TWI796067B - Phase splitter and phase processing system - Google Patents

Phase splitter and phase processing system Download PDF

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TWI796067B
TWI796067B TW110148955A TW110148955A TWI796067B TW I796067 B TWI796067 B TW I796067B TW 110148955 A TW110148955 A TW 110148955A TW 110148955 A TW110148955 A TW 110148955A TW I796067 B TWI796067 B TW I796067B
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outer plate
phase
plate
baffle
channel
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TW110148955A
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TW202228831A (en
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楊慕震
高陳璣
蕭錦燻
金志龍
蔡易良
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財團法人工業技術研究院
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Abstract

A phase splitter includes a main body, a first baffle plate, a plurality of second baffle plates, an inlet, a first outlet and a second outlet. The main body includes a first outer plate, a second outer plate opposite to the first outer plate and a third outer plate. The first baffle plate and the third outer plate are disposed opposite to each other. The second baffle plates are separately disposed among the first outer plate, the second outer plate, the third outer plate and the first baffle plate, and each second baffle plate has a first end and a second end opposite to the first end. There is a first channel between each first end and the first outer plate, and there is a second channel between each second end and the second outer plate. The inlet is disposed on the third outer plate and faces one of the second baffle plates. The first outlet is disposed on the second outer plate and adjacent to the first baffle plate. The first baffle plate has a third end having a third channel and a fourth end opposite to the third end, and the fourth end is connected to the second outer plate, and the second outlet communicates with the third channel.

Description

分相器及分相製程系統 Phase splitter and phase split process system

本揭露有關於一種分相器及分相製程系統。 The present disclosure relates to a phase splitter and a phase splitting process system.

習知分相器多使用薄膜,連續分離出二種不互溶液體。然而,薄膜式分相器具有流通量小、分相速度慢以及操作成本高等問題。因此,提出一種新的分相器以改善前述問題是本技術領域業者努力目標之一。 Conventional phase separators mostly use membranes to continuously separate two immiscible liquids. However, thin-film phase separators have problems such as small throughput, slow phase separation speed, and high operating costs. Therefore, proposing a new phase splitter to improve the aforementioned problems is one of the goals of the practitioners in this technical field.

本揭露係有關於一種分相器及分相製程系統,可改善前述先前技術之問題。 The present disclosure relates to a phase splitter and a phase splitting process system, which can improve the aforementioned problems in the prior art.

根據本揭露之一實施例,提出一種分相器。分相器包括本體、第一檔板、複數第二檔板、入口、第一出口及第二出口。本體包括相對的第一外側板與第二外側板以及第三外側板。第一檔板與第三外側板相對配置。此些第二檔板彼此間隔地配置在第一外側板、第二外側板、第三外側板與第一檔板之間,且各第二檔板具有相對之第一端與第二端,各第一端與第一外側板之間具有第一通道且各第二端與第二外側板之間具有第二通道。入口配 置在第三外側板,且朝向此些第二檔板之一者。第一出口配置於第二外側板且鄰近於第一檔板配置。第一檔板具有相對之第三端與第四端,第三端具有第三通道,而第四端連接於第二外側板,第二出口連通第三通道。 According to an embodiment of the present disclosure, a phase splitter is provided. The phase splitter includes a body, a first baffle, a plurality of second baffles, an inlet, a first outlet and a second outlet. The body includes a first outer panel, a second outer panel and a third outer panel opposite to each other. The first baffle plate is arranged opposite to the third outer plate. The second baffles are spaced apart from each other between the first outer panel, the second outer panel, the third outer panel and the first baffle, and each second baffle has a first end and a second end opposite to each other, There is a first channel between each first end and the first outer plate, and a second channel between each second end and the second outer plate. Import Placed on the third outer panel and facing one of the second baffles. The first outlet is disposed on the second outer plate and adjacent to the first baffle plate. The first baffle plate has a third end and a fourth end opposite to each other, the third end has a third channel, and the fourth end is connected to the second outer plate, and the second outlet communicates with the third channel.

根據本揭露之另一實施例,提出一種分相製程系統。分相製程系統包括分相器及混合器。分相器包括本體、第一檔板、複數第二檔板、入口、第一出口及第二出口。本體包括相對的第一外側板與第二外側板以及第三外側板。第一檔板與第三外側板相對配置。此些第二檔板彼此間隔地配置在第一外側板、第二外側板、第三外側板與第一檔板之間,且各第二檔板具有相對之第一端與第二端,各第一端與第一外側板之間具有第一通道且各第二端與第二外側板之間具有第二通道。入口配置在第三外側板,且朝向此些第二檔板之一者。第一出口配置於第二外側板且鄰近於第一檔板配置。第一檔板具有相對之第三端與第四端,第三端具有第三通道,而第四端連接於第二外側板,第二出口連通第三通道。混合器具有混合液出口,混合液出口連通分相器之入口。 According to another embodiment of the present disclosure, a phase separation process system is provided. The phase separation process system includes a phase splitter and a mixer. The phase splitter includes a body, a first baffle, a plurality of second baffles, an inlet, a first outlet and a second outlet. The body includes a first outer panel, a second outer panel and a third outer panel opposite to each other. The first baffle plate is arranged opposite to the third outer plate. The second baffles are spaced apart from each other between the first outer panel, the second outer panel, the third outer panel and the first baffle, and each second baffle has a first end and a second end opposite to each other, There is a first channel between each first end and the first outer plate, and a second channel between each second end and the second outer plate. The inlet is disposed on the third outer plate and faces one of the second barrier plates. The first outlet is disposed on the second outer plate and adjacent to the first baffle plate. The first baffle plate has a third end and a fourth end opposite to each other, the third end has a third channel, and the fourth end is connected to the second outer plate, and the second outlet communicates with the third channel. The mixer has a mixed liquid outlet, and the mixed liquid outlet is connected to the inlet of the phase separator.

