US1651680A - Leaching apparatus - Google Patents

Leaching apparatus Download PDF

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US1651680A
US1651680A US647985A US64798523A US1651680A US 1651680 A US1651680 A US 1651680A US 647985 A US647985 A US 647985A US 64798523 A US64798523 A US 64798523A US 1651680 A US1651680 A US 1651680A
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tank
launder
pulp
particles
solution
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US647985A
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Henry Y Eagle
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ARCHER E WHEELER
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ARCHER E WHEELER
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0238Moving bed of solid material on fixed or rotating flat surfaces, e.g. tables combined with rotating elements or on rotating flat surfaces

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  • This invention relates to apparatus such as are used in installations where pulverized ore is subjected to the action of leaching sov lutions with agitation.
  • the dissolving of the soluble constituent of the material is effected in tanks provided with agitators, in which the material and the solution are continuously agitated for the length l0 of time necessary to effect the desired degree of dissolution.
  • the size of particle which such a leaching device could successfully handle has been limited to very1 smalll sizes.
  • the work is only accomplished by maintaining -definite conditions of pulp density-that is, the larger the size of particles to be kept in suspension, the thicker must be the pulp.
  • the solid material is agitated with the solvent, continuously flowing into the agitating tank at one point and out at another point at substantially the same rate.
  • the difficulty is Vto get the larger particles to go to the outlet. Unless they do this, they gradually accumulate in the bottom of the tank and in time stop its operation.
  • This necessity of carrying the larger particles to the outlet at the same rate at which they enter the tank has made it necessary to maintain the solution in the tank of a comparatively high density so that the solid particles will not fall rapidly through it, but will be held up long enough to pass to the outlet, near' the level in the tank. And even with a comparatively dense solution the size of the solid particles which the ordinary machine can andle is limited. A portion of the solution, in thc subsequent Washing operations, is always held in the apparatus, and becomes practically part of the capital thereof, and this retained portion of the solution is the more valuableas the solution isdenser.
  • Fig. 1 is a vertical longitudinal'section
  • Fig. 2 is a top plan thereof and Fig. 3 is a 1an of a detail.
  • e apparatus comprises a substantially cylindrical wall 10 having a bottom l2 through the center of which extends a pipe 14 connected with suitable air supply line 16 having'a control valve 18 located therein.
  • a tubular shaft 20 Centrally disposed within the tank 10 is a tubular shaft 20 having outwardly extending trough-like arms 22 and 2.4 connected at its upper end.
  • the shaft 2() and arms 22 l rotate together and are ldriven by a pulley 26 secured to a stub shaft 28 fast lin a hub 30 which is suitably secured to the arms 22 and 24.
  • the pulley 26 is driven by a belt 32 connected to a motor or other suitable source of power, notl shown.
  • Bearings 34 and 36 of any usual or suitable design are provided for rotatably mounting the shaft 20 and the parts carried thereby.
  • the shaft has, secured thereto outwardly extending arms 38 provided with prongs or projections 40 which serve to rake the particles of material which 'fall to the bottom of the tank.
  • the projections 40 are inclined as shown in Fig. 2 so that they Vgradually force the large particles of solid material on the bottom to the center and to the inlet of the airlift.
  • annular launder 42 which is adapted to receive the pulp which is discharged from the arms 22 and 24 as the latter rotate, it being apparent that the pulp discharged from the rotating troughs 22 and 24 will be distributed quite uniformly throughout the length of the annular launder.
  • the launder 42 does not extend fully around the inner periphery of the tank but is formed with end walls 44 and 46 leaving an opening 48 into which extends the inlet launder so that the material flowing therefrom enters directly into the tank'and not into the peripheral launder 42.
  • the launder 42 is adapted to discharge part of. its contents into an outlet launder 52 and part of its contents into the tank through an -outlet port 54 formed in the vertical wall 43 of said launder 42.
  • the outflow will be greater than the 'iniow through the launder 50. If the weir is lowered progressively, the'outfiow through the launder 52 will be reduced to a point where it is less than the inflow, and the level in the tank will gradually'rise to the Weir and slightly above it. thus increasing the outflow to the launder 52 until a balance is reached and thelevel in the tank remains stationary slightly above the weir.
  • the port 54 may be adjustable, as shown in Fig. 3.
  • I would pro-l vide flanges 58 at the sides for the introduction of plates of different sizes. to reduce the opening accordingly.
  • the apparatus may be used also for pulp ofv different densities, which in ordinaryv leaching work permits .the use oflow grade solutions and of a cheap washing installation. y
  • the vterm launder herein is used generally to-indicate a ⁇ variety ofv 'receptacles and pipes which will serve the Ysame purpose.
  • the apparatus may comprise other known means 'of agitation and of directing the larger particles at the bottom to the air lift.
  • the annular launder is arranged to receive approximately or substantially all the pulp lifted. But it will be appreciated that it may be arranged'to receive less than .this and still function satisfactorily. It is important that it shall be of such Size as to hold a substantial proportion of the coarser materialwhich is in process of passing'through the tank at any given time. Of the -material lifted into the annular launder, the coarser particles move the more slowly toward the outlet. Thus after a short initial period the annular launder will carry at all times a sufficient proportion of the coarser particles to substantially diminish the tendency to choke the air lift.
  • a leaching apparatus comprising a tank provided with means for admitting and discharging pulp, means for agitating and forcing pulp from a lower zone of the tank to an upper zone and means adapted to receive and hold more lifted nlp than is introduced through said admitting means in a given time and adapted to discharge part of it directly and return part of it to the 2.
  • a leaching apparatus comprising a tank with 'inlet and outlet launders near the top thereof, means for lifting-the pulp from a lower to an upper zone in the tank and a receiving launder ⁇ for the pulp thus lifted having a discharge opening into said outlet launder, and having also a discharge opening into the tank.
  • A. leaching apparatus comprising a tank having at a point above the normal level of the pulp a receiver arranged to discharge part of its contents from the tank and to return part to the tank, and means for lifting agitated pulp into said receiver.
  • a leaching apparatus having an air ⁇ lift adapted to distribute the pulp in a circular zone near the top of the apparatus and a receiver for the pulp so distributed, saidre DCver having a discharge opening to a point outside of the apparatus and having an opening discharging back into the. apparatus and adapted to maintain the level thereof.
  • a leaching apparatus having an air lift with a rotary member adapted to distribute the pulp in a circular zone near theI top of the tank and an annular receptacle Ahaving a discharge opening to a point outside ofv the tank, said receptacle being adapted to receive and to hold asubstantial proportion of the coarser material which is inthe tank at any given time.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crushing And Grinding (AREA)

