TWI818215B - Elastic gel composition with protective function - Google Patents
Elastic gel composition with protective function Download PDFInfo
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- TWI818215B TWI818215B TW109144536A TW109144536A TWI818215B TW I818215 B TWI818215 B TW I818215B TW 109144536 A TW109144536 A TW 109144536A TW 109144536 A TW109144536 A TW 109144536A TW I818215 B TWI818215 B TW I818215B
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- Taiwan
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- weight
- oil
- liquid
- elastic gel
- composition
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 38
- 230000009993 protective function Effects 0.000 title 1
- 239000003921 oil Substances 0.000 claims abstract description 44
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 239000000419 plant extract Substances 0.000 claims abstract description 20
- 235000019198 oils Nutrition 0.000 claims description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
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- JYKSTGLAIMQDRA-UHFFFAOYSA-N tetraglycerol Chemical compound OCC(O)CO.OCC(O)CO.OCC(O)CO.OCC(O)CO JYKSTGLAIMQDRA-UHFFFAOYSA-N 0.000 description 1
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- FYGDTMLNYKFZSV-BYLHFPJWSA-N β-1,4-galactotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-BYLHFPJWSA-N 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Materials For Medical Uses (AREA)
- Dental Preparations (AREA)
Abstract
Description
本發明是關於一種擁有強度與柔軟性，具有高彈性的彈力凝膠狀組合物，其包含植物萃取液。此外，本發明特別是用於化妝材料，可作為醫藥品、化妝品、保養品、香氛或人體清潔用品等產品之原料。 The present invention relates to an elastic gel-like composition with strength, softness and high elasticity, which contains plant extract. In addition, the present invention is especially used in cosmetic materials and can be used as raw materials for pharmaceuticals, cosmetics, skin care products, fragrances or human body cleaning products.
中華民國發明專利申請號103141497提出一種水中油型乳化化妝料，其於油相中高調配紫外線吸收劑及紫外線散射劑，達成高SPF(Sun Protection Factor，防曬係數)，同時於塗佈於皮膚時具有獨特之嬌嫩之使用觸感。其特徵在於：其含有0.05~1質量%之疏水改性烷基纖維素、5~40質量%之油分、2.5~30質量%之具有疏水性表面之紫外線散射劑以及耐鹽性較低之水相增黏劑，且上述紫外線散射劑分散於油相中。 The Republic of China Invention Patent Application No. 103141497 proposes an oil-in-water emulsified cosmetic, which contains a high proportion of ultraviolet absorbers and ultraviolet scattering agents in the oil phase to achieve a high SPF (Sun Protection Factor, sun protection factor), and at the same time has the ability to be applied to the skin when applied to the skin. Unique and delicate touch. It is characterized in that it contains 0.05 to 1 mass % of hydrophobic modified alkyl cellulose, 5 to 40 mass % of oil, 2.5 to 30 mass % of ultraviolet scattering agent with hydrophobic surface and water with low salt resistance. phase tackifier, and the above-mentioned ultraviolet scattering agent is dispersed in the oil phase.
中華民國發明專利申請號106114234提出一種水中油型固形化妝料，其係水中油型製劑，且能夠於維持由增黏劑產生之彈性之狀態下固化為穩定之固形狀，具有所期望之彈力感，指蘸取性良好，且水潤之使用感優異。其特徵在於：包含疏水改性聚醚胺基甲酸酯0.1重量%~5重量%、親水性板狀粉末0.01重量%~5重量%、疏水性粉末、油分以及水。 The Republic of China Invention Patent Application No. 106114234 proposes an oil-in-water solid cosmetic. It is an oil-in-water preparation and can be solidified into a stable solid shape while maintaining the elasticity generated by the thickening agent, and has the desired elasticity. , means it has good dipping properties and has an excellent moist feel. It is characterized in that it contains 0.1% to 5% by weight of hydrophobic modified polyether urethane, 0.01% to 5% by weight of hydrophilic plate-like powder, hydrophobic powder, oil and water.
日本特許公告號2013-82686，揭示一種水中油型乳化皮膚外用劑，含有具有疏水基之水溶性增黏劑、具有HLB值14以上之非離子性界面活性劑、具有HLB3至5之聚醚改性有機矽及非乳化性之交聯型有機矽。 Japanese Patent Announcement No. 2013-82686 discloses an oil-in-water emulsified skin external preparation, which contains a water-soluble thickener with a hydrophobic group, a nonionic surfactant with an HLB value of 14 or more, and a polyether modification with HLB 3 to 5. Organic silicone and non-emulsifying cross-linked silicone.
日本特許公告號2006-213730，揭示一種化妝料，含有三-三甲基矽氧基異丁基矽烷15.0重量%、為聚甘油改性有機聚矽氧烷之非離子性界面活性劑1.0重量%、於交聯構造中具有聚甘油部分之交聯型有機聚矽氧烷1.5重量%及水。 Japanese Patent Publication No. 2006-213730 discloses a cosmetic containing 15.0% by weight of tri-trimethylsiloxyisobutylsilane and 1.0% by weight of a nonionic surfactant that is polyglycerol-modified organopolysiloxane. , 1.5% by weight of cross-linked organopolysiloxane having a polyglycerol part in the cross-linked structure and water.