為了對本揭露之上述及其他方面有更佳的瞭解,下文特舉實施例,並配合所附圖式詳細說明如下: In order to have a better understanding of the above and other aspects of the present disclosure, the following specific embodiments are described in detail in conjunction with the attached drawings as follows:

10,20:分相製程系統 10,20: Phase separation process system

11:混合器 11: Mixer

11a:第一入口 11a: First entrance

11b:第二入口 11b: Second entrance

11c:混合液出口 11c: Mixed solution outlet

100,200,300,400:分相器 100,200,300,400: phase splitter

110,210:本體 110,210: Ontology

111:第一外側板 111: the first outer plate

112:第二外側板 112: the second outer plate

113:第三外側板 113: The third outer plate

115:第五外側板 115: Fifth outer plate

116:第六外側板 116: The sixth outer plate

120:第一檔板 120: The first baffle

121:第三端 121: third end

122:第四端 122: Fourth end

123:第七端 123: seventh end

124:第八端 124: eighth terminal

130,130’:第二檔板 130,130': Second baffle

131:第一端 131: first end

132:第二端 132: second end

133:第五端 133: fifth end

134:第六端 134: sixth end

140:入口 140: Entrance

150:第一出口 150: The first exit

160:第二出口 160: The second exit

214:第四外側板 214: The fourth outer plate

LQ1,LQ2:液體 LQ1, LQ2: liquid

A1:角度 A1: angle

C1:中間位置 C1: middle position

F1,F1’:混合液 F1, F1': mixed solution

F11,F11’:重相 F11, F11': heavy phase

F12,F12’:輕相 F12, F12': light phase

H:高度 H: height

t1:長度 t1: length

P1:第一通道 P1: first channel

P2:第二通道 P2: second channel

P3:第三通道 P3: the third channel

P4:第四通道 P4: the fourth channel

SP1:容置空間 SP1: Accommodating Space

T,t2:厚度 T, t2: Thickness

W:寬度 W: width

第1A圖繪示依照本揭露一實施例之分相器之示意圖。 FIG. 1A shows a schematic diagram of a phase splitter according to an embodiment of the present disclosure.

第1B圖繪示第1A圖之分相器沿方向1B-1B’之剖面圖。 Fig. 1B shows a cross-sectional view of the phase splitter in Fig. 1A along the direction 1B-1B'.

第1C圖繪示第1A圖之分相器之俯視圖。 Figure 1C shows a top view of the phase splitter of Figure 1A.

第2圖繪示依照本揭露另一實施例之分相器之剖面圖。 FIG. 2 shows a cross-sectional view of a phase splitter according to another embodiment of the present disclosure.

第3圖繪示依照本揭露另一實施例之分相器之剖面圖。 FIG. 3 shows a cross-sectional view of a phase splitter according to another embodiment of the present disclosure.

第4圖繪示依照本揭露另一實施例之分相器之剖面圖。 FIG. 4 shows a cross-sectional view of a phase splitter according to another embodiment of the present disclosure.

第5圖繪示依照本揭露一實施例之分相製程系統的示意圖。 FIG. 5 is a schematic diagram of a phase separation process system according to an embodiment of the present disclosure.

第6圖繪示依照本揭露另一實施例之分相製程系統的示意圖。 FIG. 6 is a schematic diagram of a phase separation process system according to another embodiment of the present disclosure.

請參照第1A~1C圖,第1A圖繪示依照本揭露一實施例之分相器100之示意圖,第1B圖繪示第1A圖之分相器100沿方向1B-1B’之剖面圖,而第1C圖繪示第1A圖之分相器100之俯視圖。 Please refer to Figures 1A~1C, Figure 1A shows a schematic diagram of a phase splitter 100 according to an embodiment of the present disclosure, and Figure 1B shows a cross-sectional view of the phase splitter 100 of Figure 1A along the direction 1B-1B', 1C shows a top view of the phase splitter 100 shown in FIG. 1A.

如第1A及1B圖所示,分相器100包括本體110、複數第一檔板120、第二檔板130(130’)、入口140、第一出口150及第二出口160。本體110包括相對的第一外側板111與第二外側板112以及第三外側板113。第一檔板120與第三外側板113相對配置。複數第二檔板130彼此間隔地配置在第一外側板111、第二外側板112、第三外側板113與第一檔板120之間,且各第二檔板130具有相對之第一端131與第二端132,各第一端131與第一外側板111之間具有第一通道P1且各第二端132與第二外側板112之間具有第二通道P2。入口140配置在第三外側板113且朝向此些第二檔板130之一者。第一出口150配置於第二外側板112且鄰近 於第一檔板120配置。第一檔板120具有相對之第三端121與第四端122,第三端121具有一第三通道P3,第四端122連接於第二外側板112,而第二出口160連通第三通道P3。 As shown in FIGS. 1A and 1B , the phase splitter 100 includes a body 110 , a plurality of first baffles 120 , a second baffle 130 ( 130 ′), an inlet 140 , a first outlet 150 and a second outlet 160 . The body 110 includes a first outer panel 111 , a second outer panel 112 and a third outer panel 113 opposite to each other. The first baffle plate 120 is arranged opposite to the third outer plate 113 . A plurality of second baffle plates 130 are arranged at intervals between the first outer plate 111 , the second outer plate 112 , the third outer plate 113 and the first baffle plate 120 , and each second baffle plate 130 has an opposite first end. 131 and the second end 132 , there is a first channel P1 between each first end 131 and the first outer plate 111 , and there is a second channel P2 between each second end 132 and the second outer plate 112 . The inlet 140 is disposed on the third outer plate 113 and faces one of the second barrier plates 130 . The first outlet 150 is disposed on the second outer plate 112 and adjacent to the It is configured on the first baffle plate 120 . The first baffle plate 120 has a third end 121 and a fourth end 122 opposite to each other, the third end 121 has a third channel P3, the fourth end 122 is connected to the second outer plate 112, and the second outlet 160 communicates with the third channel P3.

藉由分相器100,由重相F11與輕相F 12混合而成之混合液F1從入口140進入本體110內部後,受到第一個第二檔板130’(最靠近入口140)之消波作用,重相F11與輕相F12分離,其中重相F11往下沉澱而輕相F12往上漂浮。混合液F1可透過第一通道P1及第二通道P2往下一個第二檔板130流動,並重複前述之消波、沉澱及漂浮動作。經過一段時間後,如第1B圖所示,重相F11(以密度較大之網點表示)與輕相F12(以密度較小之網點表示)處於平衡狀態,此時重相F11與輕相F12幾乎完全分離。重相F11可從第一出口150流出,而輕相F12可從第二出口160流出。依據模擬結果,本揭露實施例之分相器100可以在數秒內(如,10秒、25秒、更常或甚至更短)完成混合液F1之重相F11與輕相F12分離,而習知分相器在相同時間內仍處於震盪期。 Through the phase separator 100, the mixed liquid F1 formed by mixing the heavy phase F11 and the light phase F12 enters the interior of the body 110 from the inlet 140, and is eliminated by the first and second baffles 130' (closest to the inlet 140). Wave action, the heavy phase F11 is separated from the light phase F12, wherein the heavy phase F11 settles down and the light phase F12 floats up. The mixed liquid F1 can flow to the next second baffle plate 130 through the first channel P1 and the second channel P2, and repeat the aforementioned wave breaking, settling and floating actions. After a period of time, as shown in Figure 1B, the heavy phase F11 (represented by denser dots) and the light phase F12 (represented by less dense dots) are in a state of equilibrium. At this time, the heavy phase F11 and the light phase F12 almost completely separated. The heavy phase F11 can flow out from the first outlet 150 , while the light phase F12 can flow out from the second outlet 160 . According to the simulation results, the phase separator 100 of the embodiment of the present disclosure can complete the separation of the heavy phase F11 and the light phase F12 of the mixed liquid F1 within a few seconds (such as 10 seconds, 25 seconds, more often or even shorter), while conventional The phase splitter is still in the oscillation period during the same period.