Description

Patented Dec. 6, 1927.
UNITED STATE-s PATENT OFFICE.
nENnY Y. EAGLE, oF BROOKLYN, NEW Yonx, AssIGNoB oF ONE-HALL' 'ro AEcHEn E WHEELER, oENEw YoEx, N. Y. v v
LEACHING APPARATUS.
Application led June 27, 1923. Serial No. 647,985.
This invention .relates to apparatus such as are used in installations where pulverized ore is subjected to the action of leaching sov lutions with agitation.
In the leaching of various materials, the dissolving of the soluble constituent of the material is effected in tanks provided with agitators, in which the material and the solution are continuously agitated for the length l0 of time necessary to effect the desired degree of dissolution. Heretofore, the size of particle which such a leaching device could successfully handle has been limited to very1 smalll sizes. Moreover,'on4 the largest sizes which have been successfully agitated, the work is only accomplished by maintaining -definite conditions of pulp density-that is, the larger the size of particles to be kept in suspension, the thicker must be the pulp.
This limiting factor makes it necessary to grind the ore so as to form very fine particles, which is an expensive operation. With the larger size particle, requiring pulp of greater density to keep it in suspension, a correspondingly small quantity of solution f per unit of solid results.
This latter effect naturally results in a solution carrying large quantities of the soluble material, and which makes the capital expenditure of any washing scheme in the resulting separation of the solids from the liquid, very expensive.
The solid material is agitated with the solvent, continuously flowing into the agitating tank at one point and out at another point at substantially the same rate. The difficulty is Vto get the larger particles to go to the outlet. Unless they do this, they gradually accumulate in the bottom of the tank and in time stop its operation. This necessity of carrying the larger particles to the outlet at the same rate at which they enter the tank has made it necessary to maintain the solution in the tank of a comparatively high density so that the solid particles will not fall rapidly through it, but will be held up long enough to pass to the outlet, near' the level in the tank. And even with a comparatively dense solution the size of the solid particles which the ordinary machine can andle is limited. A portion of the solution, in thc subsequent Washing operations, is always held in the apparatus, and becomes practically part of the capital thereof, and this retained portion of the solution is the more valuableas the solution isdenser.
By my invention; I am enabled to use a less dense solution than was possible before my ap aratus, and I am enabled to carry through the apparatus continuously solid particles of larger size than formerly, thus saving considerable expense in the grinding of solid material.
An embodiment of the invention is illustrated in the accompanying drawings in which- Fig. 1 is a vertical longitudinal'section;
Fig. 2 is a top plan thereof and Fig. 3 is a 1an of a detail.
e apparatus comprises a substantially cylindrical wall 10 having a bottom l2 through the center of which extends a pipe 14 connected with suitable air supply line 16 having'a control valve 18 located therein. Centrally disposed within the tank 10 is a tubular shaft 20 having outwardly extending trough-like arms 22 and 2.4 connected at its upper end. The shaft 2() and arms 22 lrotate together and are ldriven by a pulley 26 secured to a stub shaft 28 fast lin a hub 30 which is suitably secured to the arms 22 and 24. The pulley 26 is driven by a belt 32 connected to a motor or other suitable source of power, notl shown. Bearings 34 and 36 of any usual or suitable design are provided for rotatably mounting the shaft 20 and the parts carried thereby.
At its lower end, the shaft has, secured thereto outwardly extending arms 38 provided with prongs or projections 40 which serve to rake the particles of material which 'fall to the bottom of the tank.-
The projections 40 are inclined as shown in Fig. 2 so that they Vgradually force the large particles of solid material on the bottom to the center and to the inlet of the airlift.
Near the upper end of the tank, but below .the trough-like arms 22 and 24, I mount an annular launder 42 which is adapted to receive the pulp which is discharged from the arms 22 and 24 as the latter rotate, it being apparent that the pulp discharged from the rotating troughs 22 and 24 will be distributed quite uniformly throughout the length of the annular launder.
