TWI635890B - Flow distributor for liquid descending - Google Patents

Flow distributor for liquid descending Download PDF

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Publication number
TWI635890B
TWI635890B TW103103576A TW103103576A TWI635890B TW I635890 B TWI635890 B TW I635890B TW 103103576 A TW103103576 A TW 103103576A TW 103103576 A TW103103576 A TW 103103576A TW I635890 B TWI635890 B TW I635890B
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TW
Taiwan
Prior art keywords
liquid
distribution
elongated side
side member
elongated
Prior art date
Application number
TW103103576A
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Chinese (zh)
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TW201436845A (en
Inventor
達倫馬修 荷德利
艾薩克 尼歐瓦特
史帝芬安德魯 派爾
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科氏格利奇有限合夥公司
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001Processes specially adapted for distillation or rectification of fermented solutions
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F25/00Component parts of trickle coolers
    • F28F25/02Component parts of trickle coolers for distributing, circulating, and accumulating liquid
    • F28F25/04Distributing or accumulator troughs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/008Liquid distribution
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18Absorbing units; Liquid distributors therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D21/00Heat-exchange apparatus not covered by any of the groups F28D1/00 - F28D20/00
    • F28D21/0015Heat and mass exchangers, e.g. with permeable walls

Abstract

本發明提供一種用於在垂直長形質量轉移塔中下降的液體的流量分配器、用於其之質量轉移塔、及處理在質量轉移塔中的流體流的方法。流量分配器包含用於轉移液體至複數個向外延伸之側臂構件之中央分配構件,其依序將液體饋送進入位在長形側構件下之複數個分配槽。分配槽可基本上垂直或平行於長形側構件定向,分配槽包含設置其中之填料床。在汽-液或液-液塔中使用這樣的分配器導致跨越質量轉移塔的直徑的液體更均勻的水平分佈。 The present invention provides a flow distributor for a liquid falling in a vertically elongated mass transfer tower, a mass transfer tower therefor, and a method of processing a fluid flow in the mass transfer tower. The flow distributor includes a central distribution member for transferring liquid to a plurality of outwardly extending side arm members, which sequentially feeds liquid into a plurality of distribution slots located below the elongated side member. The distribution trough may be oriented substantially perpendicular or parallel to the elongated side member, the distribution trough containing a packed bed disposed therein. The use of such a distributor in a vapor-liquid or liquid-liquid column results in a more uniform horizontal distribution of liquid across the diameter of the mass transfer column.

Description

用於液體下降之流量分配器 Flow distributor for liquid drop

本發明大致係關於熱及質量轉移塔,且更精確地係關於在這樣的塔中使用液體流量分配器及使用這樣的液體流量分配器分配液體的方法。 The present invention relates generally to heat and mass transfer towers, and more precisely to the use of liquid flow distributors in such towers and methods of distributing liquids using such liquid flow distributors.

質量轉移塔被設置以接觸兩個彼此特性不同的液體流,實現質量及/或熱在不同相之間交換。在本文中所使用的用語「質量轉移塔」並不意在限制其中質量轉移為塔內的液體流的處理的主要目的之塔,而是也意在涵蓋在其中的熱轉移,而不是質量轉移為前述處理的主要目的之塔。某些質量轉移塔,諸如在多組分蒸餾及吸收應用中使用,以液體流接觸氣體或蒸氣流,而另一些,如萃取塔,可被設計為促進兩不同密度的液相之間的接觸。質量轉移塔被設置以通常沿著設置於塔中之多個質量轉移表面使上升的蒸氣或液體流與下降的液體流接觸。通常此些轉移表面被定義於設置以促進兩個流體相之間的緊密接觸之隨機或規整填料的一或多個區域或床內。其結果是,增強兩相之間轉移的質量及熱的速率及/或程度。 The mass transfer tower is arranged to contact two liquid flows with different characteristics from each other, enabling mass and / or heat to be exchanged between different phases. The term "mass transfer tower" as used in this article is not intended to limit a tower in which mass transfer is the main purpose of the treatment of the liquid stream in the tower, but also to cover the heat transfer therein, not the mass transfer as Tower of the main purpose of the aforementioned treatment. Some mass transfer towers, such as those used in multi-component distillation and absorption applications, contact liquid or gas streams with a liquid stream, while others, such as extraction towers, can be designed to promote contact between two liquid phases of different densities . The mass transfer tower is arranged to contact a rising vapor or liquid stream with a falling liquid stream, typically along a plurality of mass transfer surfaces provided in the tower. Usually such transfer surfaces are defined in one or more regions or beds of random or structured packing arranged to promote intimate contact between two fluid phases. As a result, the quality and rate and / or extent of heat transfer between the two phases is enhanced.

