US1297171A - Apparatus for the treatment of one liquid with another. - Google Patents

Apparatus for the treatment of one liquid with another. Download PDF

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Publication number
US1297171A
US1297171A US20557417A US20557417A US1297171A US 1297171 A US1297171 A US 1297171A US 20557417 A US20557417 A US 20557417A US 20557417 A US20557417 A US 20557417A US 1297171 A US1297171 A US 1297171A
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Prior art keywords
liquid
agitators
separator
another
treatment
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Expired - Lifetime
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US20557417A
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Alfred Ewart Holley
Owen Edwin Mott
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Chance and Hunt Ltd
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Chance and Hunt Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/009Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/54Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
    • C07C2/56Addition to acyclic hydrocarbons
    • C07C2/58Catalytic processes
    • C07C2/62Catalytic processes with acids

Definitions

  • the stirrer may take the form of an injector for air or steam.
  • Thev apparja'tus isV particularly applicable for ynitrating organic matter and for washing nitro compounds'but the plant 1s useful for manyother physical and chemical interactions.
  • the lighter liquid from any separator passes to the agitator next in the series in one direction and the heavier liquid from that separator to the next agitator in the other direction.
  • provided light liquid is supplied to the first agitator and heavy leading' from the bottom ofv the bottom of the separators and'k are pipes leading from the top of the agitators to the' liquid to the last, there will be, due to the head produced in the separator, a constant flow of light liquid from the last separator and of heavy liquid from the first, the flow of the liquid being controlled by valves.
  • a are the agitators to the first of which heav. liquid is supplied by the plpe b, and to the ast of which light liquid is supplied by the pipe c.
  • the liquid in the agitators is the stirrers d.
  • e are the separators communicating with the agitators by a passage f.
  • g are pipes the agitators to top of the'separators.
  • z' arevalves for controlling the iiow of thev liquid.
  • the separators need notfbe in one with the agitators but may be separate vessels com- ;.municating with the agitators at about half Way.- up.
  • Each separator also mayconsist of two arts one for the light and one for the heavy iquid.
  • FIG. 2 shows only these features the apparatus being otherwise identical with Fig. 1. Similar parts are indicated by the same letters.
  • the .separator consists of two parts j and l, the part j being open top and bottom and collectmg the lighter liquid and the part'Z being closed ai; the bottom and open at the to and collecting the heavier liquid.
  • Apparatus for the treatment of one liquid with another comprising a series of agitators all at the same level, a, series of separators at the same level as the agitators, the bottom of a; separator ⁇ being connected to the bottom of an agitator in one direction and the top of a separator to the top of an agitator in the other direction, and each stirred by separator 'boing in dmo: communication mth the agitator ai, a point situatod betwoon the other connections.
  • apparatus for the treatment of one liquid with another comprising o, series Off agtai'ors an at the same level, a seas of separatos oommunoavng with and ish@ somo ovo as th@ ogto'foor and mem@ where by sho flow of the awo liquids im oppoate directions is .caused goely by the hea ⁇ prolo Jerusalem in the separatorss.