本發明之一目的在於提供一種包含植物萃取液之彈力凝膠狀組合物，其可用為醫藥品、化妝品、保養品、香氛、凍凝露或人體清潔用品等產品。 One object of the present invention is to provide an elastic gel-like composition containing plant extracts, which can be used as pharmaceuticals, cosmetics, skin care products, fragrances, gels, or human body cleaning products.
為達成上述目的之功效，本發明提供一種彈力凝膠狀組合物，其具有一下層以及一上層，其中：該下層為一液體，其中以該液體總重量計，該液體之組成包含：水：10重量%~40重量%、甘油：5重量%~20重量%、植物萃取液：1重量%-10重量%、多元醇：1重量%~10重量%、玻尿酸鈉：0.01重量%~5重量%、聚丙烯酸：0.5重量%~5重量%、海藻酸鈉：0.5重量%~5重量%、三仙膠：0.5重量%~5重量%、小核菌膠：0.5重量%~2重量%、羥乙基纖維素：0.04重量%~2重量%、與瓜爾膠：0.04重量%~2重量%；該上層為一油體，其中以該油體總重量計，該油體之組成包含：低黏度矽油(1~20cst)：1重量%~5重量%、中黏度矽油(50~5000cst)：1重量%~5重量%、聚矽氧化合物：15重量%~30重量%、有機矽膠聯共聚物：5重量%~15重量%、有機矽彈體乳化劑：3重量%~6重量%、植物油：1重量%~5重量%、與合成酯：1重量%~10重量%，並且該上層與該下層之重量比例為1：1至1：10之間。 In order to achieve the above purpose, the present invention provides an elastic gel-like composition, which has a lower layer and an upper layer, wherein: the lower layer is a liquid, and based on the total weight of the liquid, the composition of the liquid includes: water: 10%~40% by weight, glycerin: 5%~20% by weight, plant extract: 1%~10% by weight, polyol: 1%~10% by weight, sodium hyaluronate: 0.01%~5% by weight %, polyacrylic acid: 0.5 wt% ~ 5 wt%, sodium alginate: 0.5 wt% ~ 5 wt%, Sanxian gum: 0.5 wt% ~ 5 wt%, Sclerotinia gum: 0.5 wt% ~ 2 wt%, Hydroxyethyl cellulose: 0.04% to 2% by weight, and guar gum: 0.04% to 2% by weight; the upper layer is an oil body, and based on the total weight of the oil body, the composition of the oil body includes: Low viscosity silicone oil (1~20cst): 1wt%~5wt%, medium viscosity silicone oil (50~5000cst): 1wt%~5wt%, polysilicone compound: 15wt%~30wt%, organic silicone compound Copolymer: 5%~15% by weight, organic silicone elastomer emulsifier: 3%~6% by weight, vegetable oil: 1%~5% by weight, and synthetic ester: 1%~10% by weight, and the The weight ratio of the upper layer to the lower layer is between 1:1 and 1:10.
更佳者，該上層之比重介於0.7~0.95之間，該下層之比重介於1.0~1.5之間。 Even better, the proportion of the upper layer is between 0.7 and 0.95, and the proportion of the lower layer is between 1.0 and 1.5.
更佳者，該油體與該液體為分別製備。 More preferably, the oil body and the liquid are prepared separately.
本發明之彈力凝膠狀組合物可實現快速分層之效果，使得位於下層液體中之植物萃取液能被上層之油體保護而不會與空氣、光線或灰塵直接接觸，由此，其不易產生質變，可以提升植物萃取液之存放時間，進而長時間地維持植物萃取液之生物活性。 The elastic gel-like composition of the present invention can achieve a rapid layering effect, so that the plant extract liquid located in the lower liquid layer can be protected by the oil body in the upper layer without direct contact with air, light or dust. Therefore, it is not easy to Producing qualitative changes can extend the storage time of plant extracts and maintain the biological activity of plant extracts for a long time.
此外，一含有矽聚合物之油體的上層，除了能保護下層所包含之植物萃取液，使其免於變質或受汙，亦可用於肌膚時形成一薄膜，具保護皮膚，防止水分散失、滋潤修護等防護功效。 In addition, the upper layer of an oil body containing silicone polymers can not only protect the plant extract contained in the lower layer from deterioration or contamination, but can also form a film when applied to the skin to protect the skin and prevent water loss. Moisturizing, repairing and other protective effects.
此外，本發明在不受外力之情況、倒置或者輕微晃動後不會使油液混合。 In addition, the present invention will not mix the oil when no external force is applied, or when it is inverted or slightly shaken.