為了確保在質量轉移塔內的兩個流體相之間的最大接觸,下降的液相當其從塔的上層區域進入填料床時必須均勻地分佈。不均勻的分 佈減小了兩相之間的接觸,並破壞了液體/蒸氣或液體/液體沿塔的剖面的比例,該比例在塔的正常運作過程中應保持實質上的恆定。各種液體分配器以均勻地分佈跨越填料床的上表面的液體為目的而設計,同時仍提供低的壓降、最小的阻塞、及廣的表現窗口。 To ensure maximum contact between the two fluid phases in the mass transfer column, the descending liquid must be distributed evenly as it enters the packed bed from the upper area of the column. Uneven points The cloth reduces the contact between the two phases and destroys the ratio of liquid / vapor or liquid / liquid along the cross section of the tower, which ratio should be kept substantially constant during the normal operation of the tower. Various liquid distributors are designed with the goal of uniformly distributing liquid across the upper surface of the packed bed, while still providing low pressure drop, minimal blockage, and a wide performance window.

大部分的分配器將液體運送到在多個隔開的位置上的填料的表面,被稱作滴點。事實上,滴點密度是特定分配器的分配性能的量度。此外,形成在滴點的液滴的尺寸亦相當重要。若液滴過大,滴點同樣也可能過大,且橫跨填料的表面的液體的水平分配可能會受到阻礙。若液滴過小,則液體冒著被夾帶進上升蒸氣或氣體並帶出塔外,從而減少了塔中熱量及/或質量轉移的效率。 Most dispensers carry liquid to the surface of the packing at multiple spaced locations, called the drip point. In fact, drop point density is a measure of the dispensing performance of a particular dispenser. In addition, the size of the droplets formed at the drip point is also important. If the droplet is too large, the dropping point may also be too large, and the horizontal distribution of the liquid across the surface of the filler may be hindered. If the droplets are too small, the liquid is entrained into the rising vapor or gas and taken out of the tower, thereby reducing the efficiency of heat and / or mass transfer in the tower.

因此,需要有一種液體分配器,具有提供沿一系列間隔開的滴點的每單位填料床表面的液體更均勻的分配的能力。分配器應該仍表現出理想的工作特性,如低的壓降,耐污染性及在低運轉時的性能,同時足夠強大和有彈性以被使用在各種各樣的熱量及質量轉移操作中。 Therefore, what is needed is a liquid dispenser with the ability to provide more uniform distribution of liquid per unit of packed bed surface along a series of spaced-apart drip points. The distributor should still exhibit ideal operating characteristics, such as low pressure drop, pollution resistance and performance at low operation, while being strong and flexible enough to be used in a variety of heat and mass transfer operations.

