US174691A - Improvement in nickel-plating - Google Patents

Improvement in nickel-plating Download PDF

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Publication number
US174691A
US174691A US174691DA US174691A US 174691 A US174691 A US 174691A US 174691D A US174691D A US 174691DA US 174691 A US174691 A US 174691A
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Prior art keywords
nickel
plating
improvement
zinc
metals
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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00Electroplating: Baths therefor
    • C25D3/02Electroplating: Baths therefor from solutions
    • C25D3/56Electroplating: Baths therefor from solutions of alloys
    • C25D3/565Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of zinc
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/922Static electricity metal bleed-off metallic stock
    • Y10S428/9335Product by special process
    • Y10S428/934Electrical process
    • Y10S428/935Electroplating
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771Transition metal-base component
    • Y10T428/12785Group IIB metal-base component
    • Y10T428/12792Zn-base component
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771Transition metal-base component
    • Y10T428/12861Group VIII or IB metal-base component
    • Y10T428/12937Co- or Ni-base component next to Fe-base component

Definitions

  • OAMILLO MAGGIO AND GIUSEPPE MAFFIOLA, OF SAhl FRANCISCO, CAL.
  • Our invention relates to certain improvements in the art of plating with nickel upon other metals; and it consists, first, in a novel preparation of the base metals to be plated, so as to prevent rust or oxidation beneath the nickel-plating; and in a new solutionby which we are enabled to deposit the metal' more perfectly, and upon metals which it has hitherto been impossible to protect with nickel.
  • Zinc in its pure state, is very little liable to become corroded or tarnished, and from its malleability will form a complete protecting coat.
  • This coat may be put upon the article to be plated in the same manner that is employed for tinning iron sheets for the purpose of making commercial sheet tin, and the article (is then ready for the nickel solution.
  • The, other non-oxidizable metals might be employed but they are too expensive to be available.
  • OAMILLO MAGGIO OAMILLO MAGGIO.
  • GIUSEPPE MAFFIOLA.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Electroplating And Plating Baths Therefor (AREA)

Description

UMTED STATES PATENT OFFIGE.
OAMILLO MAGGIO AND GIUSEPPE MAFFIOLA, OF SAhl FRANCISCO, CAL.
IMPROVEMENT IN NICKEL-PLATING.
Specification forming part of Letters Patent No. 174,691, dated March 14, 1876; application filed December 2, 1875.
To all whom it may concern Be it known that we, GAMILLO MAGGIO and GIUsEPPE MAFFIOLA, of San Francisco city and county, State of California, have invented Improvements in N ickel-Plating and we do hereby declare the following description and accompanying drawings are sufficient to enable any person skilled in the art or science to which itmost nearly appertains to make and 'use our said invention or improvement without further invention or experiment.
Our invention relates to certain improvements in the art of plating with nickel upon other metals; and it consists, first, in a novel preparation of the base metals to be plated, so as to prevent rust or oxidation beneath the nickel-plating; and in a new solutionby which we are enabled to deposit the metal' more perfectly, and upon metals which it has hitherto been impossible to protect with nickel.
It is well known that in the process of' electroplating the metal is deposited in the form of minute grains, and when the metal is malleable, as in the case of gold and silver, these grains are welded or united in the process of burnishing, so as to completely cover and protect the whole surface, but when nickel is deposited in this manner it cannot be made to protect the surface any more completely than is done bya simple deposition of the particles on account of its brittleness, which does not allow of burnishiug and proper protection successfully. .The surface beneath is therefore more or less exposed to the action of air, acids, or other substances, and will in time become oxidized or corroded in spots, especially in the ease 'of iron, steel, lead, copper, and other base pose. Zinc, in its pure state, is very little liable to become corroded or tarnished, and from its malleability will form a complete protecting coat. This coat may be put upon the article to be plated in the same manner that is employed for tinning iron sheets for the purpose of making commercial sheet tin, and the article (is then ready for the nickel solution. The, other non-oxidizable metals might be employed but they are too expensive to be available.
Attempts to deposit nickel upon zinc directly have hitherto failed because when the zinc is plunged into any bath usually employed, it becomes blackened and will not receive the nickel.
In completing our process, therefore, we employ a bath composed of chloride of nickel and ammonium, together with chloride of iron, by means of which we deposit the nickel 1. The solution, composed of chloride of nickel and ammonium, and chloride of iron, for the purpose of plating directly upon zinc, substantially as described.
2. The method of preparing base metals to receive an electroplating of nickel, the same consisting in applying a surface of zinc previous to the nickel-plating, substantially as described.
3. As new articles of manufacture, metal goods having a nickel-plating deposited directly on a zinc surface, as set forth.
OAMILLO MAGGIO. GIUSEPPE MAFFIOLA.
Witnesses:
GEO. H. STRONG, O. M. RICHARDSON.
US174691D Improvement in nickel-plating Expired - Lifetime US174691A (en)

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US174691A true US174691A (en) 1876-03-14

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