Description

A. E. HOLLEY I O. E. IVIOTT.
APPARATUS FOR THE TREATMENT 0E ONE LIQUID WITH ANOTHER.
APPLICATION FILED DEC. 5, 19H.
Patented Mur. 1I, IUIJ.
f v\ \\\\\////f//// \\\\\\\\W////////// 1km/f -UNITED STATES PATENT oFFIoE.
ALFRED EWABT HOLLEY, OF OLDBURY, AND OWEN EDWIN MOTT, OF WOOLWICH,
ENGLAND, ASSIGNOBS T0 THEMSELVES, AND CHANCE OLDIBURY, ENGLAND.
AND HUNT, LIMITED, 0F
Specification of Letters Patent.
Patented Mar. 11, 1919.
Application ilelv December 5, 1917. Serial No. 24.175,574.
there are two liquids of different specificv gravities and not completely miscible.
According to this invention oneliquid'is treated with another 'liquid by miinng'them' in a series ofvesse'ls fitted vwithstlrrers and all at the 4same level, which vessels are hereinafterreferred to as agitators, and allow- Y ing'the mixture` to ow" intolvessels atthe same level 'astheagitators and hereinafter referredfto as separators, in which gravity I may "cause 'a1 separation, and romawlilcli" asses by an openmg "near heavier liquid the bottom and 'ghter' liquid by an opening near the top, the assage from the agitator to the separator ying between these openings.4 The stirrer may take the form of an injector for air or steam.
Physical or chemical interactions may be carried out by these Vmeans and provisions may be made ',.forgcooling onheating the liquids.
Thev apparja'tus isV particularly applicable for ynitrating organic matter and for washing nitro compounds'but the plant 1s useful for manyother physical and chemical interactions.
The lighter liquid from any separator passes to the agitator next in the series in one direction and the heavier liquid from that separator to the next agitator in the other direction. Thus, provided light liquid is supplied to the first agitator and heavy leading' from the bottom ofv the bottom of the separators and'k are pipes leading from the top of the agitators to the' liquid to the last, there will be, due to the head produced in the separator, a constant flow of light liquid from the last separator and of heavy liquid from the first, the flow of the liquid being controlled by valves.
The invention is illustrated in the accompanying drawings in which Figure 1 is a section and Fig. 2 is a similar view showing a modification.
In the drawings a are the agitators to the first of which heav. liquid is supplied by the plpe b, and to the ast of which light liquid is supplied by the pipe c.
The liquid in the agitators is the stirrers d.
e are the separators communicating with the agitators by a passage f. g are pipes the agitators to top of the'separators.
z' arevalves for controlling the iiow of thev liquid.
The separators need notfbe in one with the agitators but may be separate vessels com- ;.municating with the agitators at about half Way.- up.
Each separator also mayconsist of two arts one for the light and one for the heavy iquid.
This is illustrated in Fig. 2 which shows only these features the apparatus being otherwise identical with Fig. 1. Similar parts are indicated by the same letters.
The .separator consists of two parts j and l, the part j being open top and bottom and collectmg the lighter liquid and the part'Z being closed ai; the bottom and open at the to and collecting the heavier liquid.
TVhat We claim is 1. Apparatus for the treatment of one liquid with another, comprising a series of agitators all at the same level, a, series of separators at the same level as the agitators, the bottom of a; separator` being connected to the bottom of an agitator in one direction and the top of a separator to the top of an agitator in the other direction, and each stirred by separator 'boing in dmo: communication mth the agitator ai, a point situatod betwoon the other connections.
2. l'n apparatus for the treatment of one liquid with another comprising o, series Off agtai'ors an at the same level, a seas of separatos oommunoavng with and ish@ somo ovo as th@ ogto'foor and mem@ where by sho flow of the awo liquids im oppoate directions is .caused goely by the hea` prolo duced in the separatorss.
Ammo @WAM HoLLEY. o-WEN @DMN Mom.
US20557417A 1917-12-05 1917-12-05 Apparatus for the treatment of one liquid with another. Expired - Lifetime US1297171A (en)

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Cited By (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2682453A (en) * 1952-03-19 1954-06-29 Atomic Energy Commission Mixer-settler contact apparatus
US2778717A (en) * 1950-11-21 1957-01-22 Decker Peter Process and apparatus for the separation of mixtures of substances by continuous countercurrent distribution in solvents
US2881920A (en) * 1956-06-11 1959-04-14 Shell Dev Settler with paddle
US2895808A (en) * 1954-10-19 1959-07-21 Fisons Pest Control Ltd Apparatus for the separation of solutes by partition
US2937078A (en) * 1956-02-03 1960-05-17 Atomic Energy Authority Uk Mixer-settler apparatus
US2990254A (en) * 1958-01-29 1961-06-27 Ca Atomic Energy Ltd Liquid-liquid contact extractor
US3089756A (en) * 1957-01-10 1963-05-14 Atomic Energy Authority Uk Liquid-liquid contacting apparatus
US3173908A (en) * 1962-12-17 1965-03-16 Rexall Drug Chemical Method of fractionating polysaccharide mixtures
US3212857A (en) * 1960-05-23 1965-10-19 Buckau Wolf Maschf R Counter-current extraction apparatus
US3220802A (en) * 1959-10-06 1965-11-30 Fisons Pest Control Ltd Separation of solutes by liquid-liquid extraction
US3325255A (en) * 1963-09-17 1967-06-13 Robert E Treybal Liquid extractor
US3549332A (en) * 1969-01-13 1970-12-22 Upjohn Co Countercurrent liquid-liquid extraction device
US3862039A (en) * 1973-03-28 1975-01-21 Robert L Summers Gravity oil-water separator with two interconnected singular cells having automatic free oil discharge
US4271128A (en) * 1976-02-10 1981-06-02 Hoechst Aktiengesellschaft Apparatus for recovering alcoholic phosphoric acid solutions from acid phosphates
US5076930A (en) * 1988-10-19 1991-12-31 Stone & Webster Engineering Corporation Apparatus and process for liquid-liquid contact
US5160623A (en) * 1988-10-19 1992-11-03 Stone & Webster Engineering Corp. Apparatus and process for fluid-fluid contact
US5609764A (en) * 1994-02-08 1997-03-11 In.Tec. International Environment Technology S.R.L. Extraction column or tower with separate volumes
US6054060A (en) * 1998-11-19 2000-04-25 Aquitic Technology Inc. Liquid purfication system and method for decontaminating microbe infested liquid
US6454103B1 (en) * 1997-04-09 2002-09-24 Bayer Aktiengesellschaft Multiphase extractor with a wash chamber
US6569339B1 (en) * 1998-10-29 2003-05-27 Outokumpu Oyj Method for reducing the size of solvent extraction process steps and cell for using in the solvent extraction process
US20070095765A1 (en) * 2005-10-28 2007-05-03 Kozak Andrew F Iii Liquid purification system and method for purifying a liquid using liquid-to-liquid heating and cooling
US20080237107A1 (en) * 2007-03-29 2008-10-02 Aquitic Technology, Inc. Desalinization system and method
CN112999692A (en) * 2019-12-19 2021-06-22 国立研究开发法人日本原子力研究开发机构 Device for producing specific substances by liquid-liquid extraction

Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2778717A (en) * 1950-11-21 1957-01-22 Decker Peter Process and apparatus for the separation of mixtures of substances by continuous countercurrent distribution in solvents
US2682453A (en) * 1952-03-19 1954-06-29 Atomic Energy Commission Mixer-settler contact apparatus
US2895808A (en) * 1954-10-19 1959-07-21 Fisons Pest Control Ltd Apparatus for the separation of solutes by partition
US2937078A (en) * 1956-02-03 1960-05-17 Atomic Energy Authority Uk Mixer-settler apparatus
US2881920A (en) * 1956-06-11 1959-04-14 Shell Dev Settler with paddle
US3089756A (en) * 1957-01-10 1963-05-14 Atomic Energy Authority Uk Liquid-liquid contacting apparatus
US2990254A (en) * 1958-01-29 1961-06-27 Ca Atomic Energy Ltd Liquid-liquid contact extractor
US3220802A (en) * 1959-10-06 1965-11-30 Fisons Pest Control Ltd Separation of solutes by liquid-liquid extraction
US3212857A (en) * 1960-05-23 1965-10-19 Buckau Wolf Maschf R Counter-current extraction apparatus
US3173908A (en) * 1962-12-17 1965-03-16 Rexall Drug Chemical Method of fractionating polysaccharide mixtures
US3325255A (en) * 1963-09-17 1967-06-13 Robert E Treybal Liquid extractor
US3549332A (en) * 1969-01-13 1970-12-22 Upjohn Co Countercurrent liquid-liquid extraction device
US3862039A (en) * 1973-03-28 1975-01-21 Robert L Summers Gravity oil-water separator with two interconnected singular cells having automatic free oil discharge
US4271128A (en) * 1976-02-10 1981-06-02 Hoechst Aktiengesellschaft Apparatus for recovering alcoholic phosphoric acid solutions from acid phosphates
US5076930A (en) * 1988-10-19 1991-12-31 Stone & Webster Engineering Corporation Apparatus and process for liquid-liquid contact
US5160623A (en) * 1988-10-19 1992-11-03 Stone & Webster Engineering Corp. Apparatus and process for fluid-fluid contact
US5609764A (en) * 1994-02-08 1997-03-11 In.Tec. International Environment Technology S.R.L. Extraction column or tower with separate volumes
US6454103B1 (en) * 1997-04-09 2002-09-24 Bayer Aktiengesellschaft Multiphase extractor with a wash chamber
US6569339B1 (en) * 1998-10-29 2003-05-27 Outokumpu Oyj Method for reducing the size of solvent extraction process steps and cell for using in the solvent extraction process
US6054060A (en) * 1998-11-19 2000-04-25 Aquitic Technology Inc. Liquid purfication system and method for decontaminating microbe infested liquid
US20070095765A1 (en) * 2005-10-28 2007-05-03 Kozak Andrew F Iii Liquid purification system and method for purifying a liquid using liquid-to-liquid heating and cooling
US20080237107A1 (en) * 2007-03-29 2008-10-02 Aquitic Technology, Inc. Desalinization system and method
US7470873B2 (en) 2007-03-29 2008-12-30 Aquitic Technology, Inc. Desalinization system and method
CN112999692A (en) * 2019-12-19 2021-06-22 国立研究开发法人日本原子力研究开发机构 Device for producing specific substances by liquid-liquid extraction

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