(10):上層 (10):Upper level
(20):下層 (20):Lower level
(30):彈力凝膠狀組合物 (30): Elastic gel composition
(40):第一對照品 (40): First reference substance
(50):第二對照品 (50):Second reference substance
圖1為一剖面示意圖，用以繪示本發明之一實施方式的彈力凝膠狀組合物；圖2A為一照片圖，用以比較本發明之彈力凝膠狀組合物與第一對照品倒置前的狀態；圖2B為一照片圖，用以比較本發明之彈力凝膠狀組合物與第一對照品倒置後的狀態；圖2C為一照片圖，用以比較本發明之彈力凝膠狀組合物與第二對照品倒置後的狀態。 Figure 1 is a schematic cross-sectional view illustrating an elastic gel-like composition according to an embodiment of the present invention; Figure 2A is a photograph comparing the elastic gel-like composition of the present invention with the first reference substance. The state before; Figure 2B is a photograph for comparing the elastic gel-like composition of the present invention and the state after the first control substance is inverted; Figure 2C is a photograph for comparing the elastic gel-like composition of the present invention; The composition and the second control substance are inverted.
為讓本發明上述及/或其他目的、功效、特徵更明顯易懂，下文特舉較佳實施方式，作詳細說明於下：請參照圖1，為本發明的一實施方式，本發明之彈力凝膠狀組合物(30)可為一容置於化妝品包裝內之化妝品，但實際應用與包裝載體不以此為限。 In order to make the above and/or other objects, effects, and features of the present invention more obvious and easy to understand, preferred embodiments are listed below and described in detail: Please refer to Figure 1, which is an embodiment of the present invention. The elasticity of the present invention is The gel composition (30) can be a cosmetic contained in a cosmetic package, but the actual application and packaging carrier are not limited to this.
更佳者，本發明之彈力凝膠狀組合物(30)可為醫藥品、化妝品、保養品、香氛或人體清潔用品，但不以此為限。 More preferably, the elastic gel composition (30) of the present invention can be pharmaceuticals, cosmetics, skin care products, fragrances or human body cleaning products, but is not limited thereto.
更佳者，該彈力凝膠狀組合物(30)具有一上層(10)以及一相對於該上層(10)設置之下層(20)，其中該上、下兩層(10、20)可相互接觸。 More preferably, the elastic gel composition (30) has an upper layer (10) and a lower layer (20) arranged relative to the upper layer (10), wherein the upper and lower layers (10, 20) can interact with each other. get in touch with.
更佳者，該下層(20)包含含有膠體之液體，該上層(10)包含含有矽聚合物之油體。 More preferably, the lower layer (20) includes a liquid containing colloid, and the upper layer (10) includes an oil containing a silicone polymer.
更佳者，該上層(10)之比重介於0.7~0.95之間，該下層(20)之比重介於1.0~1.5之間。 More preferably, the proportion of the upper layer (10) is between 0.7 and 0.95, and the proportion of the lower layer (20) is between 1.0 and 1.5.
更佳者，該油體與該液體為分別製備。 More preferably, the oil body and the liquid are prepared separately.
更佳者，以該油體總重量計，該油體之組成包含：低黏度矽油(1~20cst)：1重量%~5重量%、中黏度矽油(50~5000cst)：1重量%~5重量%、聚矽氧化合物：15重量%~30重量%、有機矽膠聯共聚物：5重量%~15重量%、有機矽彈體乳化劑：3重量%~6重量%、植物油：1重量%~5重量%、合成酯：1重量%~10重量%。 More preferably, based on the total weight of the oil body, the composition of the oil body includes: low viscosity silicone oil (1~20cst): 1wt%~5wt%, medium viscosity silicone oil (50~5000cst): 1wt%~5 Weight %, polysilicone compound: 15 weight % ~ 30 weight %, organic silicone copolymer: 5 weight % ~ 15 weight %, organic silicone elastomer emulsifier: 3 weight % ~ 6 weight %, vegetable oil: 1 weight % ~5% by weight, synthetic ester: 1% by weight~10% by weight.
更佳者，該有機矽彈體乳化劑和該有機矽膠聯共聚物之重量比例的範圍為1：1.5~1：10之間、1：1.5~1：5之間、1：1.5~1：4之間、1：0.5~1：3之間、或1：1~1：2之間，但不以此為限。 More preferably, the weight ratio of the organic silicone elastomer emulsifier and the organic silicone copolymer ranges from 1:1.5 to 1:10, from 1:1.5 to 1:5, and from 1:1.5 to 1: Between 4, 1:0.5~1:3, or 1:1~1:2, but not limited to this.
更佳者，以該液體總重量計，該液體之組成包含：水：10重量%~40重量%、甘油：5重量%~20重量%、植物萃取液：1重量%~10重量%、多元醇：1 重量%~10重量%、玻尿酸鈉：0.01重量%~5重量%、聚丙烯酸：0.5重量%~5重量%、海藻酸鈉：0.5重量%~5重量%、三仙膠：0.5重量%~5重量%、小核菌膠：0.5重量%~2重量%、羥乙基纖維素：0.04重量%~2重量%、瓜爾膠：0.04重量%~2重量%。 More preferably, based on the total weight of the liquid, the composition of the liquid includes: water: 10% to 40% by weight, glycerin: 5% to 20% by weight, plant extract: 1% to 10% by weight, multi-component Alcohol: 1 Weight % ~ 10 weight %, sodium hyaluronate: 0.01 weight % ~ 5 weight %, polyacrylic acid: 0.5 weight % ~ 5 weight %, sodium alginate: 0.5 weight % ~ 5 weight %, Sanxian gum: 0.5 weight % ~ 5 % by weight, Sclerotinia gum: 0.5% by weight to 2% by weight, hydroxyethyl cellulose: 0.04% by weight~2% by weight, guar gum: 0.04% by weight~2% by weight.