此外,本揭露實施例之第一檔板120及/或第二檔板130結構簡單,例如是平板,使分相器100以簡單結構就能實現分相的技術功效。在另一實施例中,視分相性能而定,第一檔板120及/或第二檔板130也可以是曲面板,或者為平面與曲面所所形成的板件。 In addition, the first baffle plate 120 and/or the second baffle plate 130 in the embodiment of the present disclosure has a simple structure, such as a flat plate, so that the phase splitter 100 can achieve the technical effect of phase separation with a simple structure. In another embodiment, depending on the phase separation performance, the first baffle plate 120 and/or the second baffle plate 130 may also be a curved plate, or a plate formed by a plane and a curved surface.

前述重相F11意指密度相對較大之組成,而輕相F12意指密度相對較小之組成。重相F11與輕相F12分別為二完全不互 溶之液相,或互溶性很小的液相。在一實施例中,重相F11與輕相F12的密度差等於或大於0.1公克/立方公分,可得到符合預期的分相效果。 The aforementioned heavy phase F11 means a composition with a relatively high density, while the light phase F12 means a composition with a relatively low density. The heavy phase F11 and the light phase F12 are two and completely different from each other Soluble liquid phase, or liquid phase with little miscibility. In one embodiment, the density difference between the heavy phase F11 and the light phase F12 is equal to or greater than 0.1 g/cm 3 , and an expected phase separation effect can be obtained.

此外,適用於本揭露實施例之分相器的混合液F1例如是藥液、化學液等不同密度成分組成之混合液體。 In addition, the mixed liquid F1 suitable for the phase separator of the embodiments of the present disclosure is, for example, a mixed liquid composed of components with different densities such as medical liquid and chemical liquid.

如第1A及1B圖所示,在本實施例中,第二出口160為第三通道P3之一開口,且第一檔板120構成本體110之第四外側板。 本體110更包括相對之第五外側板115與第六外側板116。第一外側板111、第二外側板112、第三外側板113、第一檔板120(第四外側板)、第五外側板115與第六外側板116構成本體110的外邊界,且圍繞出一容置空間SP1。第一檔板120之內表面及第二檔板130(130’)位於容置空間SP1內。 As shown in FIGS. 1A and 1B , in this embodiment, the second outlet 160 is an opening of the third channel P3 , and the first baffle plate 120 constitutes the fourth outer plate of the main body 110 . The body 110 further includes a fifth outer panel 115 and a sixth outer panel 116 opposite to each other. The first outer plate 111, the second outer plate 112, the third outer plate 113, the first baffle plate 120 (the fourth outer plate), the fifth outer plate 115 and the sixth outer plate 116 constitute the outer boundary of the body 110, and surround An accommodating space SP1 is created. The inner surface of the first baffle 120 and the second baffle 130 (130') are located in the accommodation space SP1.

在一實施例中,容置空間SP1的容積介於10毫升~10公升之間。此外,本體110具有高度H、寬度W及厚度T,其中高度H例如是介於5公分~30公分,寬度W例如是介於5公分~30公分,而厚度T例如是介於1公分~15公分,然亦可更大或更小。 In one embodiment, the volume of the accommodating space SP1 is between 10 milliliters and 10 liters. In addition, the body 110 has a height H, a width W and a thickness T, wherein the height H is, for example, between 5 cm and 30 cm, the width W is, for example, between 5 cm and 30 cm, and the thickness T is, for example, between 1 cm and 15 cm. cm, but it can be larger or smaller.

如第1C圖所示,各第二檔板130具有相對之第五端133與第六端134,各第二檔板130之第五端133與第六端134分別連接第五外側板115與第六外側板116,如此能限制混合液F1只能透過第一通道P1及第二通道P2流動。此外,第一檔板120具有相對之第七端123與第八端124,第一檔板120之第七端123與第八 端124分別連接第五外側板115與第六外側板116,如此能限制混合液F1只能透過第一出口150及第二出口160流出本體110外。 As shown in Figure 1C, each second baffle plate 130 has a fifth end 133 and a sixth end 134 opposite to each other, and the fifth end 133 and the sixth end 134 of each second baffle plate 130 are respectively connected to the fifth outer plate 115 and the sixth end 134. The sixth outer plate 116 can restrict the flow of the mixed liquid F1 only through the first channel P1 and the second channel P2. In addition, the first baffle 120 has a seventh end 123 and an eighth end 124 opposite to each other, and the seventh end 123 and the eighth end 124 of the first baffle 120 are opposite to each other. The ends 124 are respectively connected to the fifth outer plate 115 and the sixth outer plate 116 , so that the mixed liquid F1 can only flow out of the main body 110 through the first outlet 150 and the second outlet 160 .

如第1B及1C圖所示,入口140朝向最外側之第二檔板130’的中間位置C1或中間區域。如此,可使從入口140進入本體110之內部的混合液F1在撞擊到中間位置C1(或中間區域)後,往上、下方向大致上等距地進入第一通道P1及第二通道P2。 As shown in Figures 1B and 1C, the inlet 140 faces the middle position C1 or the middle area of the outermost second baffle plate 130'. In this way, the mixed liquid F1 entering the body 110 from the inlet 140 can enter the first channel P1 and the second channel P2 substantially equidistantly upward and downward after hitting the middle position C1 (or the middle area).

請參照第2圖,其繪示依照本揭露另一實施例之分相器200之剖面圖。分相器200包括本體210、複數第一檔板120、第二檔板130、入口140、第一出口150及第二出口160。本體210包括相對的第一外側板111與第二外側板112、相對之第三外側板113與第四外側板214以及相對之第五外側板115與第六外側板116。 本揭露實施例之分相器200具有類似或同於分相器100之技術特徵,不同處在於,分相器200之第一檔板120完全位於本體210內。 Please refer to FIG. 2 , which shows a cross-sectional view of a phase splitter 200 according to another embodiment of the present disclosure. The phase splitter 200 includes a body 210 , a plurality of first baffles 120 , a second baffle 130 , an inlet 140 , a first outlet 150 and a second outlet 160 . The body 210 includes a first outer panel 111 and a second outer panel 112 , a third outer panel 113 and a fourth outer panel 214 , and a fifth outer panel 115 and a sixth outer panel 116 . The phase splitter 200 of the disclosed embodiment has similar or same technical features as the phase splitter 100 , except that the first baffle plate 120 of the phase splitter 200 is completely inside the body 210 .

