UA85619U - Process for the preparation of titanium carbide using shs-process - Google Patents
Process for the preparation of titanium carbide using shs-processInfo
- Publication number
- UA85619U UA85619U UAU201306814U UAU201306814U UA85619U UA 85619 U UA85619 U UA 85619U UA U201306814 U UAU201306814 U UA U201306814U UA U201306814 U UAU201306814 U UA U201306814U UA 85619 U UA85619 U UA 85619U
- Authority
- UA
- Ukraine
- Prior art keywords
- furnace charge
- container
- samples
- furnace
- shs
- Prior art date
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- Carbon And Carbon Compounds (AREA)
Abstract
A process for the preparation of titanium carbide using SHS-process comprises the preliminary operations for preparation of exothermic mixture from initial powders of metallic titanium powder and nonmetallic powder of carbon soot in a form of furnace charge, loading of furnace charge to graphite container of reactor, heating of furnace charge to ignition temperature and burning of exothermic mixture in regime of self-spreading high temperature synthesis (SHS), cooling of reactor and unloading of synthesized material. Furnace charge is prepared in a form of press tailings using organic compound, which is burned, then obtained press tailing is compacted in a form of samples of fixed size, dried to constant mass. As container unpressurized graphite container is used. Dried compacted samples of furnace charge are placed to back filling of carbon powder (fine soot). Support with container is placed to the preliminary heated working zone of the heated furnace with air atmosphere. Container with loaded compacted samples of furnace charge is hold in heating furnace to the appearance of traces of intense gas release, cooled it to room temperature and samples of synthesized titanium carbide are unloaded.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAU201306814U UA85619U (en) | 2013-05-31 | 2013-05-31 | Process for the preparation of titanium carbide using shs-process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UAU201306814U UA85619U (en) | 2013-05-31 | 2013-05-31 | Process for the preparation of titanium carbide using shs-process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA85619U true UA85619U (en) | 2013-11-25 |
Family
ID=52285136
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAU201306814U UA85619U (en) | 2013-05-31 | 2013-05-31 | Process for the preparation of titanium carbide using shs-process |
Country Status (1)
| Country | Link |
|---|---|
| UA (1) | UA85619U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110615682A (en) * | 2019-09-23 | 2019-12-27 | 西安建筑科技大学 | Graphite surface modification method for carbon-containing refractory castable and application thereof |
-
2013
- 2013-05-31 UA UAU201306814U patent/UA85619U/en unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110615682A (en) * | 2019-09-23 | 2019-12-27 | 西安建筑科技大学 | Graphite surface modification method for carbon-containing refractory castable and application thereof |
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