更佳者，該彈力凝膠狀組合物之製法包含：先加入液體後加入油體，並將其混合物搖晃混合均勻然後靜置。 More preferably, the preparation method of the elastic gel composition includes: first adding liquid and then adding oil, shaking the mixture to mix evenly and then letting it stand.
更佳者，該油體與液體之重量比例的範圍為1：1~1：10之間、1：1~1：5之間、1：1.5~1：4之間、1：0.5~1：3之間、或1：1~1：2之間，但不以此為限。 Even better, the weight ratio of the oil to the liquid ranges from 1:1 to 1:10, from 1:1 to 1:5, from 1:1.5 to 1:4, and from 1:0.5 to 1 : between 3, or between 1:1~1:2, but not limited to this.
更佳者，該靜置時間至少為五分鐘。 Better yet, this resting time is at least five minutes.
更佳者，以該油體總重量計，該油體之組成包含：低黏度矽油(1~20cst)：1重量%~5重量%、中黏度矽油(50~5000cst)：1重量%~5重量%、聚矽氧化合物：15重量%~30重量%、有機矽膠聯共聚物：5重量%~15重量%、有機矽彈體乳化劑：3重量%~6重量%、植物油：1重量%~5重量%、合成酯：1重量%~10重量%，而以該液體總重量計，該液體之組成包含：水：10重量%~40重量%、甘油：5重量%~20重量%、植物萃取液：1重量%-10重量%、多元醇：1重量%~10重量%、玻尿酸鈉：0.01重量%~5重量%、聚丙烯酸：0.5重量%~5重量%、海藻酸鈉：0.5重量%~5重量%、三仙膠：0.5重量%~5重量%、小核菌膠：0.5重量%~2重量%、羥乙基纖維素：0.04重量%~2重量%、瓜爾膠：0.04重量%~2重量%。 More preferably, based on the total weight of the oil body, the composition of the oil body includes: low viscosity silicone oil (1~20cst): 1wt%~5wt%, medium viscosity silicone oil (50~5000cst): 1wt%~5 Weight %, polysilicone compound: 15 weight % ~ 30 weight %, organic silicone copolymer: 5 weight % ~ 15 weight %, organic silicone elastomer emulsifier: 3 weight % ~ 6 weight %, vegetable oil: 1 weight % ~5% by weight, synthetic ester: 1%~10% by weight, and based on the total weight of the liquid, the composition of the liquid includes: water: 10%~40% by weight, glycerin: 5%~20% by weight, Plant extract: 1% to 10% by weight, polyol: 1% to 10% by weight, sodium hyaluronate: 0.01% to 5% by weight, polyacrylic acid: 0.5% to 5% by weight, sodium alginate: 0.5 Weight % ~ 5 weight %, Sanxian gum: 0.5 weight % ~ 5 weight %, Sclerotinia gum: 0.5 weight % ~ 2 weight %, Hydroxyethyl cellulose: 0.04 weight % ~ 2 weight %, Guar gum: 0.04% by weight~2% by weight.
本發明之彈力凝膠狀組合物(30)可實現快速分層之效果，使得位於下層(20)液體中之植物萃取液能被上層(10)之油層保護而不會與空氣、光線或灰塵直接接觸，由此，其不易產生質變，可以提升植物萃取液之保護效果。 The elastic gel-like composition (30) of the present invention can achieve a rapid layering effect, so that the plant extract liquid located in the lower layer (20) can be protected by the oil layer of the upper layer (10) and will not interact with air, light or dust. Direct contact makes it less likely to undergo qualitative changes, which can enhance the protective effect of plant extracts.
更佳者，一含有矽聚合物之油體的上層(10)，除了能保護下層(20)所包含之植物萃取液，使其免於變質或受汙，亦可用於肌膚時形成一薄膜，具保護皮膚，防止水分散失、滋潤修護等防護功效。 Even better, an upper layer (10) containing a silicone polymer oil body can not only protect the plant extract contained in the lower layer (20) from deterioration or contamination, but can also form a film when applied to the skin. It has protective effects such as protecting the skin, preventing moisture loss, moisturizing and repairing.
更佳者，該植物萃取液可為花草萃取液、瓜果萃取液或其組合，且不以此為限。 More preferably, the plant extract can be flower and plant extract, melon and fruit extract, or a combination thereof, and is not limited thereto.
