US100668A - Improvement in the manufacture of illuminating-gas - Google Patents

Improvement in the manufacture of illuminating-gas Download PDF

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US100668A
US100668A US100668DA US100668A US 100668 A US100668 A US 100668A US 100668D A US100668D A US 100668DA US 100668 A US100668 A US 100668A
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gas
retorts
superheater
illuminating
manufacture
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/02Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils in retorts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/26Fuel gas

Definitions

  • my invention consists in the employment of a vaporizing-vessel in connection with a superheater or superheaters and the ordinary clay or iron retorts, for the purpose of making an illuminating-gas of a uniform quality.
  • the vapors are carried into a superheater that is heated by the waste heat of the furnace under the retorts.
  • No w as the retorts are only heated to a cherryred heat, and the super-heaters are raised above and in the rear of them, it follows that the temperature ofthe superheaters will always bear a relatively lesser amount of heat than the retorts themselves, and as the tem perature of the vapor in passing into and through the superheaters before it enters the retorts is largely increased, the retorts are not cooled olf, but we are enabled to keep up the necessary cherry-red heat.
  • A represents an ordinary furnace under the still or vaporizer B.
  • C is a vapor-pipe, provided with a stopcook, D, and communicatingwith the superheater E, and has an upward inclination to the superheater, so that any condensation that occurs before reaching the superheater may return to the vaporizer.
  • This superheater is connected with an additional horizontal superheater, L, in the brick masonry in the rear of and below the superheater E, by a pipe entering the superheater near its bottom.
  • the horizontal superheater L is connected with the backs of the retorts G G1 (l2 by the pipes and stop-cocks F Fl F2.
  • the gas is now thoroughly decomposed by passing through the retorts, and makes its exit into the stand-pipes H I-I1 H2, thence into and through an ordinary condenser or coolerand from thence into the gas-holder.
  • I is an additional vapor-pipe leading from the vaporizer B into an ordinary condensing-coil, J, and is provided with a stop-cock, K.
  • the object of vthis is to test atjany time the rapidity of the production of vapor. This is accomplished by shutting of the stop-cock D on the pipe (l leading from the vaporizer B to the superheater, and opening the stop-cock K, and measuring the condensed vapor for a specied time.
  • the hydrocarbon liquid is supplied to the vaporizer B through the pipe M provided with a stop-cock, N.
  • This apparatus or combination furnishes a very compact, reliable, and perfect hydrocarbon-gas generator, unlike the older process of permitting the liquid hydrocarbons to drop upon the hot surfaces of the retorts, where either destructive or imperfect decomposition is always taking place, by reason of the coke or dry carbon forming upon the vhotretorts; and preventing thel liquid from cominginto communicate with the furnace, whereby the waste' heat from the furnace is utilized, all constructed and arranged substantially asset forth.
  • test-pipe I arranged and operated in combination with the above, substantially as and for the purposes described.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Description

UNITEDSTATES PATENT OFFICE.
ALONZO o. RAND, OE NEw YORRL'N. Y., AssIGNoR To'wM. J. NroHoLs, ALDEN D. RAND, AND RICHARD E. BROWN, OE sAME PLAGE.
IMPRQVEMENTIN'TH MANUFACTURE oF |L|.uw||NAT|NG.GAs.
Specification forming part of Letters Patent N0.'100,668,' dated March 8, 1870. i
To all whom it may concern:
Be it known that I, ALONZO C. RAND., ofr
New York, in the county of New York and in the State of New York, have invented certain new and usefullmprovements inthe Manufacture of Illuminating-Gas; and do hereby declare that the following is a full, clear, and
exact description thereof, reference being had to the accompanying drawings and to the letters of reference marked thereon, making a part of this specification.
The nature of my invention consists in the employment of a vaporizing-vessel in connection with a superheater or superheaters and the ordinary clay or iron retorts, for the purpose of making an illuminating-gas of a uniform quality.
In order to enable others skilled in the art to which my invention appertains to make and use the same, I will vnow proceed to describe its construction and operation, referring to the annexed drawings, in which- Figure lis a vertical cross-section, and Fig. 2 is a plan view,of my machine. Fig. 3 is a view of a condensing-coil, the use of which will be hereinafterset forth.
From experience it is found that it is very essential that the vapor arising from the liquid hydrocarbons should be heated up to a point where thorough decomposition takes place, andnot to a greater or lesser temperature. An excess of heat will produce destructive decomposition, and not sufficient will so imperv fectly decompose the vapor as to produce condensation.` Now, as the boiling-point of most of the lighter specific gravities of hydrocarbon liquids ranges from 1000 to 2000, and the heavier or last products of the distillation of the ordinary crude petroleum approximates 4000 Fahrenheit, and the proper temperature necessary for the perfect decomposition of the vapor is about 10000 Fahrenheit, it most certainly follows that if the vapors that have been created at the lowboiling-points mentioned are permitted to come into immediate contact with retorts heated to 10000 Fahrenheit, a diminution of temperature in the retorts will be the result, and a large portion of the vapor pass through the retorts and condense. To prevent this the vapors are carried into a superheater that is heated by the waste heat of the furnace under the retorts. No w, as the retorts are only heated to a cherryred heat, and the super-heaters are raised above and in the rear of them, it follows that the temperature ofthe superheaters will always bear a relatively lesser amount of heat than the retorts themselves, and as the tem perature of the vapor in passing into and through the superheaters before it enters the retorts is largely increased, the retorts are not cooled olf, but we are enabled to keep up the necessary cherry-red heat.
In the annexed drawings, A represents an ordinary furnace under the still or vaporizer B. C is a vapor-pipe, provided with a stopcook, D, and communicatingwith the superheater E, and has an upward inclination to the superheater, so that any condensation that occurs before reaching the superheater may return to the vaporizer. This superheater is connected with an additional horizontal superheater, L, in the brick masonry in the rear of and below the superheater E, by a pipe entering the superheater near its bottom. The horizontal superheater L is connected with the backs of the retorts G G1 (l2 by the pipes and stop-cocks F Fl F2. The gas is now thoroughly decomposed by passing through the retorts, and makes its exit into the stand-pipes H I-I1 H2, thence into and through an ordinary condenser or coolerand from thence into the gas-holder. I is an additional vapor-pipe leading from the vaporizer B into an ordinary condensing-coil, J, and is provided with a stop-cock, K. The object of vthis is to test atjany time the rapidity of the production of vapor. This is accomplished by shutting of the stop-cock D on the pipe (l leading from the vaporizer B to the superheater, and opening the stop-cock K, and measuring the condensed vapor for a specied time. The hydrocarbon liquid is supplied to the vaporizer B through the pipe M provided with a stop-cock, N.
This apparatus or combination furnishes a very compact, reliable, and perfect hydrocarbon-gas generator, unlike the older process of permitting the liquid hydrocarbons to drop upon the hot surfaces of the retorts, where either destructive or imperfect decomposition is always taking place, by reason of the coke or dry carbon forming upon the vhotretorts; and preventing thel liquid from cominginto communicate with the furnace, whereby the waste' heat from the furnace is utilized, all constructed and arranged substantially asset forth.
l 2. The test-pipe I, arranged and operated in combination with the above, substantially as and for the purposes described.
In testimony that I claim the foregoing I have hereunto set my hand this 18th day of February, 1870. i A. C. RAND.
Witnesses J. M. MASON, W. J. NICHOLS'.
US100668D Improvement in the manufacture of illuminating-gas Expired - Lifetime US100668A (en)

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