TWI823620B - Stirring device with double rotors - Google Patents
Stirring device with double rotors Download PDFInfo
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- TWI823620B TWI823620B TW111139146A TW111139146A TWI823620B TW I823620 B TWI823620 B TW I823620B TW 111139146 A TW111139146 A TW 111139146A TW 111139146 A TW111139146 A TW 111139146A TW I823620 B TWI823620 B TW I823620B
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- rotor
- crucible
- stirring
- inner ring
- carrying barrel
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- 238000003756 stirring Methods 0.000 title claims abstract description 98
- 239000002002 slurry Substances 0.000 claims abstract description 19
- 238000004821 distillation Methods 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 18
- 238000005194 fractionation Methods 0.000 claims description 15
- 238000002360 preparation method Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000000265 homogenisation Methods 0.000 abstract description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 18
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 15
- 239000010426 asphalt Substances 0.000 description 15
- 229910052710 silicon Inorganic materials 0.000 description 14
- 239000010703 silicon Substances 0.000 description 14
- 239000011294 coal tar pitch Substances 0.000 description 13
- 239000011248 coating agent Substances 0.000 description 12
- 238000000576 coating method Methods 0.000 description 12
- 229910052799 carbon Inorganic materials 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 4
- 229910003481 amorphous carbon Inorganic materials 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 4
- 239000010439 graphite Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 239000007773 negative electrode material Substances 0.000 description 3
- 238000010008 shearing Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 230000002427 irreversible effect Effects 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000005543 nano-size silicon particle Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000011295 pitch Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000004904 shortening Methods 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 229910021383 artificial graphite Inorganic materials 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910001416 lithium ion Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910021382 natural graphite Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- -1 polypropylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000011863 silicon-based powder Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
- 238000001947 vapour-phase growth Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
Description
本發明係關於一種攪拌裝置,特別是一種雙轉子攪拌裝置。The invention relates to a stirring device, in particular to a double-rotor stirring device.
鋰電池與傳統電池相比有較多優勢,例如能量密度高、放電電壓高、重量輕等。目前鋰電池負極材料主要是採用石墨負極材料,又分為天然石墨和石油焦人造石墨,其中石墨作為負極材料,石墨粉末顆粒外部表面和內部的晶體結構差異較大,與電解液反應的不均勻性差別較大,在充電過程中,容易發生溶劑化鋰離子共嵌入,引起石墨層的膨脹和崩塌,由於消耗了更多的電解液,增加了不可逆容量,從而影響了循環壽命。Lithium batteries have many advantages over traditional batteries, such as high energy density, high discharge voltage, and light weight. At present, the negative electrode material of lithium batteries mainly uses graphite negative electrode material, which is divided into natural graphite and petroleum coke artificial graphite. Graphite is used as the negative electrode material. The external surface and internal crystal structure of the graphite powder particles are quite different, and the reaction with the electrolyte is uneven. There is a large difference in properties. During the charging process, co-intercalation of solvated lithium ions is prone to occur, causing expansion and collapse of the graphite layer. As more electrolyte is consumed, the irreversible capacity is increased, thus affecting the cycle life.
對此,為了克服上述的缺點,即在碳或石墨粉末表面上包覆無定形碳,無定形碳的前驅體有很多種,使用的包覆材料包括酚醛樹脂,聚丙烯等樹脂類材料,以及石油瀝青,煤焦瀝青等瀝青類材料,其中瀝青類材料的包覆,不但在表面包覆了一層無定形碳,還可顯著的降低石墨的比表面積,減少首次放電過程中的不可逆容量,提高首次放電效能。In this regard, in order to overcome the above shortcomings, amorphous carbon is coated on the surface of carbon or graphite powder. There are many kinds of precursors of amorphous carbon. The coating materials used include phenolic resin, polypropylene and other resin materials, and Petroleum asphalt, coal tar pitch and other asphalt materials, among which the coating of asphalt materials not only coats the surface with a layer of amorphous carbon, but can also significantly reduce the specific surface area of graphite, reduce the irreversible capacity during the first discharge process, and improve First discharge performance.
然而,目前將瀝青包覆碳或石墨粉末的方法,例如固相包覆,是利用瀝青粉末與碳或石墨粉末混合,在常溫或加熱條件下進行攪拌完成包覆,但是難以確保混合均勻性和瀝青粉包覆的完整性,因此生產質量不穩定。氣相包覆是利用烷、烴類氣體在高溫下分解碳而沉積在碳或石墨粉末表面,但是氣相沉積的條件比較苛刻,生產成本高昂。液相混合包覆是將加熱熔化瀝青在150〜300°C與碳或石墨粉末進行混捏包覆,但包覆效果不好,其中熔融瀝青在混捏過程中難以做到均勻分散,因而無法達到均勻包覆碳或石墨粉末顆粒表面的目的。另外,將瀝青與有機混合,浸潤後蒸發溶劑,然後炭化石墨化,其包覆效果也不好,原因在於瀝青中各組分性質差異較大,難以在某一種特定溶劑裡較好的溶解和分散,即使在強力攪拌下也無法達到理想的浸潤和包覆效果,如果在瀝青溶解度不夠的情況下加大瀝青用量又會導致炭化後無定形炭含量過高造成材料容量偏低的情況。However, the current method of coating carbon or graphite powder with pitch, such as solid phase coating, is to mix pitch powder with carbon or graphite powder and stir under normal temperature or heating conditions to complete the coating. However, it is difficult to ensure uniformity and uniformity of mixing. The integrity of the asphalt powder coating is unstable, so the production quality is unstable. Vapor phase coating uses alkanes and hydrocarbon gases to decompose carbon at high temperatures and deposit it on the surface of carbon or graphite powder. However, the conditions for vapor phase deposition are relatively harsh and the production cost is high. Liquid phase mixing coating is to knead and coat heated molten asphalt with carbon or graphite powder at 150~300°C, but the coating effect is not good. The molten asphalt is difficult to disperse evenly during the kneading process, so uniformity cannot be achieved. The purpose of coating the surface of carbon or graphite powder particles. In addition, when asphalt is mixed with organic matter, the solvent is evaporated after infiltration, and then carbonized and graphitized, the coating effect is not good. The reason is that the properties of the various components in the asphalt are quite different, making it difficult to dissolve and dissolve well in a specific solvent. Dispersion, even under strong stirring, cannot achieve the ideal wetting and coating effects. If the asphalt solubility is insufficient and the amount of asphalt is increased, the amorphous carbon content after carbonization will be too high, resulting in low material capacity.