此外，本發明所添加之植物萃取液可定義為具有促進皮膚保護修護、抗皺、抗氧化、抗發炎、抗老化、及美白等功效之一的成分。舉例而言，植物萃取液可為中華民國發明專利公告號I697332所述之牛樟芽胚組織萃取物、中華民國發明專利公告號I417127所述之牡丹皮萃取物、中華民國發明專利公告號I495490所述之南國小薊萃取物、中華民國發明專利公告號I561254所述之月桃子萃取物、中華民國發明專利公告號I606836所述之牛至萃取物、中華民國發明專利公告號I474828所述之防風草萃取物、中華民國發明專利公告號I477292所述之沙苑子萃取物、中華民國發明專利公開號201536304所述之川續斷萃取物、中華民國發明專利公開號202021609所述之蘭花芽胚組織萃取物、中華民國發明專利公開號202023527所述之仙茅萃取物、大陸發明專利公開號CN109276493A所述之龍眼花萃取物、或大陸發明專利公開號CN108852924A所述之紅藜萃取物，但不以此為限，該等文獻全文併於此以供參考。 In addition, the plant extract added in the present invention can be defined as an ingredient that has the effects of promoting skin protection and repair, anti-wrinkle, antioxidant, anti-inflammation, anti-aging, and whitening. For example, the plant extract can be the Cinnamomum camphora bud embryo tissue extract described in the Republic of China Invention Patent Announcement No. I697332, the peony bark extract described in the Republic of China Invention Patent Announcement No. I417127, and the extract described in the Republic of China Invention Patent Announcement No. I495490. Southern thistle extract, moon peach extract described in the Republic of China Invention Patent Announcement No. I561254, oregano extract described in the Republic of China Invention Patent Announcement No. I606836, parsnip extract described in the Republic of China Invention Patent Announcement No. I474828 Objects, the Semen chinensis extract described in the Republic of China Invention Patent Publication No. I477292, the Dipsacus scutellariae extract described in the Republic of China Invention Patent Publication No. 201536304, the orchid germ tissue extract described in the Republic of China Invention Patent Publication No. 202021609, The curculigo extract described in the Republic of China Invention Patent Publication No. 202023527, the longan flower extract described in the Mainland Invention Patent Publication No. CN109276493A, or the red quinoa extract described in the Mainland Invention Patent Publication No. CN108852924A, but is not limited to this. , the full texts of these documents are hereby incorporated by reference.
更佳者，本發明所添加之合成酯之種類包含鄰苯二甲酸酯、己二酸酯、磷酸酯、偏苯三酸酯或具有C7-C9基團之合成性新戊四醇酯，但不以此為限。 More preferably, the types of synthetic esters added in the present invention include phthalate esters, adipate esters, phosphate esters, trimellitate esters or synthetic neopenterythritol esters with C7-C9 groups, But it is not limited to this.
更佳者，本發明所添加之低黏度矽油，其因該優異的光澤感、進展性、清爽感、潤滑性、撥水性、安全性等，被使用於各種用途，亦被多數使用於化妝料。 More preferably, the low-viscosity silicone oil added in the present invention is used in various applications due to its excellent gloss, progression, freshness, lubricity, water repellency, safety, etc., and is also used in many cosmetics. .
更佳者，本發明所添加之植物油種類包含玉米油、菜籽油或橄欖油，且不以此為限。 More preferably, the vegetable oil added in the present invention includes corn oil, rapeseed oil or olive oil, but is not limited thereto.
更佳者，本揭示之彈力凝膠狀組合物在不阻礙本揭示效果之範圍，必要時可適當含有其他成分，例如水性溶劑、陰離子性界面活性劑、陽離子界面活性劑、親油性非離子性界面活性劑、粉體、保濕劑、水溶性高分子、增黏劑、油性成分、皮膜劑、紫外線吸收劑、金屬離子封鎖劑、胺基酸、有機胺、高分子乳液、pH調整劑、皮膚營養劑、維生素、抗氧化劑、抗氧化助劑、香料等。 More preferably, the elastic gel-like composition of the present disclosure may appropriately contain other ingredients, such as aqueous solvents, anionic surfactants, cationic surfactants, lipophilic nonionics, if necessary, within the scope that does not hinder the effects of the disclosure. Surfactants, powders, moisturizers, water-soluble polymers, thickeners, oily ingredients, film agents, ultraviolet absorbers, metal ion blocking agents, amino acids, organic amines, polymer emulsions, pH adjusters, skin Nutrients, vitamins, antioxidants, antioxidant aids, spices, etc.
更佳者，本發明使用之水可使用可於化妝料、醫藥部外品等使用之水，例如可使用精製水、離子交換水、自來水等，但不以此為限。 More preferably, the water used in the present invention can be water that can be used in cosmetics, quasi-drugs, etc., such as purified water, ion exchange water, tap water, etc., but is not limited thereto.