The launder 42, as shown in Fig. 2, does not extend fully around the inner periphery of the tank but is formed with end walls 44 and 46 leaving an opening 48 into which extends the inlet launder so that the material flowing therefrom enters directly into the tank'and not into the peripheral launder 42. The launder 42 is adapted to discharge part of. its contents into an outlet launder 52 and part of its contents into the tank through an -outlet port 54 formed in the vertical wall 43 of said launder 42.
` This .general type of apparatus, in which 2 the material is clrculated by forcing it conthe level, as in previous machines.
tinuously from theY bottom to the top is known 'and there are various machines operating on this principle. But the material (or most of the material) lifted to the top has .generally ,been discharged directly into `the tank again; And in order that it shall all pass out of the discharge launder it has been necessary to make the solution so dense and the particles so finethat they would pass from the upper part of the solution into the discharge launder. It is clear that any solid particle which enters the tank and which at the density of the pulp in the tank is incapable of being lkept in suspension, will eventually find its way to the bottom of the tank. In agitating leaching apparat-us heretofore constructed-,such particles have accumulated onthe tank bottom and have frequently resulted in breaking the agitating mechanism or otherwise rendering it inoperative. Even in cases where the particles have been carried upward by the a'irlift` their quick settling properties have prevented them froml being distrlliirged.l
In my,l improved. apparatus the material Vflows in at the launder 50, the particles which settle on the bottom are carried to the center andthe airlift carries them to a point above But, instead of discharging the lifted particles and solution, or most of them, back 1nto the tank directly, I discharge substantially or approximately all of the pulp, that is the particles and the lsolution into the annular launder or receiver 42. Thence the pulp is discharged, AVwithout opportunity. for the heavier particlesto separate from thelighter,
into the discharge launder 52 at substantially the same ratev at which 'the solution and the solids enter Ythe tank; the excess received by thekannular launder being` returned to the an Y The discharge from the annular launder into the tank isover a low weir 56 calculated to delivei into the tank the excess of solution carried Ytof-the annular launder over that the outlet launder 52. The risel in the level willoccur of course only during the period in which the discharge continues tobe less 1 than the feed. We assumethe-feed to be constant. While the level -in the tank is below the Aweir a Vcertain percentage of the solution will flow out through the launder 52, the quantity which will be discharged in this way being dependent on the height of the weir. Ifthe Weir-is too high the outflow will be greater than the 'iniow through the launder 50. If the weir is lowered progressively, the'outfiow through the launder 52 will be reduced to a point where it is less than the inflow, and the level in the tank will gradually'rise to the Weir and slightly above it. thus increasing the outflow to the launder 52 until a balance is reached and thelevel in the tank remains stationary slightly above the weir.
The port 54 may be adjustable, as shown in Fig. 3. For thispurpose, I would pro-l vide flanges 58 at the sides for the introduction of plates of different sizes. to reduce the opening accordingly. Generally the openmakes it unnecessary to secure the accurater sizing of the materials which was formerly required. The apparatus may be used also for pulp ofv different densities, which in ordinaryv leaching work permits .the use oflow grade solutions and of a cheap washing installation. y
. As I have said' above, there are various Astyles of agitator in which the ulp is agitatedand then forced from a ower to an upper zone and circulated thus through the tank.' My invention-is applicable to various agitators working-on this principle, and improves their operation and their capacities as described by receiving the pulp thus lifted to an upper zone .and discharging it at the desired rate without giving the solid particles therein an opportunity to settle into the genk again before reaching the outlet launer. Y .The A4annular launder maybe substituted by receptacle's'of various other shapes according tothe design of the agitator to whichv it isA to'be applied. And the vterm launder herein, is used generally to-indicate a `variety ofv 'receptacles and pipes which will serve the Ysame purpose. Also the apparatus may comprise other known means 'of agitation and of directing the larger particles at the bottom to the air lift.