在一個態樣中,本發明涉及用於在垂直方向上延伸的處理塔中之下降液體的流量分配器。分配器包含一個中央分配構件,其包含用於接收液體流的至少一入口,及用於從中央分配構件排出液體流的一部分一或多個液體出口。分配器包含配置以接收從中央分配構件的液體出口排出的至少一部分的液體流之複數個長形側構件。長形側構件在縱向上沿著中央分配構件的長度相互間隔且包含一或多個用於自其排出液體的開口。分配器包含位置靠近長形側構件的複數個個分配槽。各分配槽包含一對長形側壁和基本上敞開的底板。長形側壁在橫向上彼此間隔開 以在其間定義液體接收空間,且液體接收空間被設置為接收從長形側構件的開口中排出的液體且排出從基本上敞開的底板接收的液體。液體接收空間的至少一部分以填料床填充,且從分配槽的敞開底板排出的液體已通過填料的至少一部分。 In one aspect, the invention relates to a flow distributor for descending liquid in a processing tower extending in a vertical direction. The dispenser includes a central distribution member including at least one inlet for receiving a liquid stream, and one or more liquid outlets for discharging a portion of the liquid stream from the central distribution member. The dispenser includes a plurality of elongated side members configured to receive at least a portion of a liquid flow discharged from a liquid outlet of a central distribution member. The elongated side members are spaced from each other along the length of the central distribution member in the longitudinal direction and contain one or more openings for discharging liquid therefrom. The distributor includes a plurality of distribution grooves located near the elongated side member. Each distribution slot includes a pair of elongated side walls and a substantially open floor. The elongated side walls are spaced from each other in the lateral direction To define a liquid receiving space therebetween, and the liquid receiving space is configured to receive liquid discharged from an opening of the elongated side member and discharge liquid received from a substantially open bottom plate. At least a portion of the liquid receiving space is filled with a packed bed, and the liquid discharged from the open floor of the distribution tank has passed through at least a portion of the packing.

在另一態樣中,本發明係關於一種質量轉移塔,係包含定義一開放內部容積之塔外部殼體、位在開放內部容積內且具有上表面的質量轉移床、及用於接收及分配液體流至質量轉移床的上表面的液體分配器。液體分配器包含至少一中央分配構件、複數個長形側構件、及複數個分配槽。長形側構件位置接近中央分配構件且在基本上垂直於中央分配構件的延伸軸之方向上延伸。分配槽位置靠近長形側構件。各分配槽包含一對橫向間隔開之長形側壁。定義在長形側壁之間的空間的至少一部分以填料填充且離開設置在分配槽內的填料的液體在離開分配槽後下降至底層質量轉移床的上表面。 In another aspect, the present invention relates to a mass transfer tower comprising a tower outer shell defining an open internal volume, a mass transfer bed located within the open internal volume and having an upper surface, and for receiving and distributing Liquid flows to the liquid distributor on the upper surface of the mass transfer bed. The liquid distributor includes at least a central distribution member, a plurality of elongated side members, and a plurality of distribution grooves. The elongated side member is located close to the central distribution member and extends in a direction substantially perpendicular to the extension axis of the central distribution member. The distribution slot is located near the elongated side member. Each distribution slot includes a pair of laterally spaced elongated sidewalls. At least a portion of the space defined between the elongated side walls is filled with a filler and the liquid leaving the filler disposed in the distribution tank drops to the upper surface of the underlying mass transfer bed after leaving the distribution tank.