因此,為克服現有技術中的缺點和不足,本發明有必要提供改良的一種雙轉子攪拌裝置,以解決上述習用技術所存在的問題。Therefore, in order to overcome the shortcomings and deficiencies in the prior art, it is necessary for the present invention to provide an improved dual-rotor stirring device to solve the problems existing in the above conventional technology.
本發明之主要目的在於提供一種雙轉子攪拌裝置,利用內圈轉子以及外圈轉子反向旋轉的設計,提高漿料均質化的攪拌效率。The main purpose of the present invention is to provide a dual-rotor mixing device that utilizes the design of the inner rotor and the outer rotor to rotate in opposite directions to improve the mixing efficiency of slurry homogenization.
為達上述之目的,本發明提供一種雙轉子攪拌裝置,該雙轉子攪拌裝置包括一機台以及一攪拌單元;該機台包含一座體、一固定板以及一底板,該固定板以及該底板設置在該座體上,而且該座體具有一預備區、一攪拌區以及一蒸餾區,其中該攪拌區位於該預備區及該蒸餾區之間;該攪拌單元設置在該機台上,而且該攪拌單元包含一第一軌道、一第一坩鍋承載桶、一第一升降組件、一第一緊固夾頭、一內圈轉子、一內圈馬達、一外圈轉子及一外圈馬達,該第一軌道設置在該底板上而且自該攪拌區延伸至該預備區;該第一坩鍋承載桶用以承載一坩鍋而且配置為在該第一軌道上移動,該第一升降組件設置在該固定板及該底板之間,該第一升降組件位於該攪拌區而且配置為帶動該第一坩鍋承載桶上升或下降,該第一緊固夾頭設置在該固定板,該第一緊固夾頭位於該第一坩鍋承載桶上方而且配置為用於覆蓋該第一坩鍋承載桶以及密閉該坩鍋,該內圈轉子穿過該第一緊固夾頭而且伸入該坩鍋中,該內圈馬達設置在該固定板,該內圈馬達位於該攪拌區而且配置為驅動該內圈轉子轉動,該外圈轉子設置在該內圈轉子的外圍,該外圈馬達設置在該固定板,該外圈馬達位於該攪拌區而且配置為驅動該外圈轉子轉動,其中該內圈轉子與該外圈轉子配置為攪拌該坩鍋中的一漿料,而且該內圈轉子與該外圈轉子的轉動方向相反。In order to achieve the above purpose, the present invention provides a dual-rotor stirring device. The dual-rotor stirring device includes a machine platform and a mixing unit; the machine platform includes a base body, a fixed plate and a bottom plate. The fixed plate and the bottom plate are provided On the base body, the base body has a preparation area, a stirring area and a distillation area, wherein the stirring area is located between the preparation area and the distillation area; the stirring unit is arranged on the machine platform, and the The stirring unit includes a first track, a first crucible carrying barrel, a first lifting component, a first fastening chuck, an inner ring rotor, an inner ring motor, an outer ring rotor and an outer ring motor. The first track is provided on the bottom plate and extends from the stirring area to the preparation area; the first crucible carrying barrel is used to carry a crucible and is configured to move on the first track, and the first lifting component is configured Between the fixed plate and the bottom plate, the first lifting component is located in the stirring area and is configured to drive the first crucible carrying barrel to rise or fall, the first fastening chuck is provided on the fixed plate, and the first The fastening chuck is located above the first crucible carrying barrel and is configured to cover the first crucible carrying barrel and seal the crucible. The inner ring rotor passes through the first fastening chuck and extends into the crucible. In the pot, the inner ring motor is disposed on the fixed plate, the inner ring motor is located in the stirring area and is configured to drive the inner ring rotor to rotate, the outer ring rotor is disposed on the periphery of the inner ring rotor, and the outer ring motor is disposed on The fixed plate, the outer ring motor is located in the stirring area and is configured to drive the outer ring rotor to rotate, wherein the inner ring rotor and the outer ring rotor are configured to stir a slurry in the crucible, and the inner ring rotor and The outer rotor rotates in the opposite direction.
在本發明之一實施例中,該第一升降組件具有一第一升降桿以及一第一氣壓缸,該第一氣壓缸配置為驅動該第一升降桿伸縮而帶動該第一坩鍋承載桶上升或下降。In one embodiment of the present invention, the first lifting assembly has a first lifting rod and a first pneumatic cylinder. The first pneumatic cylinder is configured to drive the first lifting rod to expand and contract to drive the first crucible carrying barrel. rise or fall.
