US1004676A - Process for refining silver bullion. - Google Patents

Process for refining silver bullion. Download PDF

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Publication number
US1004676A
US1004676A US53573109A US1909535731A US1004676A US 1004676 A US1004676 A US 1004676A US 53573109 A US53573109 A US 53573109A US 1909535731 A US1909535731 A US 1909535731A US 1004676 A US1004676 A US 1004676A
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United States
Prior art keywords
bullion
silver bullion
refining
refining silver
speiss
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Expired - Lifetime
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US53573109A
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Balmer Neilly
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Individual
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Priority to US53573109A priority Critical patent/US1004676A/en
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Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B13/00Obtaining lead
    • C22B13/06Refining

Definitions

  • My invention relates to an improved process for refining silver bullion and the object of the invention is to provide a process in which the loss will be exceedingly low and the cost of refining small.
  • the apparatus I now use for carrying out the above process comprises a suitable furnace and means for supplying a blast of air to the surface of the molten metal contained in the furnace.
  • the process for refining silver bullion consisting in first melting the bullion and adding to the fused metal iron to form a speiss then suddenly cooling the metal to separate the bullion from the speiss then remelting the bullion and covering the surface of the melted bullion with a flux of a mixture of sand and boraX and finally subjecting the surface of the flux to a blast of air, as and for the purpose specified.

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Description

BALMER NEILLY, OF BRADFORD, ONTARIO, CANADA.
PROCESS FOR REFIN'ING SILVER BULLION.
No Drawing.
Specification of Letters Patent.
Application filed December 31, 1909.
Patented Oct. 3, 1911.
Serial No. 535,731.
To all whom it may concern:
Be it known that I, BALMER NEILLY, of the town of Bradford, in the county of Simcoe, in the Province of Ontario, Canada, have invented certain new and useful Improvements in Improved Processes for Itefining Silver Bullion, of which the following is the specification.
My invention relates to an improved process for refining silver bullion and the object of the invention is to provide a process in which the loss will be exceedingly low and the cost of refining small.
The apparatus I now use for carrying out the above process comprises a suitable furnace and means for supplying a blast of air to the surface of the molten metal contained in the furnace.
In order to get rid of nickel copper or cobalt present along with as much arsenic and antimony as possible I form what is termed a speiss. In order to do this the bullion is melted down in the cyclone furnace at about a temperature of 11 10 C. and iron in the form of nails added until the iron is attacked by the arsenic and antimony present. The crucible is then removed and cooled suddenly. Under these conditions the speiss separates cleanly from the bullion. The bullion is again melted down at a temperature of about 1090 C. with enough flux such as sand and borax to form a thin covering on the top of the molten metal. Air With sufficient pressure to cause a depression of about 9; of an inch on the surface is then blown on the metal until the arsenic first and then antimony are oxidized off leaving the bullion pure. This point of course is easily determined. Samples are dipped out and after cooling hammered. If they are inclined to be brittle to the least degree the metal still retains some impurities. Even a small fraction of one per cent. impurities will cause it to crack. Again on becoming pure the molten metal changes from white to a clear sea green in color.
The above process it will be seen is accomplished with a very simple apparatus and is cheap and quick.
What I claim as my invention is:
The process for refining silver bullion consisting in first melting the bullion and adding to the fused metal iron to form a speiss then suddenly cooling the metal to separate the bullion from the speiss then remelting the bullion and covering the surface of the melted bullion with a flux of a mixture of sand and boraX and finally subjecting the surface of the flux to a blast of air, as and for the purpose specified.
BALMER NEILLY.
Witnesses:
R. GOBAIN, B. Born.
Copies of this patent may be obtained for five cents each, by addressing the Commissioner of Patents, Washington, D. G.
US53573109A 1909-12-31 1909-12-31 Process for refining silver bullion. Expired - Lifetime US1004676A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US53573109A US1004676A (en) 1909-12-31 1909-12-31 Process for refining silver bullion.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US53573109A US1004676A (en) 1909-12-31 1909-12-31 Process for refining silver bullion.

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US1004676A true US1004676A (en) 1911-10-03

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2485542A (en) * 1945-01-25 1949-10-25 Socony Vacuum Oil Co Inc Protection of heat transfer media
US3892562A (en) * 1970-01-20 1975-07-01 Pyromet Inc Process for producing high purity silver
US3902890A (en) * 1973-03-12 1975-09-02 Int Nickel Co Refining silver-bearing residues

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2485542A (en) * 1945-01-25 1949-10-25 Socony Vacuum Oil Co Inc Protection of heat transfer media
US3892562A (en) * 1970-01-20 1975-07-01 Pyromet Inc Process for producing high purity silver
US3902890A (en) * 1973-03-12 1975-09-02 Int Nickel Co Refining silver-bearing residues

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