-12 1996-08-06 Hoeganaes Corporation Thermoplastic coated magnetic powder compositions and methods of making same
US5536985A (en) * 1994-05-09 1996-07-16 General Motors Corporation Composite armature assembly
US5982073A (en) * 1997-12-16 1999-11-09 Materials Innovation, Inc. Low core loss, well-bonded soft magnetic parts
US6129790A (en) * 1997-12-16 2000-10-10 Materials Innovation, Inc. Low core loss, well-bonded soft magnetic
US6251514B1 (en) 1997-12-16 2001-06-26 Materials Innovation, Inc. Ferromagnetic powder for low core loss, well-bonded parts, parts made therefrom and methods for producing same
US6309748B1 (en) 1997-12-16 2001-10-30 David S. Lashmore Ferromagnetic powder for low core loss parts
US6340397B1 (en) 1997-12-16 2002-01-22 Materials Innovation, Inc. Method for making low core loss, well-bonded, soft magnetic parts
US6342108B1 (en) 1997-12-16 2002-01-29 Materials Innovation, Inc. Low core loss, well-bonded soft magnetic stator, rotor, and armature
US6372348B1 (en) 1998-11-23 2002-04-16 Hoeganaes Corporation Annealable insulated metal-based powder particles
US6635122B2 (en) 1998-11-23 2003-10-21 Hoeganaes Corporation Methods of making and using annealable insulated metal-based powder particles
US7510766B2 (en) 2003-02-05 2009-03-31 Corporation Imfine Inc. High performance magnetic composite for AC applications and a process for manufacturing the same
EP2722118A1 (en) * 2011-06-17 2014-04-23 Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.) Iron-base soft magnetic powder for dust cores, manufacturing method thereof, and dust core
EP2722118A4 (en) * 2011-06-17 2015-03-11 Kobe Steel Ltd Iron-base soft magnetic powder for dust cores, manufacturing method thereof, and dust core
US9472328B2 (en) 2011-06-17 2016-10-18 Kobe Steel, Ltd. Iron-based soft magnetic powder for dust core use, manufacturing method thereof, and dust core
EP4075461A1 (en) * 2021-03-31 2022-10-19 Universität Stuttgart Method of manufacturing an electric component

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