US1097474A - Device for mixing emulsions. - Google Patents

Device for mixing emulsions. Download PDF

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Publication number
US1097474A
US1097474A US78080513A US1913780805A US1097474A US 1097474 A US1097474 A US 1097474A US 78080513 A US78080513 A US 78080513A US 1913780805 A US1913780805 A US 1913780805A US 1097474 A US1097474 A US 1097474A
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Prior art keywords
cone
working surfaces
members
mixing
liquid
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Expired - Lifetime
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US78080513A
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Wilhelm Gotthilf Schroeder
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/44Mixers in which the components are pressed through slits
    • B01F25/441Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
    • B01F25/4413Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the slits being formed between opposed conical or cylindrical surfaces
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/44Mixers in which the components are pressed through slits
    • B01F25/442Mixers in which the components are pressed through slits characterised by the relative position of the surfaces during operation
    • B01F25/4422Mixers in which the components are pressed through slits characterised by the relative position of the surfaces during operation the surfaces being maintained in a fixed but adjustable position, spaced from each other, therefore allowing the slit spacing to be varied

Definitions

  • This invention relates to a device for mixing emulsions
  • the invention relates more particularly to devices in which the mixing is efiected by means of stepped cones, that is to say, the fluid to be ground, is pressed through the seat of a cone or of a valve which itself, in the same Way as its seat, consists of single steps, as described in the U. S. Patent 1062554.
  • stepped cones that is to say, the fluid to be ground
  • the valve seats were adjustable relatively to each other.
  • the cone is formed of single sections adjustable relatively to each other, in such manner that each single part is adjustable relatively to the others, and in that way the size of the slot or gap can be adjusted independently.
  • This device makes it possible to regulate exactly the slots and therefore the activity in the single stages, and to grind the working surfaces accurately. Moreover, liquids or gases can be introduced. between the single steps during the operation.
  • the invention relates both to devices in which this cone is stationary, and to devices in which it is rotated inany desired manner.
  • This r0- tatio-n can be effected either by providing the cone in the known manner with helical screw-thread or blades on which the liquid first into hollow spacesto be ground acts as in a turbine, or the cone can be supported by a spindle which is .guided outward and provided with a driving pulley by means of which it can be rotated.
  • the single steps of the cone can have straight or oblique surfaces. The liquid escaping from the surfaces preferably passes in which a mixing of the liquid takes place, which also prevents the fine liquid jets from impinging direct against the metalsurfaces and thus damaging it.
  • a device according to this invention is Specification of Letters Patent.
  • FIG. 1 is a vertical section
  • Fig. 2 a section on the line A-B of Fig. 1
  • Fig. 3- is a section on the line CD of Fig. 1.
  • the cone has four'working surfaces 6 b b 6* and the casing has also a corresponding num nular spaces c e e a
  • the cone pressed on with heavy pressure consists according to this inventiom'of four sections (2 (Z d and d screwed into each other.
  • the upper end of each single cone section is provided with a screwthread m m m with which it engages with the corresponding tapped thread of the superposed cone section.
  • the perforationof each cone carrying the tapped thread is exactly cylindrical at n n and a so that the single cones can fit exactly into each other.
  • two coacting members as used in the claims applies to those members carry- *r of aning a series of working-surfaces coacting with a corresponding series of working surfaces carried by the other.
  • the grinding in of the working surfaces of the cones is effected by the single cone sections being first screwed together and turned as a whole in such a manner a curately as possible to the corresponding that they correspond as working surfaces of the casing. The absolutely accurate grinding in then takes place, so that during the grinding process all the working surfaces grind simultaneously.
  • the casing is provided in addition'to the inletconduit slot-oz is slightly I a, with two further inlet branches a and a the former of which opens into the hollow chamber 6 and the latter into the hollow chamber a
  • These inlet branches make it possible to supply to the emulsion to be treated, certain ingredients such as gases, liquids or even solid substances, for instance, those acting as catalyzers, when it is desired to impart to the fats treated special properties, for instance higher melting points or the like.
  • the slots 0: a of, etc are of course adjusted in such manner that the increase of liquid or other substance should bealso taken into account, so that approximately the same work of emulsioning is performed at each working stage.
  • the cone is guided in the casing by making its bottom end triangular as shown in Fig. 3.
  • the uppermost cone d is provided at the circumference with grooves 0 and for the rest turned to suit exactly the inner wall of the casing, so that the liquid can escape only through the grooves 0. In any case, the cone can also rotate, and to that purpose to be driven positively from the outside, or rotated by the liquid itself. I i
  • a device for mixing emulsions the combination of two coacting members, one of said members being provided with annular grooves adjacent to the Working surfaces, means for introducing and discharging liquid, means for introducing matter 7 at a plurality of points between said coacting members, and means for independently adjusting and setting the said members.
  • a device for mixing emulsions the combination of a member carrying a V- shaped opening, stepped working surfaces within said opening, a second member, V- shaped, carrying working surfaces adapted to coact with first-mentloned working surfaces, said second member being formed of aseries of units, each unit carrying a working surface, externally threaded at its upper portion and internally threaded at its lower portion, each unit adapted to screw into the unit above it and to receive-the upper portion of the unit below it.
  • a member carrying. a V- shaped opening, stepped working surfaces within said opening, a second member, V- shaped, carrying working surfaces adapted to coact with first-mentioned working surfaces, said second member being formed of a series of units, each unitcarrying a working surface, externally threaded at its upper portion and internally threaded at Its lower portion, each unit adapted to screw into the unit above it and to receive the upper portion of the unit below it, and means for regulating the distances between said working surfaces, comprising a" plurality of disks, adapted to limit ,the distance that one unitis screwed into the one above it.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)