然而,本發明另一實施例關於一種用於處理在質量轉移塔中流體流的方法。該方法包括以下步驟:(a)將液體流引入設置在質量轉移塔之內部容積內之液體流分配器,其中引入包含傳送液體流在第一方向上進入第一分配器構件;(b)將液體流分成二或更多之液體部份;(c)將各液體部份引入設置在垂直高度低於分配構件之分配槽,其中該引入包含在第二方向上傳送液體部份進入分配槽;(d)將引入分配槽之各液體部份傳送通過設置在分配槽中之填料床;(e)從分配槽之下部排出複數個液體流且將液體流至設置在低於液體分配器之垂直高度上之質量轉移床之上表面上;以及(f)以向上上升之流體流接觸排出在填料床之上表面之液體之至少一部分以從而使在該液體及該流體流之間之熱量及/或質量轉 移生效。 However, another embodiment of the present invention relates to a method for processing a fluid flow in a mass transfer tower. The method includes the steps of: (a) introducing a liquid flow into a liquid flow distributor disposed within an internal volume of the mass transfer tower, wherein introducing includes conveying the liquid flow into a first distributor member in a first direction; (b) introducing The liquid flow is divided into two or more liquid portions; (c) each liquid portion is introduced into a distribution trough arranged at a lower vertical height than the distribution member, wherein the introduction includes transferring the liquid portion into the distribution trough in a second direction; (d) transmitting the liquid portions introduced into the distribution tank through the packed bed provided in the distribution tank; (e) discharging a plurality of liquid streams from the lower part of the distribution tank and flowing the liquid to a level lower than the liquid distributor On the upper surface of the mass transfer bed at an altitude; and (f) contacting at least a portion of the liquid discharged on the upper surface of the packed bed with an upwardly flowing fluid so that the heat between the liquid and the fluid flow and / Or quality transfer Move takes effect.

10‧‧‧質量轉移塔 10‧‧‧mass transfer tower

12‧‧‧圓柱形外殼 12‧‧‧ cylindrical shell

14‧‧‧內部區域 14‧‧‧Internal area

16‧‧‧質量轉移床 16‧‧‧mass transfer bed

18、118、218‧‧‧分配器 18, 118, 218‧‧‧‧ Distributors

20、22‧‧‧流體入口 20, 22‧‧‧fluid inlet

24‧‧‧蒸氣入口 24‧‧‧Steam inlet

26‧‧‧蒸氣出口 26‧‧‧Steam Outlet

13、30、130、230‧‧‧中心分配構件 13, 30, 130, 230‧‧‧ Center distribution components

28、35‧‧‧液體出口 28, 35‧‧‧Liquid outlet

36、136、236‧‧‧長形側構件 36, 136, 236‧‧‧‧Long side members

38、145a、145b、245‧‧‧開口 38, 145a, 145b, 245‧‧‧ opening

36a‧‧‧上部 36a‧‧‧upper

36b‧‧‧下部 36b‧‧‧lower

40、140、240‧‧‧分配槽 40, 140, 240‧‧‧‧ Distributors

31、42a、42b、131a、131b、141a、141b、174a、174b、142a、142b、231a、241a、241b、242a、242b、286a、286b‧‧‧側壁 31, 42a, 42b, 131a, 131b, 141a, 141b, 174a, 174b, 142a, 142b, 231a, 241a, 241b, 242a, 242b, 286a, 286b

44、144、244‧‧‧液體接收空間 44,144,244‧‧‧‧Liquid receiving space

46a、46b、137a、137b、143a、143b、146a、146b、176、237a、237b‧‧‧端壁 46a, 46b, 137a, 137b, 143a, 143b, 146a, 146b, 176, 237a, 237b