在本發明之一實施例中,該攪拌單元另包含一第一迴旋缸以及一第一旋轉支撐架,該第一旋轉支撐架設置在該第一坩鍋承載桶的頂部,該第一迴旋缸設置在該第一升降桿的底部而且配置為轉動該第一旋轉支撐架,使得該第一坩鍋承載桶沿著該第一軌道自該攪拌區移動至該預備區。In one embodiment of the present invention, the stirring unit further includes a first rotating cylinder and a first rotating support frame. The first rotating supporting frame is disposed on the top of the first crucible carrying barrel. The first rotating cylinder It is provided at the bottom of the first lifting rod and is configured to rotate the first rotating support frame so that the first crucible carrying barrel moves from the stirring area to the preparation area along the first track.
在本發明之一實施例中,該第一軌道的路徑呈半圓形。In one embodiment of the invention, the path of the first track is semicircular.
在本發明之一實施例中,該雙轉子攪拌裝置另包括設置在該機台上的一分餾單元,該分餾單元包含一第二軌道、一第二坩鍋承載桶、一第二升降組件及一第二緊固夾頭,該第二軌道設置在該底板上而且自該蒸餾區延伸至該攪拌區,該第二坩鍋承載桶用以承載該坩鍋並對該坩鍋進行加熱分餾,而且該第二坩鍋承載桶配置為在該第二軌道上移動,該第二升降組件設置在該固定板及該底板之間,該第二升降組件位於該蒸餾區而且配置為帶動該第二坩鍋承載桶上升或下降,該第二緊固夾頭設置在該固定板,該第二緊固夾頭位於該第二坩鍋承載桶上方而且配置為用於覆蓋該第二坩鍋承載桶以及密閉該坩鍋。In one embodiment of the present invention, the dual-rotor stirring device further includes a fractionation unit disposed on the machine platform. The fractionation unit includes a second track, a second crucible carrying barrel, a second lifting assembly and a second fastening chuck, the second track is provided on the bottom plate and extends from the distillation zone to the stirring zone, the second crucible carrying barrel is used to carry the crucible and perform heating and fractionation of the crucible, Moreover, the second crucible carrying barrel is configured to move on the second track, the second lifting component is disposed between the fixed plate and the bottom plate, the second lifting component is located in the distillation area and is configured to drive the second The crucible carrying barrel rises or falls, the second fastening chuck is provided on the fixed plate, the second fastening chuck is located above the second crucible carrying barrel and is configured to cover the second crucible carrying barrel and sealing the crucible.
在本發明之一實施例中,該第二升降組件具有一第二升降桿以及一第二氣壓缸,該第二氣壓缸配置為驅動該第二升降桿伸縮而帶動該第二坩鍋承載桶上升或下降。In one embodiment of the present invention, the second lifting assembly has a second lifting rod and a second pneumatic cylinder. The second pneumatic cylinder is configured to drive the second lifting rod to expand and contract to drive the second crucible carrying barrel. rise or fall.
在本發明之一實施例中,該分餾單元另包含一第二迴旋缸以及一第二旋轉支撐架,該第二旋轉支撐架設置在該第二坩鍋承載桶的頂部,該第二迴旋缸設置在該第二升降桿的底部而且配置為轉動該第二旋轉支撐架,使得該第二坩鍋承載桶沿著該第二軌道自該蒸餾區移動至該攪拌區。In one embodiment of the present invention, the fractionation unit further includes a second rotating cylinder and a second rotating support frame. The second rotating supporting frame is disposed on the top of the second crucible carrying barrel. The second rotating cylinder It is provided at the bottom of the second lifting rod and is configured to rotate the second rotating support frame so that the second crucible carrying barrel moves from the distillation zone to the stirring zone along the second track.
在本發明之一實施例中,該第二軌道的路徑呈半圓形。In one embodiment of the invention, the path of the second track is semicircular.
在本發明之一實施例中,該內圈轉子具有一內圈傳動皮帶、一內圈轉軸以及一攪拌片,該內圈傳動皮帶配置為受到該內圈馬達的驅動而帶動該內圈轉軸旋轉,該攪拌片設置在該內圈轉軸的一端。In one embodiment of the present invention, the inner ring rotor has an inner ring driving belt, an inner ring rotating shaft and a stirring blade. The inner ring driving belt is configured to be driven by the inner ring motor to drive the inner ring rotating shaft to rotate. , the stirring blade is arranged at one end of the inner ring rotating shaft.
在本發明之一實施例中,該外圈轉子具有一外圈傳動皮帶、一外圈轉軸以及一攪拌格柵,該外圈傳動皮帶配置為受到該外圈馬達的驅動而帶動該外圈轉軸旋轉,該攪拌格柵設置在該外圈轉軸的一端。In one embodiment of the present invention, the outer ring rotor has an outer ring driving belt, an outer ring rotating shaft and a stirring grid. The outer ring driving belt is configured to be driven by the outer ring motor to drive the outer ring rotating shaft. Rotate, and the stirring grid is arranged at one end of the outer ring rotating shaft.
如上所述,本發明雙轉子攪拌裝置透過該內圈轉子以及該外圈轉子反向旋轉的設計,兩者維持相對轉速及剪切作用的情況下,帶動高黏度煤焦瀝青形成交錯流場,並提供大範圍的矽漿料擾動與混合,使得高黏度瀝青及奈米矽團簇能夠被均質化,同時減少設備空間,縮短均質化製程的所需時間,提高漿料均質化的攪拌效率。As mentioned above, the dual-rotor mixing device of the present invention drives the high-viscosity coal tar pitch to form a staggered flow field through the counter-rotating design of the inner rotor and the outer rotor. When the two maintain relative rotation speed and shearing effect, It also provides a wide range of silicon slurry disturbance and mixing, allowing high-viscosity asphalt and nano-silica clusters to be homogenized, while reducing equipment space, shortening the time required for the homogenization process, and improving the mixing efficiency of slurry homogenization.