Description

W. G. SCHRO'DER.
Patented May 19, 1914.
om'runsmrus PATENT 'orrrou.
Winn-ELM eo'r'rnrnr sonnbnun, or LTFBECK, GERMANY.
nnvrcn For. mxnie EMULSIONS.
' of which the following is a specificatiom.
This invention relates to a device for mixing emulsions;
The invention relates more particularly to devices in which the mixing is efiected by means of stepped cones, that is to say, the fluid to be ground, is pressed through the seat of a cone or of a valve which itself, in the same Way as its seat, consists of single steps, as described in the U. S. Patent 1062554. In order to enable the size of the slot or gap between the .single'steps of the cone to be regulated, a solid cone with several steps was hitherto used while the valve seats were adjustable relatively to each other. According to this invention, the cone is formed of single sections adjustable relatively to each other, in such manner that each single part is adjustable relatively to the others, and in that way the size of the slot or gap can be adjusted independently. This device makes it possible to regulate exactly the slots and therefore the activity in the single stages, and to grind the working surfaces accurately. Moreover, liquids or gases can be introduced. between the single steps during the operation. The invention relates both to devices in which this cone is stationary, and to devices in which it is rotated inany desired manner. This r0- tatio-n can be effected either by providing the cone in the known manner with helical screw-thread or blades on which the liquid first into hollow spacesto be ground acts as in a turbine, or the cone can be supported by a spindle which is .guided outward and provided with a driving pulley by means of which it can be rotated. The single steps of the cone can have straight or oblique surfaces. The liquid escaping from the surfaces preferably passes in which a mixing of the liquid takes place, which also prevents the fine liquid jets from impinging direct against the metalsurfaces and thus damaging it. v
A device according to this invention is Specification of Letters Patent.
have in- Patented May 19, 1914.
Application filed July as, 1913. ser al s. 780,805.
illustrated by way of example in the accompanying drawing in which Figure 1 is a vertical section, Fig. 2 a section on the line A-B of Fig. 1, and Fig. 3- is a section on the line CD of Fig. 1.
As shown in the drawing, the cone has four'working surfaces 6 b b 6* and the casing has also a corresponding num nular spaces c e e a The cone pressed on with heavy pressure, consists according to this inventiom'of four sections (2 (Z d and d screwed into each other. To that end, the upper end of each single cone section is provided with a screwthread m m m with which it engages with the corresponding tapped thread of the superposed cone section. The perforationof each cone carrying the tapped thread, is exactly cylindrical at n n and a so that the single cones can fit exactly into each other. Tn this apparatus any desired number of conical surfaces can be screwed into each other'in the manner described; The several conical sections thus tightly screwed together form practically. one solid member. -This member fits into the casing in such a manner that the working surfaces on the several conical sections coact with corresponding working surfaces located within the casing.
The term two coacting members as used in the claims applies to those members carry- *r of aning a series of working-surfaces coacting with a corresponding series of working surfaces carried by the other. The grinding in of the working surfaces of the cones is effected by the single cone sections being first screwed together and turned as a whole in such a manner a curately as possible to the corresponding that they correspond as working surfaces of the casing. The absolutely accurate grinding in then takes place, so that during the grinding process all the working surfaces grind simultaneously.
When the grinding process is completed, the
cone is removed, divided into its single sec' slightly larger thanthe next a andso on. i
"' @In the construction illustrated, the casing is provided in addition'to the inletconduit slot-oz is slightly I a, with two further inlet branches a and a the former of which opens into the hollow chamber 6 and the latter into the hollow chamber a These inlet branches make it possible to supply to the emulsion to be treated, certain ingredients such as gases, liquids or even solid substances, for instance, those acting as catalyzers, when it is desired to impart to the fats treated special properties, for instance higher melting points or the like. When liquid is introduced through the branches in question, the slots 0: a of, etc, are of course adjusted in such manner that the increase of liquid or other substance should bealso taken into account, so that approximately the same work of emulsioning is performed at each working stage.
The cone is guided in the casing by making its bottom end triangular as shown in Fig. 3. The edges of the triang18 .are -however turned cylindrically,, so that they have, proper guidance in thex'inlet pipe a. The uppermost cone d is provided at the circumference with grooves 0 and for the rest turned to suit exactly the inner wall of the casing, so that the liquid can escape only through the grooves 0. In any case, the cone can also rotate, and to that purpose to be driven positively from the outside, or rotated by the liquid itself. I i
Having now particularly described and ascertained the nature of my said invention and in what manner the same is to be performed, I declare that what I claim is 1. In a device for mixing emulsions, the combination of two coacting members, means for introducing and discharging liquid, means for introducing matter at a plurality of points between said coacting members, and means for independently adjusting and setting the said members.
2. In a device for mixing emulsions, the combination of two coacting members, one of said members being provided with annular grooves adjacent to the Working surfaces, means for introducing and discharging liquid, means for introducing matter 7 at a plurality of points between said coacting members, and means for independently adjusting and setting the said members.
9 In a device for mixing emulsions, the combination of two coacting members, guide i means for holding the two in alinement, means for introducing and discharging fluid,
1gality of points between said coacting memers. I
4. In a device for mixing emulsions,the combination of two coacting members, one of said members being providedwith annular grooves adjacent to the working surfaces, means for introducing and discharging fluid, and means for introducing matter at a plurality ofpoints between said coacting members.
5. In a device for mixing emulsions, the combination of a member carrying a V- shaped opening, stepped working surfaces within said opening, a second member, V- shaped, carrying working surfaces adapted to coact with first-mentloned working surfaces, said second member being formed of aseries of units, each unit carrying a working surface, externally threaded at its upper portion and internally threaded at its lower portion, each unit adapted to screw into the unit above it and to receive-the upper portion of the unit below it.
6. In a device for mixing emulsions, the combination of a member carrying. a V- shaped opening, stepped working surfaces within said opening, a second member, V- shaped, carrying working surfaces adapted to coact with first-mentioned working surfaces, said second member being formed of a series of units, each unitcarrying a working surface, externally threaded at its upper portion and internally threaded at Its lower portion, each unit adapted to screw into the unit above it and to receive the upper portion of the unit below it, and means for regulating the distances between said working surfaces, comprising a" plurality of disks, adapted to limit ,the distance that one unitis screwed into the one above it.
In testimony, that I claim the foregoing as my invention, I have signed my name in presence of two witnesses, this twelfth day of July 1913.
WILHELM GOTTHILF SGIIRGDER.
55 and means for introducing matter at a p1u-. 7
US78080513A 1913-07-23 1913-07-23 Device for mixing emulsions. Expired - Lifetime US1097474A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2652234A (en) * 1950-03-31 1953-09-15 Feldmann Bernard Homogenizer
US3376023A (en) * 1964-08-28 1968-04-02 Lage James Richard Mixing process
US3684251A (en) * 1970-09-08 1972-08-15 Us Army Apparatus for continuous emulsification
US4624415A (en) * 1985-04-01 1986-11-25 American Standard Inc. Control assembly
WO2009096825A1 (en) 2008-01-29 2009-08-06 Tetra Laval Holdings & Finance S.A. A homogenizer valve
WO2013142043A1 (en) * 2012-03-20 2013-09-26 3M Innovative Properties Company A device for mixing and dispensing flowable components
US20140177382A1 (en) * 2010-12-22 2014-06-26 Tetra Laval Holdings & Finance S.A. Homogenizing valve
WO2021240123A1 (en) * 2020-05-28 2021-12-02 Micropore Technologies Limited Membrane emulsification apparatus with refiner and method of preparing a refined emulsion