如第2圖所示,第一檔板120位於此些第二檔板130之一者與第四外側板214之間。第二出口160配置於第二外側板112且位於第一檔板120與第四外側板214之間,而第二檔板130與第四外側板214之間以第四通道P4隔開,第四通道P4與第三通道P3相通,其中第二出口160係第四通道P4之開口。 As shown in FIG. 2 , the first baffle plate 120 is located between one of the second baffle plates 130 and the fourth outer plate 214 . The second outlet 160 is arranged on the second outer plate 112 and is located between the first baffle plate 120 and the fourth outer plate 214, and the second baffle plate 130 and the fourth outer plate 214 are separated by a fourth passage P4, the second The four channels P4 communicate with the third channel P3, wherein the second outlet 160 is the opening of the fourth channel P4.

藉由分相器200,由重相F11與輕相F12混合而成之混合液F1從入口140進入本體110內部後,受到第一個第二檔板130’(最靠近入口140)之消波作用,重相F11與輕相F12分離,其中重相F11往下沉澱而輕相F12往上漂浮。混合液F1可透過第一通 道P1及第二通道P2往下一個第二檔板130流動,並重複前述之消波、沉澱及漂浮動作。經過一段時間後,如第2圖所示,重相F11(以密度較大之網點表示)與輕相F12(以密度較小之網點表示)處於平衡狀態,此時重相F11與輕相F12幾乎完全分離。重相F11可從第一出口150流出,而輕相F12可從第二出口160流出。依據模擬結果,本揭露實施例之分相器200可以在數秒內(如,10秒、25秒、30秒、更長或甚至更短)完成混合液F1之重相F11與輕相F12分離,而習知分相器在相同時間內仍處於震盪期。 Through the phase separator 200, the mixed liquid F1 formed by mixing the heavy phase F11 and the light phase F12 enters the interior of the main body 110 from the inlet 140, and is subjected to wave suppression by the first and second baffles 130' (closest to the inlet 140). As a result, the heavy phase F11 is separated from the light phase F12, wherein the heavy phase F11 settles down and the light phase F12 floats up. Mixed solution F1 can pass through the first pass The channel P1 and the second channel P2 flow to the next second baffle plate 130, and repeat the aforementioned wave breaking, settling and floating actions. After a period of time, as shown in Figure 2, the heavy phase F11 (represented by denser dots) and the light phase F12 (represented by less dense dots) are in a state of equilibrium. At this time, the heavy phase F11 and the light phase F12 almost completely separated. The heavy phase F11 can flow out from the first outlet 150 , while the light phase F12 can flow out from the second outlet 160 . According to the simulation results, the phase separator 200 of the disclosed embodiment can complete the separation of the heavy phase F11 and the light phase F12 of the mixed liquid F1 within a few seconds (for example, 10 seconds, 25 seconds, 30 seconds, longer or even shorter), However, the conventional phase splitter is still in the oscillating period during the same period.

此外,第二檔板130具有長度t1及厚度t2,本揭露實施例不限定各第二檔板130的長度t1的數值及厚度t2的數值。複數第二檔板130之至少二者之長度t1可相等或相異,且/或複數第二檔板130之至少二者之厚度t2的數值可相等或相異。此外,複數第二檔板130之至少二者之角度可相等或相異,以下舉例說明。 In addition, the second baffle 130 has a length t1 and a thickness t2 , and the embodiment of the present disclosure does not limit the value of the length t1 and the thickness t2 of each second baffle 130 . The length t1 of at least two of the plurality of second baffles 130 may be equal or different, and/or the value of the thickness t2 of at least two of the plurality of second baffles 130 may be equal or different. In addition, the angles of at least two of the plurality of second baffle plates 130 can be equal or different, as illustrated below.

請參照第3圖,其繪示依照本揭露另一實施例之分相器300之剖面圖。分相器300包括本體210、複數第一檔板120、第二檔板130、入口140、第一出口150及第二出口160。分相器300具有類似或同於分相器100之技術特徵,不同處在於,分相器300之第二檔板130之角度A1不同。 Please refer to FIG. 3 , which shows a cross-sectional view of a phase splitter 300 according to another embodiment of the present disclosure. The phase splitter 300 includes a body 210 , a plurality of first baffles 120 , a second baffle 130 , an inlet 140 , a first outlet 150 and a second outlet 160 . The phase splitter 300 has similar or the same technical features as the phase splitter 100, the difference is that the angle A1 of the second baffle plate 130 of the phase splitter 300 is different.

此些第二檔板130之至少一者相對第二外側板112係傾斜配置。例如,第二檔板130相對於第二外側板112夾有一角度A1,其中角度A1例如是銳角,在一實施例中,銳角之範圍可介於45度與90度之間,然亦可更小。 At least one of the second baffle plates 130 is inclined relative to the second outer plate 112 . For example, the second baffle plate 130 forms an angle A1 with respect to the second outer plate 112, wherein the angle A1 is, for example, an acute angle. In one embodiment, the range of the acute angle can be between 45 degrees and 90 degrees, but it can also be more. Small.

請參照第4圖,其繪示依照本揭露另一實施例之分相器300之剖面圖。分相器400包括本體210、複數第一檔板120、第二檔板130、入口140、第一出口150及第二出口160。分相器300具有類似或同於分相器300之技術特徵,不同處在於,分相器400之每個第二檔板130之角度A1不同。詳言之,分相器400之第二檔板130相對第二外側板112夾有一角度A1,其中角度A1例如是鈍角,在一實施例中,鈍角之範圍可介於90度與135度之間,然亦可更大。此外,相距第三外側板113最近的第二檔板130與第三外側板113之間具有一第一角度A21,相距第三外側板113最近的第二檔板130與第二外側板112之間具有一第二角度A22,第一角度A21及第二角度A22皆為銳角且第一角度A21小於第二角度A22。 Please refer to FIG. 4 , which shows a cross-sectional view of a phase splitter 300 according to another embodiment of the present disclosure. The phase splitter 400 includes a body 210 , a plurality of first baffles 120 , a second baffle 130 , an inlet 140 , a first outlet 150 and a second outlet 160 . The phase splitter 300 has similar or the same technical features as the phase splitter 300, except that the angle A1 of each second baffle plate 130 of the phase splitter 400 is different. Specifically, the second baffle plate 130 of the phase splitter 400 forms an angle A1 relative to the second outer plate 112, wherein the angle A1 is, for example, an obtuse angle. In one embodiment, the range of the obtuse angle can be between 90 degrees and 135 degrees. space, but it can also be larger. In addition, there is a first angle A21 between the second baffle plate 130 closest to the third outer plate 113 and the third outer plate 113 , and the distance between the second baffle plate 130 closest to the third outer plate 113 and the second outer plate 112 There is a second angle A22 between them, the first angle A21 and the second angle A22 are both acute angles, and the first angle A21 is smaller than the second angle A22.