為了讓本發明之上述及其他目的、特徵、優點能更明顯易懂,下文將特舉本發明實施例,並配合所附圖式,作詳細說明如下。再者,本發明所提到的方向用語,例如上、下、頂、底、前、後、左、右、內、外、側面、周圍、中央、水平、橫向、垂直、縱向、軸向、徑向、最上層或最下層等,僅是參考附加圖式的方向。因此,使用的方向用語是用以說明及理解本發明,而非用以限制本發明。In order to make the above and other objects, features, and advantages of the present invention more apparent and understandable, embodiments of the present invention will be described in detail below along with the accompanying drawings. Furthermore, the directional terms mentioned in the present invention include, for example, up, down, top, bottom, front, back, left, right, inside, outside, side, peripheral, central, horizontal, transverse, vertical, longitudinal, axial, Radial, uppermost or lowermost, etc., are only directions with reference to the attached drawings. Therefore, the directional terms used are to illustrate and understand the present invention, but not to limit the present invention.
請參照圖1及圖2所示,為本發明實施例的一種雙轉子攪拌裝置,為一種自動化設備,其功能為產製奈米級矽及煤焦瀝青混合物,可對矽漿料(例如混合奈米級矽粉及甲基萘油)與煤焦瀝青進行均質化,其中該雙轉子攪拌裝置包括一機台2、一攪拌單元3以及一分餾單元4。本發明將於下文詳細說明各元件的細部構造、組裝關係及其運作原理。Please refer to FIG. 1 and FIG. 2 , which is a dual-rotor mixing device according to an embodiment of the present invention. It is an automated equipment whose function is to produce a mixture of nanoscale silicon and coal tar pitch, which can mix silicon slurry (such as mixing Nanoscale silicon powder and methylnaphthalene oil) and coal tar pitch are homogenized, wherein the dual-rotor mixing device includes a machine 2, a mixing unit 3 and a fractionation unit 4. The detailed structure, assembly relationship and operating principle of each component will be described in detail below.
續參照圖1及圖2所示,該機台2包含一座體21、一固定板22以及一底板23,該固定板22以及該底板23設置在該座體21上,而且該座體21具有一預備區A1、一攪拌區A2以及一蒸餾區A3,其中該攪拌區A2位於該預備區A1及該蒸餾區A3之間。Continuing to refer to Figures 1 and 2, the machine 2 includes a base 21, a fixed plate 22 and a bottom plate 23. The fixed plate 22 and the bottom plate 23 are arranged on the base 21, and the base 21 has A preparation zone A1, a stirring zone A2 and a distillation zone A3, wherein the stirring zone A2 is located between the preparation zone A1 and the distillation zone A3.
續參照圖1及圖2所示,該攪拌單元3設置在該機台2上,而且該攪拌單元3包含一第一軌道31、一第一坩鍋承載桶32、一第一升降組件33、一第一緊固夾頭34、一內圈轉子35、一內圈馬達36、一外圈轉子37及一外圈馬達38。該第一軌道31設置在該底板23上而且該第一軌道31自該攪拌區A2延伸至該預備區A1。Continuing to refer to Figures 1 and 2, the stirring unit 3 is disposed on the machine platform 2, and the stirring unit 3 includes a first track 31, a first crucible carrying barrel 32, a first lifting component 33, A first fastening chuck 34 , an inner ring rotor 35 , an inner ring motor 36 , an outer ring rotor 37 and an outer ring motor 38 . The first track 31 is disposed on the bottom plate 23 and extends from the stirring area A2 to the preparation area A1.
配合圖3及圖4所示,該第一坩鍋承載桶32用以承載一坩鍋101(見圖4),而且該第一坩鍋承載桶32配置為在該第一軌道31上移動。該第一升降組件33設置在該固定板22及該底板23之間,該第一升降組件33位於該攪拌區A2而且該第一升降組件33配置為帶動該第一坩鍋承載桶32上升或下降。該第一緊固夾頭34設置在該固定板22,而且該第一緊固夾頭34透過一第一夾頭氣壓缸341來緊固或鬆開,該第一緊固夾頭34位於該第一坩鍋承載桶32上方而且該第一緊固夾頭34配置為用於覆蓋該第一坩鍋承載桶32以及密閉該坩鍋101。在本實施例中,該內圈馬達36以及該外圈馬達38為減速馬達。As shown in FIGS. 3 and 4 , the first crucible carrying barrel 32 is used to carry a crucible 101 (see FIG. 4 ), and the first crucible carrying barrel 32 is configured to move on the first track 31 . The first lifting component 33 is disposed between the fixed plate 22 and the bottom plate 23. The first lifting component 33 is located in the stirring area A2 and the first lifting component 33 is configured to drive the first crucible carrying barrel 32 to rise or decline. The first fastening chuck 34 is disposed on the fixed plate 22, and the first fastening chuck 34 is tightened or loosened through a first chuck pneumatic cylinder 341. The first fastening chuck 34 is located on the The first fastening chuck 34 is above the first crucible carrying barrel 32 and is configured to cover the first crucible carrying barrel 32 and seal the crucible 101 . In this embodiment, the inner ring motor 36 and the outer ring motor 38 are reduction motors.