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2652234A (en) * 1950-03-31 1953-09-15 Feldmann Bernard Homogenizer
US3376023A (en) * 1964-08-28 1968-04-02 Lage James Richard Mixing process
US3684251A (en) * 1970-09-08 1972-08-15 Us Army Apparatus for continuous emulsification
US4624415A (en) * 1985-04-01 1986-11-25 American Standard Inc. Control assembly
WO2009096825A1 (en) 2008-01-29 2009-08-06 Tetra Laval Holdings & Finance S.A. A homogenizer valve
EP2237658A1 (en) * 2008-01-29 2010-10-13 Tetra Laval Holdings & Finance SA A homogenizer valve
EP2237658A4 (en) * 2008-01-29 2014-10-08 Tetra Laval Holdings & Finance A homogenizer valve
US20140177382A1 (en) * 2010-12-22 2014-06-26 Tetra Laval Holdings & Finance S.A. Homogenizing valve
US9199208B2 (en) * 2010-12-22 2015-12-01 Tetra Laval Holdings & Finance S.A. Homogenizing valve having radially and axially arranged gaps
WO2013142043A1 (en) * 2012-03-20 2013-09-26 3M Innovative Properties Company A device for mixing and dispensing flowable components
US9295530B2 (en) 2012-03-20 2016-03-29 3M Innovative Properties Company Device for mixing and dispensing flowable components
WO2021240123A1 (en) * 2020-05-28 2021-12-02 Micropore Technologies Limited Membrane emulsification apparatus with refiner and method of preparing a refined emulsion

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