如第4圖所示,由於角度A1為鈍角,因此混合液F1在進入本體210之初期(如,前幾秒內),重相F11與輕相F12分離,且大部分或幾乎全部之重相F11不會越過第二檔板130之第一端131(不通過第一通道P1)而至下一個第二檔板130,如此可獲得高分離效率且分相速度更快(即,更快達到輕、重相平衡)。只要分相初期之重相F11不會越過第二檔板130之第一端131,往後分相中、後期之重相F11也不會越過第二檔板130之第一端131,使整個分相過程達到平衡狀態之速度更快且/或分離效率更高。 As shown in Figure 4, since the angle A1 is an obtuse angle, the heavy phase F11 and the light phase F12 are separated from the light phase F12 when the mixed liquid F1 enters the body 210 (for example, in the first few seconds), and most or almost all of the heavy phase F11 will not go over the first end 131 of the second baffle plate 130 (not through the first passage P1) to the next second baffle plate 130, so that high separation efficiency can be obtained and the phase separation speed is faster (that is, reaching light and heavy phase balance). As long as the heavy phase F11 in the initial stage of phase splitting will not cross the first end 131 of the second baffle plate 130, the heavy phase F11 in the middle and later stages of phase splitting will not cross the first end 131 of the second baffle plate 130, so that the entire The phase separation process reaches equilibrium faster and/or with higher separation efficiency.

此外,可視混合液F1之輕相及重相之密度差及/或混合液F1進入入口140之速度等參數,決定第二檔板130之尺寸及/或角度,其中此些第二檔板130之至少二者的尺寸及/或角度可相 同或相異,第二檔板130的高度例如為容置空間SP1(本體210)之高度的30%至90%或50%至70%,然亦可更小或更大。 In addition, depending on parameters such as the density difference between the light phase and the heavy phase of the mixed liquid F1 and/or the speed at which the mixed liquid F1 enters the inlet 140, the size and/or angle of the second baffle plate 130 can be determined, wherein these second baffle plates 130 The size and/or angle of at least two of them can be the same Same or different, the height of the second baffle plate 130 is, for example, 30% to 90% or 50% to 70% of the height of the accommodating space SP1 (body 210 ), but it can also be smaller or larger.

以下說明本揭露實施例之分相器的實驗結果。 The experimental results of the phase splitter according to the embodiments of the present disclosure are described below.

第一實驗例 The first experimental example

如下表一所示,採用如第2圖的分相器200,混合前,輕相由100wt%之甲苯(萃取劑)組成,而重相由82.6wt%之水與17.4wt%之丙酮組成。輕相與重相混合成混合液F1,由於甲苯吸收重相中丙酮,因此混合液F1中重相之丙酮濃度下降至6.86wt%。混合液F1可經過前述分相器分離成輕相及重相,其中分離之輕相由89.83wt%之甲苯與10.17wt%之丙酮組成,而重相由93.14wt%之水與6.86wt%之丙酮組成,此結果與熱力學模擬結果相近,足證本揭露實施例之分相效果接近理想之熱力學模擬結果。 As shown in Table 1 below, using the phase separator 200 shown in Figure 2, before mixing, the light phase consists of 100wt% toluene (extractant), and the heavy phase consists of 82.6wt% water and 17.4wt% acetone. The light phase and the heavy phase are mixed to form a mixed liquid F1. Since toluene absorbs the acetone in the heavy phase, the concentration of acetone in the heavy phase in the mixed liquid F1 drops to 6.86wt%. The mixed liquid F1 can be separated into a light phase and a heavy phase through the aforementioned phase separator, wherein the separated light phase is composed of 89.83wt% toluene and 10.17wt% acetone, and the heavy phase is composed of 93.14wt% water and 6.86wt% Composition of acetone, this result is similar to the thermodynamic simulation result, which fully proves that the phase separation effect of the disclosed embodiment is close to the ideal thermodynamic simulation result.

Figure 110148955-A0305-02-0012-1
Figure 110148955-A0305-02-0012-1

第二實驗例 The second experimental example

請參照第5圖,其繪示依照本揭露一實施例之分相製程系統10的示意圖。分相製程系統10包括至少一分相器200及至少一混合器11。混合器11具有第一入口11a、第二入口11b及混合液出口11c,混合液出口11c連通分相器200之入口140。在一實施例中,混合器11可進行不互溶相液體之間的化學反應,即作為微型反應器,可參考台灣專利公開號TW202023679A,但本揭露不以此為限。 Please refer to FIG. 5 , which shows a schematic diagram of a phase separation process system 10 according to an embodiment of the present disclosure. The phase separation process system 10 includes at least one phase splitter 200 and at least one mixer 11 . The mixer 11 has a first inlet 11 a , a second inlet 11 b and a mixed liquid outlet 11 c , and the mixed liquid outlet 11 c is connected to the inlet 140 of the phase separator 200 . In one embodiment, the mixer 11 can perform a chemical reaction between immiscible liquids, that is, as a microreactor, for which reference can be made to Taiwan Patent Publication No. TW202023679A, but the present disclosure is not limited thereto.

如下表二,液體LQ1為丙酮水溶液(含19wt%丙酮),而液體LQ2為100wt%之甲苯(萃取劑),液體LQ1及液體LQ2分別從混合器11之第一入口11a及第二入口11b進入混合器11內部混合成混合液F1。混合時,甲苯吸收(萃取)水中丙酮,使後續經過分相器200之混合液F1所分離出之重相F11包含較少之丙酮(一部分都由輕相F12之甲苯吸收)。 The following table 2, liquid LQ1 is acetone aqueous solution (containing 19wt% acetone), and liquid LQ2 is 100wt% toluene (extractant), liquid LQ1 and liquid LQ2 enter from the first inlet 11a and the second inlet 11b of the mixer 11 respectively Mixer 11 internally mixes to form mixed solution F1. During mixing, the toluene absorbs (extracts) the acetone in the water, so that the heavy phase F11 separated from the mixed liquid F1 through the phase separator 200 contains less acetone (part of which is absorbed by the toluene in the light phase F12).