48、147、148‧‧‧底板區域 48, 147, 148‧‧‧ floor area

47‧‧‧側支撐元件 47‧‧‧side support elements

49、149、249‧‧‧填料床 49, 149, 249‧‧‧ packed bed

50、150、250‧‧‧填料 50, 150, 250‧‧‧ filler

139、178‧‧‧底板 139, 178‧‧‧ floor

135a、135b、235‧‧‧出口 135a, 135b, 235‧‧‧ export

159‧‧‧對 159‧‧‧pair

170、270‧‧‧側臂分配器 170, 270‧‧‧ side arm distributor

175‧‧‧孔 175‧‧‧hole

280‧‧‧側臂片 280‧‧‧Side Arm Plate

288‧‧‧長形構件 288‧‧‧long member

288a、288b‧‧‧部分 288a, 288b ‧‧‧ part

第1圖係為具有剖開之塔殼體部分以示出根據設置在其中的本發明配置的液體分配器的一個實施例的質量轉移塔的局部側透視圖;第2圖係為第1圖中所示的液體分配器的頂部透視圖;第3圖係為第1圖及第2圖中所示的液體分配器的底部透視圖;第4圖係為第1至第3圖中所示的液體分配器,沿第2圖的線4-4在箭頭方向上截取的的頂部透視圖;第5圖係為第1至第4圖中所示的液體分配器,沿第2圖的線5-5在箭頭方向上截取的垂直剖面的頂部透視圖;第6圖係為根據本發明另一實施例配置,具有剖開之部分以示出設置在液體分配器的分配槽內的填料的液體分配器的頂部透視圖;第7圖係為第6圖中所示的液體分配器,沿第6圖的線7-7在箭頭的方向上截取的垂直截面的頂部透視圖;第8圖係為第6圖及第7圖中所示的液體分配器,沿第6圖的線8-8在箭頭的方向上截取的垂直截面的頂部透視圖;第9圖係為根據本發明的再一實施例配置的液體分配器的頂部透視圖;第10圖係為第9圖中所示的液體分配器,沿第9圖的線10-10在箭頭的方向上截取的垂直截面的頂部透視圖;以及第11圖係為在第9圖及第10圖中所示的液體分配器的分配槽 中一個的放大的局部圖,特別是示出了側臂分配器及在分配槽內的填料床的配置。 FIG. 1 is a partial side perspective view of a mass transfer tower having a section of a tower housing sectioned to show one embodiment of a liquid distributor configured according to the present invention provided therein; FIG. 2 is a view of FIG. 1 Top perspective view of the liquid dispenser shown in Figure 3; Figure 3 is a bottom perspective view of the liquid dispenser shown in Figures 1 and 2; Figure 4 is shown in Figures 1 to 3 The top view of the liquid dispenser taken along the line 4-4 of Figure 2 in the direction of the arrow; Figure 5 is the liquid dispenser shown in Figures 1 to 4, along the line of Figure 2 5-5 is a top perspective view of a vertical section taken in the direction of an arrow; FIG. 6 is a configuration according to another embodiment of the present invention, with a section cut away to show the packing provided in the distribution tank of the liquid distributor Top perspective view of the liquid distributor; FIG. 7 is a top perspective view of the vertical section of the liquid distributor shown in FIG. 6, taken along the line 7-7 of FIG. 6 in the direction of the arrow; FIG. 8 It is a liquid distributor shown in Figs. 6 and 7 in a vertical section taken along the line 8-8 of Fig. 6 in the direction of the arrow. Top perspective view; FIG. 9 is a top perspective view of a liquid dispenser configured according to yet another embodiment of the present invention; and FIG. 10 is a liquid dispenser shown in FIG. 9, along line 10 of FIG. -10 is a top perspective view of a vertical section taken in the direction of an arrow; and FIG. 11 is a distribution tank of the liquid distributor shown in FIGS. 9 and 10 An enlarged partial view of one of them, in particular showing the configuration of a side arm distributor and a packed bed in a distribution tank.

現在轉到附圖,更詳細地且從第1圖開始,質量轉移塔整體是由元件符號10表示且包含直立的圓柱形外殼12,圓柱形外殼12定義了一個開放的內部區域14,在內部區域14中,二或多個液體流處在逆流或順流的關係。在質量轉移塔10中的流體流之間接觸的至少一部分是在一或多個在內部區域14中沿質量轉移塔10的高度的垂直位置設置的質量轉移床16中進行。質量轉移床16可以包含任何類型的填料,包含規整(structured)填料、隨機(random)填料、及其組合。質量轉移塔10還包含至少一個液體分配器18,液體分配器18設置在質量轉移床16的上方且用於促進在質量轉移塔10內的一或多個下降液體流更均勻的水平分配。 Turning now to the drawings, starting in more detail and starting from Figure 1, the mass transfer tower as a whole is represented by the element symbol 10 and contains an upright cylindrical shell 12, which defines an open inner area 14, in the interior In zone 14, two or more liquid flows are in a countercurrent or cocurrent relationship. At least a portion of the contact between the fluid streams in the mass transfer tower 10 is performed in one or more mass transfer beds 16 disposed in the inner region 14 along a vertical position along the height of the mass transfer tower 10. The mass transfer bed 16 may contain any type of packing, including structured packing, random packing, and combinations thereof. The mass transfer tower 10 also includes at least one liquid distributor 18 disposed above the mass transfer bed 16 and used to facilitate a more uniform horizontal distribution of one or more descending liquid streams within the mass transfer tower 10.

