UA73196C2 - Reconstituted tobacco with reduced proteinous content and a method of obtaining thereof - Google Patents
Reconstituted tobacco with reduced proteinous content and a method of obtaining thereof Download PDFInfo
- Publication number
- UA73196C2 UA73196C2 UA2003021095A UA2003021095A UA73196C2 UA 73196 C2 UA73196 C2 UA 73196C2 UA 2003021095 A UA2003021095 A UA 2003021095A UA 2003021095 A UA2003021095 A UA 2003021095A UA 73196 C2 UA73196 C2 UA 73196C2
- Authority
- UA
- Ukraine
- Prior art keywords
- tobacco
- solution
- treated
- fibers
- fraction containing
- Prior art date
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 224
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 224
- 238000000034 method Methods 0.000 title claims abstract description 55
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 121
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 111
- 239000000463 material Substances 0.000 claims abstract description 55
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims abstract description 45
- 239000001632 sodium acetate Substances 0.000 claims abstract description 45
- 235000017281 sodium acetate Nutrition 0.000 claims abstract description 45
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 claims abstract description 9
- 239000000835 fiber Substances 0.000 claims description 72
- 239000000284 extract Substances 0.000 claims description 23
- 239000003125 aqueous solvent Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 11
- 238000005119 centrifugation Methods 0.000 claims description 9
- 238000012876 topography Methods 0.000 claims 1
- 238000000605 extraction Methods 0.000 abstract description 11
- 239000000203 mixture Substances 0.000 abstract description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 62
- 239000000243 solution Substances 0.000 description 59
- 229910052757 nitrogen Inorganic materials 0.000 description 31
- 210000003462 vein Anatomy 0.000 description 20
- 238000012545 processing Methods 0.000 description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 19
- 235000018102 proteins Nutrition 0.000 description 15
- 108090000623 proteins and genes Proteins 0.000 description 15
- 102000004169 proteins and genes Human genes 0.000 description 15
- 230000000391 smoking effect Effects 0.000 description 12
- 239000007788 liquid Substances 0.000 description 9
- 230000003247 decreasing effect Effects 0.000 description 8
- 238000007796 conventional method Methods 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- 210000000170 cell membrane Anatomy 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 5
- 235000019504 cigarettes Nutrition 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- 229910002651 NO3 Inorganic materials 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 230000002255 enzymatic effect Effects 0.000 description 4
- 239000002657 fibrous material Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 230000002745 absorbent Effects 0.000 description 3
- 239000002250 absorbent Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000813 microbial effect Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 102000009027 Albumins Human genes 0.000 description 2
- 108010088751 Albumins Proteins 0.000 description 2
- 102000006395 Globulins Human genes 0.000 description 2
- 108010044091 Globulins Proteins 0.000 description 2
- 108010064851 Plant Proteins Proteins 0.000 description 2
- 239000012670 alkaline solution Substances 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 239000006286 aqueous extract Substances 0.000 description 2
- 150000001491 aromatic compounds Chemical class 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- 235000021118 plant-derived protein Nutrition 0.000 description 2
- 108060006613 prolamin Proteins 0.000 description 2
- XXRYFVCIMARHRS-UHFFFAOYSA-N propan-2-yl n-dimethoxyphosphorylcarbamate Chemical compound COP(=O)(OC)NC(=O)OC(C)C XXRYFVCIMARHRS-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000007738 vacuum evaporation Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- MTXSIJUGVMTTMU-JTQLQIEISA-N (S)-anabasine Chemical compound N1CCCC[C@H]1C1=CC=CN=C1 MTXSIJUGVMTTMU-JTQLQIEISA-N 0.000 description 1
- MYKUKUCHPMASKF-VIFPVBQESA-N (S)-nornicotine Chemical compound C1CCN[C@@H]1C1=CC=CN=C1 MYKUKUCHPMASKF-VIFPVBQESA-N 0.000 description 1