混合完成後,混合液F1從分相器200之入口140進入分相器200內部,分離成第一道重相F11與第一道輕相F12,其中第一道重相F11為包含2.18wt%之丙酮的水溶液。相較於分相前之混合液F1,第一道重相F11之丙酮含量大幅降低(如表二所示,從19wt%降低至2.18wt%)。在另一實施例中,混合液F1進入分相器200前,可先進入至少一反應器(未繪示)進行適當反應後,再進入分相器200。 After the mixing is completed, the mixed liquid F1 enters the phase separator 200 from the inlet 140 of the phase separator 200, and is separated into the first heavy phase F11 and the first light phase F12, wherein the first heavy phase F11 contains 2.18wt% Aqueous solution of acetone. Compared with the mixed solution F1 before phase separation, the acetone content of the first heavy phase F11 was greatly reduced (as shown in Table 2, from 19wt% to 2.18wt%). In another embodiment, before entering the phase separator 200 , the mixed liquid F1 may first enter at least one reactor (not shown) for proper reaction, and then enter the phase separator 200 .

為了取得更純(丙酮濃度更低)之水,可針對第一道重相F11進行第二次分相。例如,如第5圖所示,第一道重相F11與液體LQ2(萃取劑)分別從下一個混合器11之第一入口11a及第二入口11b進 入混合器11內部混合成混合液F1’。混合時,甲苯吸收(萃取)第一道重相F11中丙酮,使後續經過下一個分相器200之混合液F1’所分離出之第二道重相F11’包含更少之丙酮(一部分都由輕相F12’之甲苯吸收)。混合完成後,混合液F1’從下一個分相器200之入口140進入分相器200內部,分離成第二道重相F11’與第二道輕相F12’,其中第二道重相F11’為包含0.14wt%之丙酮的水溶液。相較於第一道重相F11,第二道重相F11’之丙酮含量大幅降低(如表二所示,從2.18wt%降低至0.14wt%)。此外,在另一實施例中,混合液F1’進入前述下一個分相器200前,可先進入至少一反應器(未繪示)進行適當反應後,再進入分相器200。如表二所示,使用本揭露實施例分相器之結果與熱力學模擬結果相近,足證本揭露實施例之分相效果接近理想之熱力學模擬結果。 In order to obtain more pure (lower acetone concentration) water, the second phase separation can be carried out for the first heavy phase F11. For example, as shown in Figure 5, the first heavy phase F11 and the liquid LQ2 (extractant) enter from the first inlet 11a and the second inlet 11b of the next mixer 11 respectively. into the interior of mixer 11 and mixed into mixed liquid F1'. When mixing, toluene absorbs (extracts) acetone in the first heavy phase F11, so that the second heavy phase F11' separated from the mixed solution F1' of the next phase separator 200 contains less acetone (a part of which is made of Toluene absorption of light phase F12'). After the mixing is completed, the mixed liquid F1' enters the phase separator 200 from the inlet 140 of the next phase separator 200, and is separated into the second heavy phase F11' and the second light phase F12', wherein the second heavy phase F11' is An aqueous solution containing 0.14 wt% acetone. Compared with the first heavy phase F11, the acetone content of the second heavy phase F11' was greatly reduced (as shown in Table 2, from 2.18wt% to 0.14wt%). In addition, in another embodiment, before entering the next phase separator 200, the mixed liquid F1' may first enter at least one reactor (not shown) for proper reaction, and then enter the phase separator 200. As shown in Table 2, the results of using the phase splitter of the disclosed embodiment are similar to the thermodynamic simulation results, which fully proves that the phase separation effect of the disclosed embodiment is close to the ideal thermodynamic simulation result.

Figure 110148955-A0305-02-0014-2
Figure 110148955-A0305-02-0014-2

在另一實施例中,若欲得到更純之水(丙酮濃度更低),可執行第5圖之分相流程數次(混合液經過一個混合器及一個分相器稱為一次分相流程),隨分相流程之次數增加,水純度會逐次提高。 In another embodiment, if one wants to obtain more pure water (lower concentration of acetone), the phase-separation process of Fig. 5 can be performed several times (the mixed liquid passes through a mixer and a phase separator, which is called a phase-separation process ), as the number of phase separation processes increases, the water purity will gradually increase.

在另一實施例中,第5圖之二個分相器200中至少一者可由分相器100、300與400之一者取代。 In another embodiment, at least one of the two phase splitters 200 in FIG. 5 can be replaced by one of the phase splitters 100 , 300 and 400 .

第三實驗例 The third experimental example

請參照第6圖,其繪示依照本揭露另一實施例之分相製程系統20的示意圖。分相製程系統20包括至少一分相器200及至少一混合器11。液體LQ1為有機溶液,而液體LQ2為100wt%之水(萃取劑),液體LQ1至少包含甲苯、四氫呋喃(THF)、硼酸及有機物(例如,藥物)等溶質。液體LQ1為製作有機物所產生的產物,內含所欲之有機物。 Please refer to FIG. 6 , which shows a schematic diagram of a phase separation process system 20 according to another embodiment of the present disclosure. The phase separation process system 20 includes at least one phase splitter 200 and at least one mixer 11 . The liquid LQ1 is an organic solution, and the liquid LQ2 is 100wt% water (extractant). The liquid LQ1 at least contains solutes such as toluene, tetrahydrofuran (THF), boric acid, and organic substances (eg, drugs). Liquid LQ1 is a product produced by making organic matter, and contains desired organic matter.

如第6圖所示,液體LQ1與液體LQ2分別從混合器11之第一入口11a及第二入口11b進入混合器11內部充分混合成混合液F1。混合時,水能吸收(萃取)有機溶液中之硼酸,以增加有機層中有機物之濃度。 As shown in FIG. 6, the liquid LQ1 and the liquid LQ2 respectively enter the mixer 11 from the first inlet 11a and the second inlet 11b of the mixer 11 and are fully mixed into the mixed liquid F1. When mixed, water can absorb (extract) boric acid in the organic solution to increase the concentration of organic matter in the organic layer.