質量轉移塔10可以是任何適合類型的製程塔,係設置以接觸兩個液體流,以便獲得分餾產物及/或以其他方式造成不同相之間的質量轉移及/或熱量轉移。例如,在質量轉移塔10中可發生原油常壓分餾(crude atmospheric)、潤滑油真空分餾(lube vacuum)、原油真空分餾(crude vacuum)、流體或熱裂解分餾(fluid or thermal cracking fractionating)、焦化或減粘裂化分餾(coker or visbreaker fractionating)、焦炭洗滌(coke scrubbing)、反應器廢氣洗滌(reactor off-gas scrubbing)、氣淬(gas quenching)、食用油除臭(edible oil deodorization)、污染控制洗滌、以及其他流程。質量轉移塔10可為配置以接觸一或多個上升蒸氣流與下降液體流之汽-液塔、配置以接觸一或多個上升氣體流與下降液體流的氣- 液塔、或配置以促進不同密度的上升及下降液體流之間的相互接觸的液-液塔。雖然在第1圖中大致描繪的是包含圓柱形、縱長殼體,包含多邊形之其他形狀可被使用作為質量轉移塔10。質量轉移塔10是任何合適的直徑和高度且由對於質量轉移塔10的操作過程中存在的流體及條件理想的為惰性或反之與其兼容的一或多種的剛性材料。 The mass transfer column 10 may be any suitable type of process column configured to contact two liquid streams in order to obtain fractionated products and / or otherwise cause mass transfer and / or heat transfer between different phases. For example, crude atmospheric pressure, lube vacuum, crude vacuum, fluid or thermal cracking fractionating, coking can occur in the mass transfer tower 10 Coker or visbreaker fractionating, coke scrubbing, reactor off-gas scrubbing, gas quenching, edible oil deodorization, pollution control Washing, and other processes. The mass transfer column 10 may be a vapor-liquid column configured to contact one or more rising vapor streams and falling liquid streams, and a gas-liquid column configured to contact one or more rising gas streams and falling liquid streams. Liquid towers, or liquid-liquid towers configured to promote contact between rising and falling liquid streams of different densities. Although it is roughly depicted in FIG. 1 as including a cylindrical, elongated shell, other shapes including a polygon may be used as the mass transfer tower 10. The mass transfer tower 10 is any one or more rigid materials of any suitable diameter and height and made of fluids and conditions that are ideally inert or otherwise compatible with the fluids and conditions present during operation of the mass transfer tower 10.