續參照圖1、圖2及圖5所示,該內圈轉子35穿過該第一緊固夾頭34而且伸入該坩鍋101中。該內圈馬達36設置在該固定板22,該內圈馬達36位於該攪拌區A2而且該內圈馬達36配置為驅動該內圈轉子35轉動。該外圈轉子37設置在該內圈轉子35的外圍。該外圈馬達38設置在該固定板22,該外圈馬達38位於該攪拌區A2而且該外圈馬達38配置為驅動該外圈轉子37轉動。Continuing to refer to FIG. 1 , FIG. 2 and FIG. 5 , the inner ring rotor 35 passes through the first fastening chuck 34 and extends into the crucible 101 . The inner ring motor 36 is disposed on the fixed plate 22, the inner ring motor 36 is located in the stirring area A2, and the inner ring motor 36 is configured to drive the inner ring rotor 35 to rotate. The outer ring rotor 37 is arranged on the periphery of the inner ring rotor 35 . The outer ring motor 38 is disposed on the fixed plate 22, the outer ring motor 38 is located in the stirring area A2, and the outer ring motor 38 is configured to drive the outer ring rotor 37 to rotate.
請參照圖1、圖2所示,該第一升降組件33具有一第一升降桿331以及一第一氣壓缸332,該第一氣壓缸332配置為驅動該第一升降桿331伸縮而帶動該第一坩鍋承載桶32上升或下降。Referring to Figures 1 and 2, the first lifting assembly 33 has a first lifting rod 331 and a first pneumatic cylinder 332. The first pneumatic cylinder 332 is configured to drive the first lifting rod 331 to expand and contract to drive the first lifting rod 331. The first crucible carrying barrel 32 rises or falls.
續參照圖1及圖2所示,該攪拌單元3另包含一第一迴旋缸301以及一第一旋轉支撐架302,該第一旋轉支撐架302設置在該第一坩鍋承載桶32的頂部,該第一迴旋缸301設置在該第一升降桿331的底部而且該第一迴旋缸301配置為轉動該第一旋轉支撐架302,使得該第一坩鍋承載桶32沿著該第一軌道31自該攪拌區A2移動至該預備區A1。在本實施例中,該第一軌道31的路徑呈半圓形。Continuing to refer to Figures 1 and 2, the stirring unit 3 further includes a first rotating cylinder 301 and a first rotating support frame 302. The first rotating support frame 302 is disposed on the top of the first crucible carrying barrel 32. , the first rotating cylinder 301 is disposed at the bottom of the first lifting rod 331 and the first rotating cylinder 301 is configured to rotate the first rotating support frame 302 so that the first crucible carrying barrel 32 moves along the first track 31 moves from the stirring zone A2 to the preparation zone A1. In this embodiment, the path of the first track 31 is semicircular.
續參照圖1、圖2及圖5所示,該內圈轉子35具有一內圈傳動皮帶351、一內圈轉軸352以及一攪拌片353,該內圈傳動皮帶351配置為受到該內圈馬達36的驅動而帶動該內圈轉軸352旋轉,該攪拌片353設置在該內圈轉軸352的一端。該外圈轉子37具有一外圈傳動皮帶371、一外圈轉軸372以及一攪拌格柵373,該外圈傳動皮帶371配置為受到該外圈馬達38的驅動而帶動該外圈轉軸372旋轉,該攪拌格柵373設置在該外圈轉軸372的一端。在本實施例中,該內圈轉子35以及該外圈轉子37配置為攪拌該坩鍋101中的一漿料,而且該內圈轉子35與該外圈轉子37的轉動方向相反,例如,該內圈轉子35為順向轉動,該外圈轉子37為逆向轉動。Continuing to refer to Figures 1, 2 and 5, the inner ring rotor 35 has an inner ring drive belt 351, an inner ring rotating shaft 352 and an agitating blade 353. The inner ring drive belt 351 is configured to be driven by the inner ring motor. 36 is driven to drive the inner ring rotating shaft 352 to rotate, and the stirring blade 353 is provided at one end of the inner ring rotating shaft 352. The outer ring rotor 37 has an outer ring driving belt 371, an outer ring rotating shaft 372 and a stirring grid 373. The outer ring driving belt 371 is configured to be driven by the outer ring motor 38 to drive the outer ring rotating shaft 372 to rotate. The stirring grid 373 is provided at one end of the outer ring rotating shaft 372 . In this embodiment, the inner rotor 35 and the outer rotor 37 are configured to stir a slurry in the crucible 101, and the inner rotor 35 and the outer rotor 37 rotate in opposite directions, for example, the The inner rotor 35 rotates in the forward direction, and the outer rotor 37 rotates in the reverse direction.