如下表三,混合完成後,混合液F1包含水層及有機層,其中水層包含11.8wt%之四氫呋喃(THF)、0.2wt%之甲苯、98wt%之水、95.7wt%之硼酸及其它溶質(不限定),而有機層包含86.4wt%之THF、99.4wt%之甲苯、2.0wt%之水、4.3wt%之硼酸及有機物(未寫於表格)。透過分相器200,可分離水層及有機層。前述成分之比例例如指個別組成在不同相之間的比例。例如,混合液F1從分相器200 之入口140進入分相器200內部,分離成重相F11(表三之水層)與輕相F12(表三之有機層)。相較於混合液F1,分離後之輕相F12之硼酸含量大幅降低(如表三所示,從100wt%降低至4.3wt%),增加了輕相F12中有機物的濃度(純化效果)。在另一實施例中,混合液F1進入分相器200前,可先進入至少一反應器(未繪示)進行適當反應後,再進入分相器200。 As shown in Table 3, after the mixing is completed, the mixed liquid F1 contains an aqueous layer and an organic layer, wherein the aqueous layer contains 11.8wt% tetrahydrofuran (THF), 0.2wt% toluene, 98wt% water, 95.7wt% boric acid and other solutes (Not limited), and the organic layer contains 86.4wt% of THF, 99.4wt% of toluene, 2.0wt% of water, 4.3wt% of boric acid and organic matter (not written in the table). Through the phase separator 200, the aqueous layer and the organic layer can be separated. The ratio of the aforementioned components refers to, for example, the ratio of individual components among different phases. For example, the mixed liquid F1 from the phase separator 200 The inlet 140 enters the phase separator 200 and is separated into heavy phase F11 (water layer in Table 3) and light phase F12 (organic layer in Table 3). Compared with the mixed solution F1, the boric acid content of the separated light phase F12 was greatly reduced (as shown in Table 3, from 100wt% to 4.3wt%), which increased the concentration of organic matter in the light phase F12 (purification effect). In another embodiment, before entering the phase separator 200 , the mixed liquid F1 may first enter at least one reactor (not shown) for proper reaction, and then enter the phase separator 200 .

Figure 110148955-A0305-02-0016-3
Figure 110148955-A0305-02-0016-3

雖然未繪示,然輕相F12與液體LQ2(萃取劑)可分別從下一個混合器11(未繪示)之第一入口11a及第二入口11b進入混合器11內部充分混合成混合液。混合時,水吸收(萃取)有機溶液中之硼酸,以增加有機層中有機物之濃度。混合完成後,混合液可再進入下一個分相器200(未繪示),以分離出硼酸含量更低之輕相(純化效果)。 Although not shown, the light phase F12 and the liquid LQ2 (extractant) can respectively enter the mixer 11 from the first inlet 11a and the second inlet 11b of the next mixer 11 (not shown) to fully mix into a mixed liquid. When mixed, the water absorbs (extracts) the boric acid in the organic solution to increase the concentration of organic matter in the organic layer. After the mixing is completed, the mixed liquid can enter the next phase separator 200 (not shown) to separate the light phase with lower boric acid content (purification effect).

在另一實施例中,若欲得到更純之有機物溶液,可執行第6圖之分相流程數次(混合液經過一個混合器及一個分相器稱為一次分相流程),隨分相流程之次數增加,有機物溶液之有機物濃度(純度)會逐次提高。 In another embodiment, if desired to obtain a purer organic solution, the phase-separation process of Fig. 6 can be performed several times (the mixed solution passes through a mixer and a phase separator, which is called a phase-separation process), and the phase-separation As the number of processes increases, the organic concentration (purity) of the organic solution will gradually increase.

在另一實施例中,第6圖之二個分相器200中至少一者可由分相器100、300與400之一者取代。 In another embodiment, at least one of the two phase splitters 200 in FIG. 6 can be replaced by one of the phase splitters 100 , 300 and 400 .

綜上,本揭露實施例之分相器採用複數間隔配置之檔板,以達到對混合液之消波效果,使重相往下沉澱,輕相往上漂浮。相較於習知薄膜式分相器,本揭露實施例之分相器至少具有以下技術功效:(1).可省略昂貴之薄膜,因此成本低;(2).結構簡單;(3).混合液可高速或高流量地進入分相器,因此分相速度快。 To sum up, the phase separator of the embodiment of the present disclosure adopts a plurality of baffles arranged at intervals to achieve the wave-absorbing effect on the mixed liquid, so that the heavy phase settles downward and the light phase floats upward. Compared with the conventional thin-film phase splitter, the phase splitter of the embodiment of the present disclosure has at least the following technical effects: (1). Expensive thin films can be omitted, so the cost is low; (2). The structure is simple; (3). The mixed liquid can enter the phase separator at high speed or high flow rate, so the phase separation speed is fast.

綜上所述,雖然本揭露已以實施例揭露如上,然其並非用以限定本揭露。本揭露所屬技術領域中具有通常知識者,在不脫離本揭露之精神和範圍內,當可作各種之更動與潤飾。因此,本揭露之保護範圍當視後附之申請專利範圍所界定者為準。 To sum up, although the present disclosure has been disclosed above with embodiments, it is not intended to limit the present disclosure. Those with ordinary knowledge in the technical field to which this disclosure belongs may make various changes and modifications without departing from the spirit and scope of this disclosure. Therefore, the scope of protection of this disclosure should be defined by the scope of the appended patent application.

100:分相器 100: phase splitter

110:本體 110: Ontology

111:第一外側板 111: the first outer plate

112:第二外側板 112: the second outer plate

113:第三外側板 113: The third outer plate

120:第一檔板 120: The first baffle

121:第三端 121: third end

122:第四端 122: Fourth end

130,130’:第二檔板 130,130': Second baffle

131:第一端 131: first end

132:第二端 132: second end

140:入口 140: Entrance

150:第一出口 150: The first exit

160:第二出口 160: The second exit

C1:中間位置 C1: middle position

F1:混合液 F1: mixed solution

F11:重相 F11: heavy phase

F12:輕相 F12: light phase

P1:第一通道 P1: first channel

P2:第二通道 P2: second channel

P3:第三通道 P3: the third channel

SP1:容置空間 SP1: Accommodating Space

Claims (14)