更佳者，多元醇可列舉例如二元醇(例如乙二醇、丙二醇、三亞甲基二醇、1,2-丁二醇、1,3-丁二醇、四亞甲基二醇、2,3-丁二醇、五亞甲基二醇、2-丁烯-1,4-二醇、己二醇、辛二醇等)；三元醇(例如甘油、三羥甲基丙烷等)；四元醇(例如1,2,6-己三醇等新戊四醇等)；五元醇(例如木糖醇等)；六元醇(例如山梨糖醇、甘露醇等)；多元醇聚合物(例如二乙二醇、二丙二醇、三乙二醇、聚丙二醇、四乙二醇、二甘油、聚乙二醇、三甘油、四甘油、聚甘油等)；二元醇烷基醚類(例如乙二醇單甲醚、乙二醇單乙醚、乙二醇單丁醚、乙二醇單苯醚、乙二醇單己醚、乙二醇單2-甲基己醚、乙二醇異戊醚、乙二醇苯甲醚、乙二醇異丙醚、乙二醇二甲醚、乙二醇二乙醚、乙二醇二丁醚等)；二元醇烷基醚類(例如二乙二醇單甲醚、二乙二醇單乙醚、二乙二醇單丁醚、二乙二醇二甲醚、二乙二醇 二乙醚、二乙二醇丁醚、二乙二醇甲基乙醚、三乙二醇單甲醚、三乙二醇單乙醚、丙二醇單甲醚、丙二醇單乙醚、丙二醇單丁醚、丙二醇異丙醚、二丙二醇甲醚、二丙二醇乙醚、二丙二醇丁醚等)；二元醇醚酯(例如乙二醇單甲醚乙酸酯、乙二醇單乙醚乙酸酯、乙二醇單丁醚乙酸酯、乙二醇單苯醚乙酸酯、乙二醇二己二酸酯、乙二醇二琥珀酸酯、二乙二醇單乙醚乙酸酯、二乙二醇單丁醚乙酸酯、丙二醇單甲醚乙酸酯、丙二醇單乙醚乙酸酯、丙二醇單丙醚乙酸酯、丙二醇單苯醚乙酸酯等)；甘油單烷基醚(例如二甲苯醇、鯊油醇、鯊肝醇等)；糖醇(例如山梨糖醇、麥芽糖醇、麥芽三糖、甘露醇、蔗糖、赤藻糖醇、葡萄糖、果糖、澱粉分解糖、麥芽糖、木糖醇、澱粉分解糖還原醇等)；格利索得；四氫糠醇；POE-四氫糠醇；POP-丁醚；POP/POE-丁醚；三聚氧伸丙基甘油醚；POP-甘油醚；POP-甘油醚磷酸；POP/POE-新戊四醇醚、聚甘油等。 More preferably, the polyhydric alcohol may include dihydric alcohols (such as ethylene glycol, propylene glycol, trimethylene glycol, 1,2-butanediol, 1,3-butanediol, tetramethylene glycol, 2 , 3-butanediol, pentamethylene glycol, 2-butene-1,4-diol, hexanediol, octanediol, etc.); trihydric alcohols (such as glycerin, trimethylolpropane, etc.) ; Tetrahydric alcohols (such as 1,2,6-hexanetriol and other neopentyl erythritol, etc.); Pentahydric alcohols (such as xylitol, etc.); Hexahydric alcohols (such as sorbitol, mannitol, etc.); Polyhydric alcohols Polymers (such as diethylene glycol, dipropylene glycol, triethylene glycol, polypropylene glycol, tetraethylene glycol, diglycerol, polyethylene glycol, triglycerol, tetraglycerol, polyglycerol, etc.); glycol alkyl ethers Classes (such as ethylene glycol monomethyl ether, ethylene glycol monoethyl ether, ethylene glycol monobutyl ether, ethylene glycol monophenyl ether, ethylene glycol monohexyl ether, ethylene glycol mono2-methylhexyl ether, ethylene glycol Alcohol isopentyl ether, ethylene glycol anisole, ethylene glycol isopropyl ether, ethylene glycol dimethyl ether, ethylene glycol diethyl ether, ethylene glycol dibutyl ether, etc.); glycol alkyl ethers (such as Diethylene glycol monomethyl ether, diethylene glycol monoethyl ether, diethylene glycol monobutyl ether, diethylene glycol dimethyl ether, diethylene glycol Diethyl ether, diethylene glycol butyl ether, diethylene glycol methyl ether, triethylene glycol monomethyl ether, triethylene glycol monoethyl ether, propylene glycol monomethyl ether, propylene glycol monoethyl ether, propylene glycol monobutyl ether, propylene glycol isopropyl ether Ether, dipropylene glycol methyl ether, dipropylene glycol ethyl ether, dipropylene glycol butyl ether, etc.); glycol ether ester (such as ethylene glycol monomethyl ether acetate, ethylene glycol monoethyl ether acetate, ethylene glycol monobutyl ether) Acetate, ethylene glycol monophenyl ether acetate, ethylene glycol diadipate, ethylene glycol disuccinate, diethylene glycol monoethyl ether acetate, diethylene glycol monobutyl ether acetate ester, propylene glycol monomethyl ether acetate, propylene glycol monoethyl ether acetate, propylene glycol monopropyl ether acetate, propylene glycol monophenyl ether acetate, etc.); glycerol monoalkyl ethers (such as xylene alcohol, shark oil alcohol, carrotol, etc.); sugar alcohols (such as sorbitol, maltitol, maltotriose, mannitol, sucrose, erythritol, glucose, fructose, amylolytic sugar, maltose, xylitol, amylolytic sugar reduction alcohol, etc.); Glisode; tetrahydrofurfuryl alcohol; POE-tetrahydrofurfuryl alcohol; POP-butyl ether; POP/POE-butyl ether; tripolyoxypropyl glyceryl ether; POP-glyceryl ether; POP-glyceryl ether phosphate; POP/POE-Neopenterythritol ether, polyglycerol, etc.