續參照圖1及圖2所示,該分餾單元4設置在該機台2上,而且該分餾單元4配置為用以將甲基萘油溶劑蒸餾及回收,該分餾單元4包含一第二軌道41、一第二坩鍋承載桶42、一第二升降組件43及一第二緊固夾頭44,該第二軌道41設置在該底板23上而且該第二軌道41自該蒸餾區A3延伸至該攪拌區A2。該第二坩鍋承載桶42用以承載該坩鍋101並對該坩鍋101進行加熱分餾,而且該第二坩鍋承載桶42配置為在該第二軌道41上移動。該第二升降組件43設置在該固定板22及該底板23之間,該第二升降組件43位於該蒸餾區A3而且該第二升降組件43配置為帶動該第二坩鍋承載桶42上升或下降。該第二緊固夾頭44設置在該固定板22,而且該第二緊固夾頭44透過一第二夾頭氣壓缸441來緊固或鬆開,該第二緊固夾頭44位於該第二坩鍋承載桶42上方而且該第二緊固夾頭44配置為用於覆蓋該第二坩鍋承載桶42以及密閉該坩鍋101。Continuing to refer to Figures 1 and 2, the fractionation unit 4 is disposed on the machine 2, and the fractionation unit 4 is configured to distill and recover the methylnaphthalene oil solvent. The fractionation unit 4 includes a second track 41. A second crucible carrying barrel 42, a second lifting assembly 43 and a second fastening clamp 44. The second rail 41 is provided on the bottom plate 23 and extends from the distillation area A3. to the stirring zone A2. The second crucible carrying barrel 42 is used to carry the crucible 101 and conduct heating and fractionation of the crucible 101 , and the second crucible carrying barrel 42 is configured to move on the second track 41 . The second lifting component 43 is disposed between the fixed plate 22 and the bottom plate 23. The second lifting component 43 is located in the distillation area A3 and is configured to drive the second crucible carrying barrel 42 to rise or decline. The second fastening chuck 44 is disposed on the fixed plate 22, and the second fastening chuck 44 is tightened or loosened through a second chuck pneumatic cylinder 441. The second fastening chuck 44 is located on the The second fastening chuck 44 is above the second crucible carrying barrel 42 and is configured to cover the second crucible carrying barrel 42 and seal the crucible 101 .
續參照圖1及圖2所示,該第二升降組件43具有一第二升降桿431以及一第二氣壓缸432,該第二氣壓缸432配置為驅動該第二升降桿431伸縮而帶動該第二坩鍋承載桶42上升或下降。Continuing to refer to Figures 1 and 2, the second lifting assembly 43 has a second lifting rod 431 and a second pneumatic cylinder 432. The second pneumatic cylinder 432 is configured to drive the second lifting rod 431 to expand and contract to drive the second lifting rod 431. The second crucible carrying barrel 42 rises or falls.
續參照圖1及圖2所示,該分餾單元4另包含一第二迴旋缸401以及一第二旋轉支撐架402,該第二旋轉支撐架402設置在該第二坩鍋承載桶42的頂部,該第二迴旋缸401設置在該第二升降桿431的底部而且該第二迴旋缸401配置為轉動該第二旋轉支撐架402,使得該第二坩鍋承載桶42沿著該第二軌道41自該蒸餾區A3移動至該攪拌區A2。在本實施例中,該第二軌道41的路徑呈半圓形。Continuing to refer to Figures 1 and 2, the fractionation unit 4 further includes a second rotating cylinder 401 and a second rotating support frame 402. The second rotating support frame 402 is disposed on the top of the second crucible carrying barrel 42. , the second rotating cylinder 401 is disposed at the bottom of the second lifting rod 431 and the second rotating cylinder 401 is configured to rotate the second rotating support frame 402 so that the second crucible carrying barrel 42 moves along the second track 41 moves from the distillation zone A3 to the stirring zone A2. In this embodiment, the path of the second track 41 is semicircular.
依據上述的結構,當矽漿料與煤焦瀝青投入該坩鍋101之後,將該坩鍋101,放置在位於該預備區A1的第一坩鍋承載桶32,將該第一坩鍋承載桶32沿著該第一軌道31移動至該攪拌區A2(見圖1),再利用該第一升降組件33將該第一坩鍋承載桶32抬升而能夠被上方的該第一緊固夾頭34覆蓋鎖緊而形成封閉空間,接著以流洗程序自動抽氣與進氣,其中該坩鍋101內的空氣經抽離再以氨氣填充,並且以氨氣填充至微正壓,再透過保壓測試程序偵測該坩鍋101是否能夠維持微正壓。According to the above structure, after the silicon slurry and coal tar pitch are put into the crucible 101, the crucible 101 is placed in the first crucible carrying barrel 32 located in the preparation area A1, and the first crucible carrying barrel is placed 32 moves along the first track 31 to the stirring area A2 (see Figure 1), and then uses the first lifting assembly 33 to lift the first crucible carrying barrel 32 so that it can be lifted by the first fastening chuck above. 34 is covered and locked to form a closed space, and then the air is automatically pumped and aired in through a flow washing process. The air in the crucible 101 is extracted and then filled with ammonia gas, and filled with ammonia gas to a slightly positive pressure, and then through The pressure holding test program detects whether the crucible 101 can maintain a slight positive pressure.