一種分相器,包括:一本體,包括相對的一第一外側板與一第二外側板以及一第三外側板;一第一檔板,與該第三外側板相對配置;複數第二檔板,彼此間隔地配置在該第一外側板、該第二外側板、該第三外側板與該第一檔板之間,且各該第二檔板具有相對之一第一端與一第二端,各該第一端與該第一外側板之間具有一第一通道且各該第二端與該第二外側板之間具有一第二通道;一入口,配置在該第三外側板,且朝向該些第二檔板之一者;一第一出口,配置於該第二外側板且鄰近於該第一檔板配置;以及一第二出口;其中,該第一檔板具有相對之一第三端與一第四端,該第三端具有一第三通道,而該第四端連接於該第二外側板,該第二出口連通該第三通道;其中,相距該第三外側板最近的該第二檔板與該第三外側板之間具有一第一角度,相距該第三外側板最近的該第二檔板與該第二外側板之間具有一第二角度,該第一角度及該第二角度皆為銳角且該第一角度小於該第二角度。 A phase splitter, comprising: a body, including a first outer plate, a second outer plate and a third outer plate opposite to each other; a first baffle plate arranged opposite to the third outer plate; a plurality of second gears Plates are spaced apart from each other between the first outer plate, the second outer plate, the third outer plate and the first baffle plate, and each of the second baffle plates has a first end opposite to a first baffle plate. Two ends, each of the first end and the first outer plate has a first channel and each of the second end and the second outer plate has a second channel; an inlet is arranged on the third outer side plate, and towards one of the second baffles; a first outlet, configured on the second outer plate and adjacent to the first baffle; and a second outlet; wherein, the first baffle has Relative to a third end and a fourth end, the third end has a third channel, and the fourth end is connected to the second outer plate, and the second outlet communicates with the third channel; There is a first angle between the second baffle plate closest to the third outer plate and the third outer plate, and a second angle between the second baffle plate closest to the third outer plate and the second outer plate , both the first angle and the second angle are acute angles, and the first angle is smaller than the second angle. 如請求項1所述之分相器,其中該第一檔板構成該本體之一第四外側板,該第二出口為該第三通道之一開口。 The phase splitter as claimed in claim 1, wherein the first baffle plate constitutes a fourth outer plate of the body, and the second outlet is an opening of the third channel. 如請求項2所述之分相器,其中該本體更包括相對之一第五外側板與一第六外側板;該第一外側板、該第二外側板、該第三外側板、該第四外側板、該第五外側板與該第六外側板構成該本體的外邊界。 The phase splitter as described in claim 2, wherein the body further includes a fifth outer plate and a sixth outer plate; the first outer plate, the second outer plate, the third outer plate, the first outer plate The four outer panels, the fifth outer panel and the sixth outer panel constitute an outer boundary of the body. 如請求項1所述之分相器,其中該本體更包括相對之一第五外側板與一第六外側板,各該第二檔板具有相對之一第五端與一第六端,各該第一檔板之該第五端與該第六端分別連接該第五外側板與該第六外側板。 The phase splitter as described in claim 1, wherein the body further includes a fifth outer plate and a sixth outer plate opposite to each other, each of the second baffle plates has a fifth end and a sixth end opposite to each other, each The fifth end and the sixth end of the first baffle are respectively connected to the fifth outer plate and the sixth outer plate. 如請求項1所述之分相器,其中該本體具有相對之一第五外側板與一第六外側板;該第一檔板具有相對之一第七端與一第八端,該第一檔板之該第七端與該第八端分別連接該第五外側板與該第六外側板。 The phase splitter as claimed in item 1, wherein the body has a fifth outer plate and a sixth outer plate opposite; the first baffle plate has a seventh end and an eighth end opposite, the first The seventh end and the eighth end of the baffle are respectively connected to the fifth outer plate and the sixth outer plate. 如請求項1所述之分相器,其中該本體更包括一與該第三外側板相對之第四外側板,該第一檔板位於該些第二檔板之一者與該第四外側板之間,且該第二出口配置於該第二外側板且位於該第一檔板與該第四外側板之間。 The phase splitter as claimed in claim 1, wherein the body further includes a fourth outer plate opposite to the third outer plate, and the first baffle plate is located between one of the second baffle plates and the fourth outer plate between the plates, and the second outlet is disposed on the second outer plate and between the first baffle plate and the fourth outer plate. 如請求項6所述之分相器,其中該第二檔板與該第四外側板之間以一第四通道隔開,該第四通道與該第三通道相通。 The phase splitter according to claim 6, wherein a fourth channel is separated between the second baffle plate and the fourth outer plate, and the fourth channel communicates with the third channel. 如請求項7所述之分相器,其中該第二出口係該第四通道之一開口。 The phase splitter as claimed in claim 7, wherein the second outlet is an opening of the fourth channel. 如請求項1所述之分相器,其中各該第二檔板相對該第二外側板係傾斜配置。 The phase splitter as claimed in claim 1, wherein each of the second baffle plates is arranged obliquely relative to the second outer plate. 如請求項9所述之分相器,其中該第二檔板相對於該第二外側板夾有一角度,該角度的範圍介於45度至90度之間。 The phase splitter as claimed in claim 9, wherein the second baffle plate forms an angle with respect to the second outer plate, and the range of the angle is between 45 degrees and 90 degrees. 如請求項9所述之分相器,其中該第二檔板相對於該第二外側板夾有一角度,該角度的範圍介於90度至135度之間。 The phase splitter as claimed in claim 9, wherein the second baffle plate forms an angle with respect to the second outer plate, and the range of the angle is between 90 degrees and 135 degrees. 如請求項1所述之分相器,其中該些第二檔板的高度為該本體之高度的30%至90%。 The phase splitter according to claim 1, wherein the height of the second baffles is 30% to 90% of the height of the main body. 如請求項1所述之分相器,其中該入口朝向最外側之該第二檔板的中間位置或中間區域。 The phase splitter as claimed in claim 1, wherein the inlet faces the middle position or the middle area of the outermost second baffle plate. 一種分相製程系統,包括:一如請求項1~13中任一項所述之分相器;以及一混合器,具有一混合液出口,該混合液出口連通該分相器之該入口。 A phase separation process system, comprising: a phase separator as described in any one of claims 1 to 13; and a mixer having a mixed solution outlet connected to the inlet of the phase separator.
TW110148955A 2021-01-26 2021-12-27 Phase splitter and phase processing system TWI796067B (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0670815B1 (en) * 1992-08-24 2000-11-29 Lemacon Techniek B.V. Method and device for the separation of a contaminated top layer
CN2868379Y (en) * 2005-12-13 2007-02-14 陕西中恒粮油工程技术有限公司 Mixed solvent phase splitter
WO2012019624A1 (en) * 2010-08-11 2012-02-16 Fmc Technologies C.V. High efficiency phase splitter
JP2018062512A (en) * 2016-10-12 2018-04-19 三菱ケミカル株式会社 Method and apparatus for producing aqueous organic carboxylic acid solution

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0670815B1 (en) * 1992-08-24 2000-11-29 Lemacon Techniek B.V. Method and device for the separation of a contaminated top layer
CN2868379Y (en) * 2005-12-13 2007-02-14 陕西中恒粮油工程技术有限公司 Mixed solvent phase splitter
WO2012019624A1 (en) * 2010-08-11 2012-02-16 Fmc Technologies C.V. High efficiency phase splitter
CN103124587A (en) * 2010-08-11 2013-05-29 Fmc科技有限合伙公司 High efficiency phase splitter
JP2018062512A (en) * 2016-10-12 2018-04-19 三菱ケミカル株式会社 Method and apparatus for producing aqueous organic carboxylic acid solution

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