In the case illustrated the annular launder is arranged to receive approximately or substantially all the pulp lifted. But it will be appreciated that it may be arranged'to receive less than .this and still function satisfactorily. It is important that it shall be of such Size as to hold a substantial proportion of the coarser materialwhich is in process of passing'through the tank at any given time. Of the -material lifted into the annular launder, the coarser particles move the more slowly toward the outlet. Thus after a short initial period the annular launder will carry at all times a sufficient proportion of the coarser particles to substantially diminish the tendency to choke the air lift.
Though I. have described with great particularity the details o'f the embodiment of the invention herein shown, it is not to be construed that I am limited thereto, as
- changes in arrangement and substitution of equivalents may be made by those skilled in the art without departing from the invention as. definedA in the appended claims.
What I claim is:
1. A leaching apparatus comprising a tank provided with means for admitting and discharging pulp, means for agitating and forcing pulp from a lower zone of the tank to an upper zone and means adapted to receive and hold more lifted nlp than is introduced through said admitting means in a given time and adapted to discharge part of it directly and return part of it to the 2. .A leaching apparatus comprising a tank with 'inlet and outlet launders near the top thereof, means for lifting-the pulp from a lower to an upper zone in the tank and a receiving launder `for the pulp thus lifted having a discharge opening into said outlet launder, and having also a discharge opening into the tank. l
4. A. leaching apparatus comprising a tank having at a point above the normal level of the pulp a receiver arranged to discharge part of its contents from the tank and to return part to the tank, and means for lifting agitated pulp into said receiver.
5. A leaching apparatus having an air` lift adapted to distribute the pulp in a circular zone near the top of the apparatus and a receiver for the pulp so distributed, saidre ceiver having a discharge opening to a point outside of the apparatus and having an opening discharging back into the. apparatus and adapted to maintain the level thereof.
6. A leaching apparatus having an air lift with a rotary member adapted to distribute the pulp in a circular zone near theI top of the tank and an annular receptacle Ahaving a discharge opening to a point outside ofv the tank, said receptacle being adapted to receive and to hold asubstantial proportion of the coarser material which is inthe tank at any given time.
In witness whereof, I have hereunto signed my name.
' HENRYY. EAGLE.
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2750265A (en) * 1950-05-15 1956-06-12 Alvah D Hadsel Chlorination apparatus
US3891593A (en) * 1972-08-08 1975-06-24 Shell Oil Co Method and apparatus for dissolution of polymer in solvent
US3958947A (en) * 1973-11-01 1976-05-25 Marcona Corporation Hydrometallurgical leaching apparatus
US4541991A (en) * 1980-01-18 1985-09-17 Elkem A/S Means for processing a solid gravel like material with a fluid
CN110641061A (en) * 2019-10-08 2020-01-03 扬州市君瑞企业管理有限公司 Pharmacy is with continuous traditional chinese medicine extraction device of press type

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2750265A (en) * 1950-05-15 1956-06-12 Alvah D Hadsel Chlorination apparatus
US3891593A (en) * 1972-08-08 1975-06-24 Shell Oil Co Method and apparatus for dissolution of polymer in solvent
US3958947A (en) * 1973-11-01 1976-05-25 Marcona Corporation Hydrometallurgical leaching apparatus
US4541991A (en) * 1980-01-18 1985-09-17 Elkem A/S Means for processing a solid gravel like material with a fluid
CN110641061A (en) * 2019-10-08 2020-01-03 扬州市君瑞企业管理有限公司 Pharmacy is with continuous traditional chinese medicine extraction device of press type

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