如第1圖所示,質量轉移塔10可包含用於引入流體流進入質量轉移塔10的內部區域14流體入口20及22。引入質量轉移塔10的流體入口20及22的流體流可包含主要液體流,主要是蒸汽流,或合併的蒸氣或液體流。典型地,引入流體入口22的流是液體流,同時透過流體入口20進入質量轉移塔10的流體流可為蒸氣流、液體流、或蒸氣及液體流的組合。質量轉移塔10也可包含用於將主要蒸氣流引入質量轉移塔10的下部之蒸氣入口24。雖然第1圖中示出僅包含二流體入口20及22以及單一蒸氣入口24,其應被理解的是,根據特定應用之需要或期望,質量轉移塔10可包含任何適合數量的流體或蒸氣入口,適當地沿質量轉移塔10的高度放置。 As shown in FIG. 1, the mass transfer tower 10 may include fluid inlets 20 and 22 for introducing a fluid stream into the interior region 14 of the mass transfer tower 10. The fluid streams introduced into the fluid inlets 20 and 22 of the mass transfer tower 10 may comprise a primary liquid stream, primarily a vapor stream, or a combined vapor or liquid stream. Typically, the flow introduced into the fluid inlet 22 is a liquid flow, while the fluid flow entering the mass transfer tower 10 through the fluid inlet 20 may be a vapor flow, a liquid flow, or a combination of vapor and liquid flows. The mass transfer tower 10 may also include a steam inlet 24 for introducing a main vapor stream into the lower portion of the mass transfer tower 10. Although shown in FIG. 1 as including only two fluid inlets 20 and 22 and a single vapor inlet 24, it should be understood that the mass transfer tower 10 may contain any suitable number of fluid or vapor inlets as needed or desired for a particular application. Place appropriately along the height of the mass transfer tower 10.

質量轉移塔10進一步包含用於將蒸氣產物從質量轉移塔10的上部排出的塔頂蒸氣出口26及液體產物流可從其提取之下部液體出口28。其他傳統的塔構件,例如回流管道(reflux stream lines)、重沸器(reboilers)、冷凝器、蒸氣笛(vapor horns)以及其他相似物亦可存在於質量轉移塔10中,但因為這些構件係習知且認為對於理解本發明是不必要的,故未繪示於此。 The mass transfer column 10 further includes an overhead vapor outlet 26 for discharging vapor products from the upper portion of the mass transfer column 10 and a lower liquid outlet 28 from which a liquid product stream can be extracted. Other traditional tower components, such as reflux stream lines, reboilers, condensers, vapor horns, and other similar objects may also be present in the mass transfer tower 10, but because these components are It is known and considered unnecessary for understanding the present invention, so it is not shown here.

另請參閱第2圖至第5圖,根據本發明之一實施例配置的液體分配器18將被描述。液體分配器18為管道或梯子型的分配器,包含沿 質量轉移塔10的直徑或弦水平延伸的至少一中央分配構件30,或至少其之一部份。在第2圖至第5圖中描繪的一實施例中的中央分配構件30,可包含具有實質上圓柱形的側壁31的拉長的管道構件。也可考慮具有包含多邊形之其他剖面形狀之中央分配構件30。此外,雖然如第2圖至第5圖所示僅包含一中央分配構件30,包含二或多個中央分配構件30的液體分配器18也完全在本發明的範疇內。 Referring also to FIGS. 2 to 5, a liquid dispenser 18 configured according to one embodiment of the present invention will be described. The liquid distributor 18 is a pipe or ladder type At least one central distribution member 30, or at least a portion thereof, of which the diameter or chord of the mass transfer tower 10 extends horizontally. The central distribution member 30 in an embodiment depicted in FIGS. 2 to 5 may include an elongated duct member having a substantially cylindrical side wall 31. It is also conceivable to have a central distribution member 30 having other cross-sectional shapes including a polygon. In addition, although only one central distribution member 30 is included as shown in FIGS. 2 to 5, the liquid distributor 18 including two or more central distribution members 30 is also fully within the scope of the present invention.

中央分配構件30包含用於接收在其中的液體流之至少一個液體入口。當液體通過中央分配構件30,其劃分成複數個較小的液體部份,複數個較小的液體部份接著透過一或多個液體出口35從中央分配構件30中被排出。如在第4圖中特定地示出,液體出口35可為任何所需的形狀,如圓形、三角形、或甚至垂直拉長,且沿中央分配構件30的長度彼此以預定距離間隔隔開。液體出口35確實的數量及尺寸不特別受限且可被選擇以配合通過液體分配器18之液體的預期的流率。 The central distribution member 30 contains at least one liquid inlet for receiving a liquid flow therein. When the liquid passes through the central distribution member 30, it is divided into a plurality of smaller liquid portions, and the plurality of smaller liquid portions are then discharged from the central distribution member 30 through one or more liquid outlets 35. As specifically shown in FIG. 4, the liquid outlets 35 may be of any desired shape, such as circular, triangular, or even vertically elongated, and spaced apart from each other by a predetermined distance along the length of the central distribution member 30. The exact number and size of the liquid outlets 35 are not particularly limited and can be selected to match the expected flow rate of liquid through the liquid distributor 18.