- HZWWPUTXBJEENE-UHFFFAOYSA-N 5-amino-2-[[1-[5-amino-2-[[1-[2-amino-3-(4-hydroxyphenyl)propanoyl]pyrrolidine-2-carbonyl]amino]-5-oxopentanoyl]pyrrolidine-2-carbonyl]amino]-5-oxopentanoic acid Chemical compound C1CCC(C(=O)NC(CCC(N)=O)C(=O)N2C(CCC2)C(=O)NC(CCC(N)=O)C(O)=O)N1C(=O)C(N)CC1=CC=C(O)C=C1 HZWWPUTXBJEENE-UHFFFAOYSA-N 0.000 description 1
- SOPPBXUYQGUQHE-JTQLQIEISA-N Anatabine Chemical compound C1C=CCN[C@@H]1C1=CC=CN=C1 SOPPBXUYQGUQHE-JTQLQIEISA-N 0.000 description 1
- SOPPBXUYQGUQHE-UHFFFAOYSA-N Anatabine Natural products C1C=CCNC1C1=CC=CN=C1 SOPPBXUYQGUQHE-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- VEVZCONIUDBCDC-UHFFFAOYSA-N Flurprimidol Chemical compound C=1N=CN=CC=1C(O)(C(C)C)C1=CC=C(OC(F)(F)F)C=C1 VEVZCONIUDBCDC-UHFFFAOYSA-N 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- 108010061711 Gliadin Proteins 0.000 description 1
- 108010068370 Glutens Proteins 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 238000007696 Kjeldahl method Methods 0.000 description 1
- 241000286819 Malo Species 0.000 description 1
- MYKUKUCHPMASKF-UHFFFAOYSA-N Nornicotine Natural products C1CCNC1C1=CC=CN=C1 MYKUKUCHPMASKF-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000910 agglutinin Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 229930014345 anabasine Natural products 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 239000002956 ash Substances 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 210000001061 forehead Anatomy 0.000 description 1
- 238000009415 formwork Methods 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- 229910017464 nitrogen compound Inorganic materials 0.000 description 1
- 150000002830 nitrogen compounds Chemical class 0.000 description 1
- 150000004005 nitrosamines Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- SETMGIIITGNLAS-UHFFFAOYSA-N spizofurone Chemical compound O=C1C2=CC(C(=O)C)=CC=C2OC21CC2 SETMGIIITGNLAS-UHFFFAOYSA-N 0.000 description 1
- 229950001870 spizofurone Drugs 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/612,119 US6508254B1 (en) | 2000-07-07 | 2000-07-07 | Reduced protein reconstituted tobacco and method of making same |
| PCT/GB2001/002735 WO2002003817A2 (en) | 2000-07-07 | 2001-06-21 | A reduced protein reconstituted tobacco and method of making same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA73196C2 true UA73196C2 (en) | 2005-06-15 |
Family
ID=24451809
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA2003021095A UA73196C2 (en) | 2000-07-07 | 2001-06-21 | Reconstituted tobacco with reduced proteinous content and a method of obtaining thereof |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US6508254B1 (xx) |
| EP (1) | EP1301095A2 (xx) |
| JP (1) | JP3761519B2 (xx) |
| CN (1) | CN1230103C (xx) |
| AU (2) | AU2001274289B2 (xx) |
| MY (1) | MY122536A (xx) |
| NZ (1) | NZ523318A (xx) |
| RU (1) | RU2248737C2 (xx) |
| UA (1) | UA73196C2 (xx) |
| WO (1) | WO2002003817A2 (xx) |
| ZA (1) | ZA200300034B (xx) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW200531647A (en) * | 2003-12-22 | 2005-10-01 | Us Smokeless Tobacco Co | Conditioning process for tobacco and/or snuff compositions |
| US20050241657A1 (en) | 2004-04-29 | 2005-11-03 | Brown & Williamson Tabacco Corporation | Removal of nitrogen containing compounds from tobacco |
| US20050263161A1 (en) * | 2004-05-27 | 2005-12-01 | Brown & Williamson Tobacco Corporation | Tobacco filler of low nitrogen content |
| RU2336789C1 (ru) * | 2004-06-16 | 2008-10-27 | Джапан Тобакко Инк. | Способ получения восстановленного табачного материала |
| US7337782B2 (en) * | 2004-08-18 | 2008-03-04 | R.J. Reynolds Tobacco Company | Process to remove protein and other biomolecules from tobacco extract or slurry |
| US20110083684A1 (en) * | 2009-10-09 | 2011-04-14 | Philip Morris Usa Inc. | Methods for removing heavy metals from aqueous extracts of tobacco |
| EP2526787A1 (en) * | 2011-05-26 | 2012-11-28 | Philip Morris Products S.A. | Methods for reducing the formation of tobacco specific nitrosamines in tobacco homogenates |
| GB201108860D0 (en) * | 2011-05-26 | 2011-07-06 | British American Tobacco Co | Tobacco treatment |
| US9220296B2 (en) | 2013-03-15 | 2015-12-29 | Safall Fall | Method of reducing tobacco-specific nitrosamines |
| CN103734905B (zh) * | 2014-01-03 | 2016-03-30 | 广东中烟工业有限责任公司 | 一种去蛋白烟草提取物的制备方法及应用 |
| CN104489909B (zh) * | 2014-11-20 | 2016-02-03 | 湖北中烟工业有限责任公司 | 提高烟梗提取率的方法 |
| GB201508671D0 (en) * | 2015-05-20 | 2015-07-01 | British American Tobacco Co | Aerosol generating material and devices including the same |
| CN105768202B (zh) * | 2016-04-29 | 2017-06-23 | 华南理工大学 | 一种提取烟草废弃物中烟碱的方法 |