當該坩鍋101中的矽漿料及煤焦瀝青要進行均質攪拌程序時,啟動該外圈馬達38,透過該外圈傳動皮帶371及該外圈轉軸372而帶動該攪拌格柵373轉動,其中該攪拌格柵373可依照適當轉速來攪拌矽漿料及煤焦瀝青,同時加熱使煤焦瀝青軟化,接著啟動該內圈馬達36,透過該內圈傳動皮帶351及該內圈轉軸352帶動該攪拌片353轉動,以攪拌矽漿料及煤焦瀝青而使其均質。攪拌過程中,該攪拌片353轉動可帶動矽漿料由軸向進入,再由離心方向脫離,矽漿料脫離時的離心向量與該攪拌片353轉動的垂直向量形成剪切作用,同時該內圈轉軸352在內,該外圈轉軸372在外,兩者反向旋轉,其中反向旋轉的攪拌格柵373具備攪拌矽漿料及煤焦瀝青的擾動及混合效果,而且具有收斂矽漿料離心向量的功能,使得瀝青能夠有效侵潤至奈米矽團簇間隙內,而且奈米矽團簇也能夠有效分散於瀝青中,進而使得矽漿料及煤焦瀝青能夠被均質化。When the silicon slurry and coal tar pitch in the crucible 101 are to be homogenized and stirred, the outer ring motor 38 is started to drive the stirring grid 373 to rotate through the outer ring drive belt 371 and the outer ring rotating shaft 372. The stirring grid 373 can stir the silicon slurry and coal tar pitch according to the appropriate rotation speed, and at the same time, heat the coal tar pitch to soften the coal tar pitch, and then start the inner ring motor 36 and drive it through the inner ring transmission belt 351 and the inner ring rotating shaft 352 The stirring blade 353 rotates to stir the silicon slurry and coal tar pitch to make them homogeneous. During the stirring process, the rotation of the stirring blade 353 can drive the silicon slurry to enter from the axial direction and then escape from the centrifugal direction. The centrifugal vector when the silicon slurry is separated and the vertical vector of the rotation of the stirring blade 353 form a shearing effect. At the same time, the inner The ring rotating shaft 352 is inside, and the outer ring rotating shaft 372 is outside, and they rotate in opposite directions. The counter-rotating stirring grid 373 has the disturbing and mixing effect of stirring the silicon slurry and coal tar pitch, and has the function of converging the centrifugal force of the silicon slurry. The function of vector enables the asphalt to effectively penetrate into the gaps of the nano-silicon clusters, and the nano-silicon clusters can also be effectively dispersed in the asphalt, thus allowing the silicon slurry and coal tar pitch to be homogenized.
當奈米級矽及瀝青的均質包焦反應作業結束之後,該坩鍋101仍然鎖緊在該第一緊固夾頭34上,先將該第一坩鍋承載桶32脫離該坩鍋101,再透過該第一升降組件33將該第一坩鍋承載桶32下降至該底板23,接著透過該第一迴旋缸301轉動該第一旋轉支撐架302,進而帶動該第一坩鍋承載桶32沿著該第一軌道31自該攪拌區A2移動至該預備區A1。After the homogeneous coking reaction operation of nanoscale silicon and asphalt is completed, the crucible 101 is still locked on the first fastening chuck 34, and the first crucible carrying barrel 32 is first separated from the crucible 101, Then the first crucible carrying barrel 32 is lowered to the bottom plate 23 through the first lifting assembly 33, and then the first rotating support frame 302 is rotated through the first rotating cylinder 301, thereby driving the first crucible carrying barrel 32 Move along the first track 31 from the stirring area A2 to the preparation area A1.
此時位於該蒸餾區A3的第二坩鍋承載桶42,透過該第一迴旋缸301轉動該第一旋轉支撐架302,進而帶動該第二坩鍋承載桶42沿著該第二軌道41自該蒸餾區A3移動至該攪拌區A2,再透過該第二升降組件43將該第二坩鍋承載桶42上升,使得該坩鍋101落入該第二坩鍋承載桶42中,此時將該坩鍋101自該第一緊固夾頭34鬆開,再透過該第二升降組件43下降該第二坩鍋承載桶42,並且將該第二坩鍋承載桶42沿著該第二軌道41自該攪拌區A2移動至該蒸餾區A3(見圖2),接著利用該第二升降組件43上升該第二坩鍋承載桶42,並且以該第二緊固夾頭44鎖緊該坩鍋101(見圖4),以進行溶劑蒸餾及回收作業。當溶劑去除之後,該坩鍋101自該第二緊固夾頭44鬆開,透過該第二升降組件43下降該第二坩鍋承載桶42,最後,由人員自位於該機台2一側的出料門102取出該坩鍋101。At this time, the second crucible carrying barrel 42 located in the distillation area A3 rotates the first rotating support frame 302 through the first rotating cylinder 301, thereby driving the second crucible carrying barrel 42 to move along the second track 41. The distillation zone A3 moves to the stirring zone A2, and then the second crucible carrying barrel 42 is raised through the second lifting assembly 43, so that the crucible 101 falls into the second crucible carrying barrel 42. At this time, The crucible 101 is loosened from the first fastening chuck 34, and then the second crucible carrying barrel 42 is lowered through the second lifting assembly 43, and the second crucible carrying barrel 42 is moved along the second track. 41 moves from the stirring area A2 to the distillation area A3 (see Figure 2), then uses the second lifting assembly 43 to lift the second crucible carrying barrel 42, and locks the crucible with the second fastening chuck 44 Pot 101 (see Figure 4) for solvent distillation and recovery operations. After the solvent is removed, the crucible 101 is loosened from the second fastening chuck 44, and the second crucible carrying barrel 42 is lowered through the second lifting assembly 43. Finally, a person is lifted from the side of the machine 2 The discharging door 102 takes out the crucible 101.
如上所述,本發明雙轉子攪拌裝置透過該內圈轉子35以及該外圈轉子37反向旋轉的設計,兩者維持相對轉速及剪切作用的情況下,帶動高黏度煤焦瀝青形成交錯流場,並提供大範圍的矽漿料擾動與混合,使得高黏度瀝青及奈米矽團簇能夠被均質化,同時減少設備空間,縮短均質化製程的所需時間,提高漿料均質化的攪拌效率。As mentioned above, the double-rotor mixing device of the present invention uses the design of the inner rotor 35 and the outer rotor 37 to rotate in opposite directions. When the two maintain relative rotation speed and shearing effect, the high-viscosity coal tar pitch is driven to form a cross flow. field, and provides a wide range of silicon slurry disturbance and mixing, allowing high-viscosity asphalt and nano-silica clusters to be homogenized, while reducing equipment space, shortening the time required for the homogenization process, and improving the mixing of the slurry homogenization efficiency.