更佳者，其他之多元醇可列舉選自例如聚氧伸乙基甲基葡萄糖苷(Glucam E-10)、聚氧伸丙基甲基葡萄糖苷(Glucam P-10)等之至少一種，且不以此為限。 More preferably, the other polyols can be at least one selected from polyoxyethylene methyl glucoside (Glucam E-10), polyoxypropyl methyl glucoside (Glucam P-10), etc., and Not limited to this.
更佳者，本發明使用之低黏度矽油包含：環四聚矽氧烷(Cyclotetrasiloxane)、環戊矽氧烷(Cyclopentasiloxane)、或聚二甲基矽氧烷(Dimethicone)(5~20cP)。 More preferably, the low-viscosity silicone oil used in the present invention includes: Cyclotetrasiloxane (Cyclotetrasiloxane), Cyclopentasiloxane (Cyclopentasiloxane), or Dimethicone (5~20cP).
更佳者，本發明所使用之中黏度矽油包含：聚二甲基矽氧烷(Dimethicone)(100~5000cP)、或苯丙基二甲基甲硅烷氧基硅酸酯(Phenylpropyl-dimethylsiloxysilicate)。 More preferably, the medium viscosity silicone oil used in the present invention includes: polydimethicone (100~5000cP) or phenylpropyl-dimethylsiloxysilicate (Phenylpropyl-dimethylsiloxysilicate).
更佳者，本發明所使用之聚矽氧化合物包含：環戊矽氧烷(Cyclopentasiloxane)/環四聚矽氧烷(Cyclotetrasiloxane)、水溶液(Aqua)/聚矽氧烷 季銨鹽-18(Silicone Quaternium-18)/十三烷醇聚醚-6(Trideceth-6)/十三烷醇聚醚-12(Trideceth-12)、或聚二甲基矽氧烷(Dimethicone)/氫化聚異丁烯(Hydrogenated Polyisobutene)。 More preferably, the polysiloxane compound used in the present invention includes: cyclopentasiloxane/cyclotetrasiloxane, aqueous solution (Aqua)/polysiloxane Silicone Quaternium-18/Trideceth-6/Trideceth-12, or Dimethicone )/Hydrogenated Polyisobutene.
更佳者，本發明所使用之有機矽膠聯共聚物包含：環戊矽氧烷與聚二甲基矽氧烷(Cyclopentasiloxane & Dimethicone)/乙烯基聚二甲矽氧烷交聯聚合物(Vinyldimethicone Crosspolymer)、或聚二甲基矽氧烷(Dimethicone)/鯨蠟硬脂基聚二甲基矽氧烷交聯聚合物(Cetearyl Dimethicone Crosspolymer、Cyclopentasiloxane)/烷基鯨蠟硬脂基聚二甲基矽氧烷交聯聚合物(C30-45 Alkyl Cetearyl Dimethicone Crosspolymer)。 More preferably, the organosilicone copolymer used in the present invention includes: Cyclopentasiloxane & Dimethicone/Vinyldimethicone Crosspolymer ), or polydimethicone/cetearyl dimethicone crosspolymer (Cyclopentasiloxane)/alkylcetearyl dimethicone Alkyl Cetearyl Dimethicone Crosspolymer (C30-45 Alkyl Cetearyl Dimethicone Crosspolymer).
更佳者，本發明所使用之有機矽彈體乳化劑包含：環戊矽氧烷(Cyclopentasiloxane)/聚乙二醇(PEG)/聚丙二醇-20/15聚二甲基矽氧烷(PPG-20/15 Dimethicone)、聚乙二醇-12聚二甲基矽氧烷(PEG-12 dimethicone)、環戊矽氧烷(Cyclopentasiloxane)/聚乙二醇-12聚二甲基矽氧烷交聯聚合物(PEG-12 Dimethicone Crosspolymer)、或乳化安定劑(Cetyl Diglyceryl Tris(Trimethylsiloxy)silylethyl Dimethicone)。 More preferably, the organic silicone elastomer emulsifier used in the present invention includes: cyclopentasiloxane (Cyclopentasiloxane)/polyethylene glycol (PEG)/polypropylene glycol-20/15 polydimethylsiloxane (PPG- 20/15 Dimethicone), polyethylene glycol-12 polydimethicone (PEG-12 dimethicone), cyclopentasiloxane/polyethylene glycol-12 polydimethylsiloxane cross-linking Polymer (PEG-12 Dimethicone Crosspolymer), or emulsion stabilizer (Cetyl Diglyceryl Tris(Trimethylsiloxy)silylethyl Dimethicone).