| JP7039562B2 (ja) * | 2016-08-17 | 2022-03-22 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | 新型たばこ基体を有するエアロゾル発生物品 |
| EP3643184A4 (en) * | 2017-08-02 | 2021-05-05 | Japan Tobacco, Inc. | METHOD FOR MANUFACTURING TOBACCO FLAVOR LIQUID AND TOBACCO FLAVOR LIQUID |
| US10897925B2 (en) | 2018-07-27 | 2021-01-26 | Joseph Pandolfino | Articles and formulations for smoking products and vaporizers |
| US20200035118A1 (en) | 2018-07-27 | 2020-01-30 | Joseph Pandolfino | Methods and products to facilitate smokers switching to a tobacco heating product or e-cigarettes |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB884435A (en) | 1958-11-20 | 1961-12-13 | C H Dexter & Sons Inc | Improvements in or relating to tobacco web material |
| US3145717A (en) * | 1959-10-22 | 1964-08-25 | C H Dexter & Sons Inc | Methods of making tobacco web material |
| CH450995A (de) | 1963-09-02 | 1968-05-15 | Tamag Basel Ag | Verfahren zur Herstellung von Tabakfolien |
| US3306307A (en) | 1964-04-17 | 1967-02-28 | American Mach & Foundry | Treatment of tobacco |
| US3860012A (en) * | 1973-05-21 | 1975-01-14 | Kimberly Clark Co | Method of producing a reconstituted tobacco product |
| US4183364A (en) | 1976-12-07 | 1980-01-15 | Gumushan Osman H | Tobacco refining process |
| US4256126A (en) | 1978-08-02 | 1981-03-17 | Philip Morris Incorporated | Smokable material and its method of preparation |
| US4289147A (en) | 1979-11-15 | 1981-09-15 | Leaf Proteins, Inc. | Process for obtaining deproteinized tobacco freed of nicotine and green pigment, for use as a smoking product |
| US4347859A (en) | 1980-12-09 | 1982-09-07 | Philip Morris Incorporated | Acid curing of tobacco |
| US4489739A (en) | 1982-05-24 | 1984-12-25 | Kimberly-Clark Corporation | Smokable tobacco composition and method of making |
| US4716911A (en) * | 1986-04-08 | 1988-01-05 | Genencor, Inc. | Method for protein removal from tobacco |
| US5435325A (en) * | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
| US4887618A (en) * | 1988-05-19 | 1989-12-19 | R. J. Reynolds Tobacco Company | Tobacco processing |
| US4941484A (en) * | 1989-05-30 | 1990-07-17 | R. J. Reynolds Tobacco Company | Tobacco processing |
| US4987906A (en) * | 1989-09-13 | 1991-01-29 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
| US5131414A (en) * | 1990-02-23 | 1992-07-21 | R. J. Reynolds Tobacco Company | Tobacco processing |
| US5148821A (en) | 1990-08-17 | 1992-09-22 | R. J. Reynolds Tobacco Company | Processes for producing a smokable and/or combustible tobacco material |
| US5343879A (en) * | 1991-06-21 | 1994-09-06 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
| US5311886A (en) | 1991-12-31 | 1994-05-17 | Imasco Limited | Tobacco extract treatment with insoluble adsorbent |
| US5322076A (en) | 1992-02-06 | 1994-06-21 | R. J. Reynolds Tobacco Company | Process for providing tobacco-containing papers for cigarettes |
| US5377698A (en) * | 1993-04-30 | 1995-01-03 | Brown & Williamson Tobacco Corporation | Reconstituted tobacco product |
-
2000
- 2000-07-07 US US09/612,119 patent/US6508254B1/en not_active Expired - Lifetime
-
2001
- 2001-06-21 AU AU2001274289A patent/AU2001274289B2/en not_active Ceased
- 2001-06-21 UA UA2003021095A patent/UA73196C2/uk unknown
- 2001-06-21 RU RU2003102619/12A patent/RU2248737C2/ru not_active IP Right Cessation
- 2001-06-21 AU AU7428901A patent/AU7428901A/xx active Pending
- 2001-06-21 CN CN01812476.3A patent/CN1230103C/zh not_active Expired - Fee Related
- 2001-06-21 EP EP01940790A patent/EP1301095A2/en not_active Withdrawn
- 2001-06-21 WO PCT/GB2001/002735 patent/WO2002003817A2/en active IP Right Grant
- 2001-06-21 NZ NZ523318A patent/NZ523318A/en unknown
- 2001-06-21 JP JP2002508281A patent/JP3761519B2/ja not_active Expired - Fee Related
- 2001-07-02 MY MYPI20013147A patent/MY122536A/en unknown
-
2003
- 2003-01-02 ZA ZA200300034A patent/ZA200300034B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP1301095A2 (en) | 2003-04-16 |
| JP2004502440A (ja) | 2004-01-29 |
| CN1440242A (zh) | 2003-09-03 |
| WO2002003817A3 (en) | 2002-05-30 |
| NZ523318A (en) | 2004-07-30 |
| AU7428901A (en) | 2002-01-21 |
| US6508254B1 (en) | 2003-01-21 |
| AU2001274289B2 (en) | 2004-08-05 |
| WO2002003817A2 (en) | 2002-01-17 |
| JP3761519B2 (ja) | 2006-03-29 |
| MY122536A (en) | 2006-04-29 |
| CN1230103C (zh) | 2005-12-07 |
| ZA200300034B (en) | 2003-11-07 |
| RU2248737C2 (ru) | 2005-03-27 |
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