UA98474C2 - Process for the sulfinylation of a pyrazole derivative - Google Patents
Process for the sulfinylation of a pyrazole derivativeInfo
- Publication number
- UA98474C2 UA98474C2 UAA200905381A UAA200905381A UA98474C2 UA 98474 C2 UA98474 C2 UA 98474C2 UA A200905381 A UAA200905381 A UA A200905381A UA A200905381 A UAA200905381 A UA A200905381A UA 98474 C2 UA98474 C2 UA 98474C2
- Authority
- UA
- Ukraine
- Prior art keywords
- acid
- sulfinylation
- pyrazole derivative
- pyrazole
- trifluoromethylsulfinic
- Prior art date
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
The present invention relates to a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trif1uoromcthyl)phenyl]-1H-pyrazole-3-carbonitrile (II) is reacted with a sulfinylating agent selected from trifluoromethylsulfinic acid, trifluoromethylsulfinic acid anhydride, and a trifluoromethylsulfinale alkaline or alkaline earth metal salt and mixtures of the acid and/or the salt(s), in the presence of at least one amino acid complex wherein the amine(s) are selected from tertiary amines and the acid(s) are selected from hydrofluoric, hydrochloric, hydrobromic and hydroiodic acid and sulfonic acid derivatives, and with the addition of a halogenating agent.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US86517806P | 2006-11-10 | 2006-11-10 | |
PCT/EP2007/061891 WO2008055877A1 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
UA98474C2 true UA98474C2 (en) | 2012-05-25 |
Family
ID=41272785
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
UAA200905383A UA98475C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
UAA200905381A UA98474C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
UAA200905234A UA98628C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
UAA200905383A UA98475C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
UAA200905234A UA98628C2 (en) | 2006-11-10 | 2007-11-05 | Process for the sulfinylation of a pyrazole derivative |
Country Status (2)
Country | Link |
---|---|
CN (3) | CN101583602A (en) |
UA (3) | UA98475C2 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104557713B (en) * | 2013-10-22 | 2018-08-21 | 江苏托球农化股份有限公司 | High-purity ethiprole preparation method |
CN104926729B (en) * | 2014-03-18 | 2018-01-19 | 上海泰禾国际贸易有限公司 | A kind of method for synthesizing ethiprole |
CN107963993A (en) * | 2018-01-06 | 2018-04-27 | 江苏托球农化股份有限公司 | A kind of preparation method of high-purity ethiprole |
CN113825743A (en) * | 2019-03-19 | 2021-12-21 | 格哈达化工有限公司 | Method for synthesizing fipronil |
CN111004155A (en) * | 2019-09-11 | 2020-04-14 | 浙江埃森化学有限公司 | Preparation method of trifluoromethyl sulfuryl halide |
-
2007
- 2007-11-05 CN CNA2007800496448A patent/CN101583602A/en active Pending
- 2007-11-05 UA UAA200905383A patent/UA98475C2/en unknown
- 2007-11-05 CN CNA2007800496556A patent/CN101578270A/en active Pending
- 2007-11-05 CN CNA2007800496452A patent/CN101589027A/en active Pending
- 2007-11-05 UA UAA200905381A patent/UA98474C2/en unknown
- 2007-11-05 UA UAA200905234A patent/UA98628C2/en unknown
Also Published As
Publication number | Publication date |
---|---|
UA98628C2 (en) | 2012-06-11 |
CN101578270A (en) | 2009-11-11 |
CN101589027A (en) | 2009-11-25 |
CN101583602A (en) | 2009-11-18 |
UA98475C2 (en) | 2012-05-25 |
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