圖2A為本發明彈力凝膠狀組合物(30)與第一對照品(40)倒置前的狀態，其中，本發明彈力凝膠狀組合物(30)與第二對照品(50)倒置前的狀態亦相同；圖2B為本發明彈力凝膠狀組合物(30)與第一對照品(40)倒置後的狀態；圖2C為本發明彈力凝膠狀組合物(30)與第二對照品(50)倒置後的狀態。 Figure 2A shows the state of the elastic gel-like composition (30) of the present invention and the first reference substance (40) before they are inverted, wherein the elastic gel-like composition (30) of the present invention and the second reference substance (50) are before they are inverted. The state is also the same; Figure 2B is the state after the elastic gel composition (30) of the present invention and the first control substance (40) are inverted; Figure 2C is the elastic gel composition (30) of the present invention (30) and the second control article. Product (50) is in an inverted state.
更佳者，本發明為先加入水相後加入油相，其中，有機矽彈體乳化劑和有機矽膠聯共聚物之重量比例為1：1.5~1：10之間，油液之重量比例為1：1~1：10之間，再經過靜置一小時來達成油液分層，並且在無外力作用下、倒置 或輕微晃動不會使油液混合；如圖2B所示，該第一對照品(40)為先加入油相後加入水相，其中，有機矽彈體乳化劑和有機矽膠聯共聚物之重量比例為1：1.5~1：10之間，油液之重量比例為1：11，再經過靜置一小時，由於油相與水相加入之順序錯誤，該油液之重量比例亦錯誤，因此該油體無法凝固，其再倒置後無法產生與本發明相同之功效；如圖2C所示，該第二對照品(50)為先加入油相後加入水相，其中，有機矽彈體乳化劑和有機矽膠聯共聚物之重量比例為1：1.5~1：10之間，油液之重量比例為1：0.8，再經過靜置一小時，由於油相與水相加入之順序錯誤，該油液之重量比例亦錯誤，因此該油體無法凝固，其再倒置後無法產生與本發明相同之功效。 More preferably, the present invention adds the water phase first and then the oil phase, wherein the weight ratio of the organic silicon elastomer emulsifier and the organic silicon copolymer is between 1:1.5 and 1:10, and the weight ratio of the oil is Between 1:1 and 1:10, let it sit for another hour to achieve oil stratification, and turn it upside down without external force. Or slight shaking will not mix the oil; as shown in Figure 2B, the first control substance (40) is added first to the oil phase and then to the water phase, in which the weight of the organic silicone elastomer emulsifier and the organic silicone copolymer The ratio is between 1:1.5~1:10, and the weight ratio of the oil is 1:11. After another hour of standing, due to the wrong order of adding the oil phase and the water phase, the weight ratio of the oil is also wrong, so The oil body cannot solidify, and it cannot produce the same effect as the present invention after being inverted; as shown in Figure 2C, the second reference substance (50) is added first to the oil phase and then to the water phase, in which the organic silicone elastomer is emulsified The weight ratio of the agent and the silicone copolymer is between 1:1.5 and 1:10, and the weight ratio of the oil is 1:0.8. After letting it stand for one hour, due to the wrong order of adding the oil phase and the water phase, the The weight ratio of the oil is also wrong, so the oil cannot solidify and cannot produce the same effect as the present invention after it is inverted.
惟以上所述者，僅為本發明之較佳實施例，但不能以此限定本創作實施之範圍；故，凡依本創作申請專利範圍及說明書內容所做之簡單的等效改變與修飾，皆仍屬本創作專利涵蓋之範圍內。 However, the above are only preferred embodiments of the present invention, but they cannot limit the scope of implementation of this invention; therefore, any simple equivalent changes and modifications made based on the patent scope of this invention and the content of the description, All are still within the scope of this creative patent.
(10):上層 (10):Upper level
(20):下層 (20):Lower level
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| CN107595761A (en) * | 2017-11-13 | 2018-01-19 | 广州市花安堂生物科技有限公司 | A kind of suspension oil droplet toner and preparation method thereof |
| WO2019043172A1 (en) * | 2017-09-04 | 2019-03-07 | Lts Lohmann Therapie-Systeme Ag | Transdermal delivery system including an emulsifier |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2019043172A1 (en) * | 2017-09-04 | 2019-03-07 | Lts Lohmann Therapie-Systeme Ag | Transdermal delivery system including an emulsifier |
| CN107595761A (en) * | 2017-11-13 | 2018-01-19 | 广州市花安堂生物科技有限公司 | A kind of suspension oil droplet toner and preparation method thereof |
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| 網路文獻 2019-07-16「必囤貨的高cp值雪芙蘭加拿大冰河泉水卸妝系列、水平衡胺基酸超濃密水感泡泡洗面乳(含全成分分析)」一文 * |
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