雖然本發明已以實施例揭露,然其並非用以限制本發明,任何熟習此項技藝之人士,在不脫離本發明之精神和範圍內,當可作各種更動與修飾,因此本發明之保護範圍當視後附之申請專利範圍所界定者為準。Although the present invention has been disclosed through embodiments, they are not intended to limit the present invention. Any person skilled in the art can make various changes and modifications without departing from the spirit and scope of the present invention. Therefore, the protection of the present invention is The scope shall be determined by the appended patent application scope.
101:坩鍋 102:出料門 2:機台 21:座體 22:固定板 23:底板 3:攪拌單元 31:第一軌道 32:第一坩鍋承載桶 33:第一升降組件 331:第一升降桿 332:第一氣壓缸 34:第一緊固夾頭 341:第一夾頭氣壓缸 35:內圈轉子 351:內圈傳動皮帶 352:內圈轉軸 353:攪拌片 36:內圈馬達 37:外圈轉子 371:外圈傳動皮帶 372:外圈轉軸 373:攪拌格柵 38:外圈馬達 301:第一迴旋缸 302:第一旋轉支撐架 4:分餾單元 41:第二軌道 42:第二坩鍋承載桶 43:第二升降組件 431:第二升降桿 432:第二氣壓缸 44:第二緊固夾頭 441:第二夾頭氣壓缸 401:第二迴旋缸 402:第二旋轉支撐架 A1:預備區 A2:攪拌區 A3:蒸餾區 101: Crucible 102:Discharge door 2:Machine 21: base body 22:Fixed plate 23: Bottom plate 3: Stirring unit 31: First track 32: The first crucible carrying barrel 33:First lifting component 331:The first lifting rod 332: First pneumatic cylinder 34: First fastening chuck 341: First chuck pneumatic cylinder 35: Inner ring rotor 351: Inner ring drive belt 352: Inner ring shaft 353: Stirring tablet 36: Inner ring motor 37: Outer ring rotor 371: Outer ring drive belt 372: Outer ring shaft 373: Stirring grate 38: Outer ring motor 301: First rotating cylinder 302: First rotating support frame 4: Fractionation unit 41:Second track 42: Second crucible carrying barrel 43:Second lifting component 431:Second lifting rod 432: Second pneumatic cylinder 44:Second fastening chuck 441:Second chuck pneumatic cylinder 401: Second swing cylinder 402: Second rotating support frame A1: Preparatory area A2: Stirring area A3: Distillation area
圖1是根據本發明實施例的一種雙轉子攪拌裝置操作在一狀態的示意圖。 圖2是根據本發明實施例的一種雙轉子攪拌裝置操作在另一狀態的示意圖。 圖3是根據本發明實施例的一種雙轉子攪拌裝置的第一坩鍋承載桶的立體圖。 圖4是根據本發明實施例的一種雙轉子攪拌裝置的第二坩鍋承載桶的立體圖。 圖5是根據本發明實施例的一種雙轉子攪拌裝置的內圈轉子及外圈轉子的示意圖。 Figure 1 is a schematic diagram of a dual-rotor stirring device operating in a state according to an embodiment of the present invention. Figure 2 is a schematic diagram of a dual-rotor stirring device operating in another state according to an embodiment of the present invention. Figure 3 is a perspective view of the first crucible carrying barrel of a dual-rotor stirring device according to an embodiment of the present invention. Figure 4 is a perspective view of the second crucible carrying barrel of a dual-rotor stirring device according to an embodiment of the present invention. Figure 5 is a schematic diagram of the inner rotor and the outer rotor of a dual-rotor stirring device according to an embodiment of the present invention.
35:內圈轉子 35: Inner ring rotor
351:內圈傳動皮帶 351: Inner ring drive belt
352:內圈轉軸 352: Inner ring shaft
353:攪拌片 353: Stirring tablet
36:內圈馬達 36: Inner ring motor
37:外圈轉子 37: Outer ring rotor
371:外圈傳動皮帶 371: Outer ring drive belt
372:外圈轉軸 372: Outer ring shaft
373:攪拌格柵 373: Stirring grate
38:外圈馬達 38: Outer ring motor
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20090071294A1 (en) * | 2002-12-21 | 2009-03-19 | Dirk Schmeisser | Rotary Stirring Device for Treating MoltenMetal |
WO2011083655A1 (en) * | 2010-01-07 | 2011-07-14 | 日新製鋼株式会社 | Operation method for mechanically stirring chrome-containing molten iron |
CN106914183A (en) * | 2017-04-05 | 2017-07-04 | 东北大学 | A kind of rotary EMS device for being arranged on metal bath furnace bottom |
CN114318165A (en) * | 2021-12-02 | 2022-04-12 | 重庆材料研究院有限公司 | Preparation method of rotor alloy capable of accurately controlling boron and nitrogen elements |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20090071294A1 (en) * | 2002-12-21 | 2009-03-19 | Dirk Schmeisser | Rotary Stirring Device for Treating MoltenMetal |
WO2011083655A1 (en) * | 2010-01-07 | 2011-07-14 | 日新製鋼株式会社 | Operation method for mechanically stirring chrome-containing molten iron |
CN106914183A (en) * | 2017-04-05 | 2017-07-04 | 东北大学 | A kind of rotary EMS device for being arranged on metal bath furnace bottom |
CN114318165A (en) * | 2021-12-02 | 2022-04-12 | 重庆材料研究院有限公司 | Preparation method of rotor alloy capable of accurately controlling boron and nitrogen elements |
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