US1082A - Improvement in the process of rectifying the oil of turpentine and other essential oils - Google Patents

Improvement in the process of rectifying the oil of turpentine and other essential oils Download PDF

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US1082A
US1082A US1082DA US1082A US 1082 A US1082 A US 1082A US 1082D A US1082D A US 1082DA US 1082 A US1082 A US 1082A
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oil
turpentine
essential oils
improvement
rectifying
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/02Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills

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  • a case is placed into a vat, H, which is supplied with and contains water, the temperature of which is to range from, say, 120 to 150 Fahrenheit, aceordin g to circumstances.
  • Said case is made with partitions D inside. One, connected to the top of the ease, reaches down to within two or three inches of the bottoms.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

A. V. H. WEBB.
Apparatus f'or Producing Camphene.
No. 1,082. Patented Feb. 19, 1839.
STATES PATENT A. v. H. WEBB, or new YORK, N. Y.
IMPROVEMENT IN THE PROCESS OF RECTlFYlNG THE OIL 0F TURPENTINE AND OTHER ESSENTIAL OILS, SEPARATELY 0R COMBINED, THE PRODUCT OF WHICH HE DENOIVHNATES CAMPHENE-OIL.
Specification forming part of Letters PatentNo. 1,4582, dated February l9, 1839.
To a]! whom it may concern:
to it known that I, AUGUSTUS V. H. \VEBB, of the city, county, and State of New York, have discovered a method of producing aliquid for the purpose of affording artificial light, which I denominate camphene or cam pheneoil; and I do hereby declare that the following is a full and exact description.
The nature of my discovery consists in dis tilling,with potash or other alkali and water, turpentine or the spirits or oil of turpentine and other essential oils, whether separate or combined, the result of which distillation is aliquid I denominate camphene or camphene-oil,andwhich,being burned in aburner of proper construction, produces a powerful and beautiful light. v
To enable others skilled in the art to make and use my discovery, I will describe its na' ture and operation.
I construct a still or boiler of any of the ap proved forms, A, leading therefrom an adapting pipe, B, passing upward and entering a case, 0, made of copper. or other metal, which case is placed into a vat, H, which is supplied with and contains water, the temperature of which is to range from, say, 120 to 150 Fahrenheit, aceordin g to circumstances. Said case is made with partitions D inside. One, connected to the top of the ease, reaches down to within two or three inches of the bottoms. The next, connected to the bottom, reaches to within the same distance of the top, and so on through the case, forming apartments 0 into and through which the steam is caused to pass before it enters through pipeE into the worm F,which,passin g through cold water contained in tub G, condenses it into a liquid or liquids. That portion of the steam which may be con densed in passing through the apartments in the case 0 is returned into the boiler by means of short tubes I, leading from the bottom of each apartment into a main returirpipe, J, the whole apparatus being represented in the drawing herewith presented. In the still or boiler I place water, with such proportion of alkali as the quantity of impure matter contained in the spirits or oils to be added may require, to be governed by the skill of the operator. I then add the turpentine or spirits or oil of turpentine, or other essential oils, in quantity almost equal to the water, and, kindling the fire under the boiler, the steam rises and passes through the apparatus described. The heavier parts,being condensed, return into the still, and the lighter and purer parts, issuing at the upper extremity of the case 0, enter the worm F, and are condensed into two liquidsviz., water and the oil, denominated camphene or camphene-oil.
.TVhat I claim as my discovery, and desire to secure by Letters Patent, is-
The manufacturing the liquid here denomiis produced by distillation with water and potash or other alkali,turpentine, or the spirits or the oil of turpentine, or other essential oils, whether separate or combined, and by what ever apparatus or mode the distillation may be effected.
AUGS. V. H. TVEBB.
. TVitnesses:
TVM. P. ELLIOT,
BEN-I. E. GREEN.
nated camphene or camphene-oil, which
US1082D Improvement in the process of rectifying the oil of turpentine and other essential oils Expired - Lifetime US1082A (en)

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