從中央分配構件30通過液體出口35排出的個別的液體流被送入複數個長形側構件36,其沿中央分配構件30的長度縱向的分隔且以一般的角方向從其向外延伸。長形側構件36通常是基本上互相平行並相對於中央分配構件30的中心軸37形成在約30°至150°、約45°至約135°、或約60°至約120°的範圍內的角度。優選地,但不一定要,各長形側構件可基本上垂直於中央分配構件30的延伸中心軸37延伸,如第2圖至第5圖中所示。如本文中所用,用語「基本上」指在5°以內,使得是「基本上垂直的」的元件是在垂直的5°以內。任何數量的長形側構件36可被選擇以便達成所需的滴點密度進入底層的質量轉移床。 The individual liquid flows discharged from the central distribution member 30 through the liquid outlet 35 are sent to a plurality of elongated side members 36 which are longitudinally partitioned along the length of the central distribution member 30 and extend outwardly therefrom in a general angular direction. The elongated side members 36 are generally substantially parallel to each other and are formed in a range of about 30 ° to 150 °, about 45 ° to about 135 °, or about 60 ° to about 120 ° with respect to the central axis 37 of the central distribution member 30. Angle. Preferably, but not necessarily, each of the elongated side members may extend substantially perpendicular to the extension central axis 37 of the central distribution member 30, as shown in FIGS. 2 to 5. As used herein, the term "substantially" means within 5 ° such that an element that is "substantially vertical" is within 5 ° vertical. Any number of elongated side members 36 may be selected to achieve the desired drop point density into the underlying mass transfer bed.

中央分配構件30可被以在長形側構件36上的關係設置,如第 2圖至第5圖所示,或,以可替代地,中央分配構件30及長形側構件36可以共平面的關係進行配置,其中中央分配構件30及長形側構件36位在大致相同的垂直高度。當各長形側構件36包含分離的上部36a及下部36b,如第2圖至第5圖中所示,上部36a(或下部36b,未示出於實施例中)中的其中之一可與中央分配構件30以共平面的關係設置,同時下部36b(或上部36a,未示出於實施例中)可被設置在較中央分配構件30低的垂直高度。此外,上部36a及下部36b皆可駐留在基本上相同於中央分配構件30的垂直高度上。 The central distribution member 30 may be provided in a relationship on the elongated side member 36, such as As shown in FIG. 2 to FIG. 5, or alternatively, the central distribution member 30 and the elongated side member 36 may be arranged in a coplanar relationship, where the central distribution member 30 and the elongated side member 36 are located at substantially the same position. Vertical height. When each of the elongated side members 36 includes a separate upper portion 36a and a lower portion 36b, as shown in Figs. 2 to 5, one of the upper portion 36a (or the lower portion 36b, not shown in the embodiment) may be combined with The central distribution member 30 is disposed in a coplanar relationship, while the lower portion 36b (or the upper portion 36a, not shown in the embodiment) may be disposed at a lower vertical height than the central distribution member 30. In addition, both the upper portion 36a and the lower portion 36b may reside at substantially the same vertical height as the central distribution member 30.

如特別在第5圖中示出的,各長形側構件36包含用於從長形側構件36排出液體且進入一或多個分配槽40的複數個開口38,其位在靠近但低於長形側構件36的垂直高度的位置。開口38沿長形側構件36的底部設置,但,額外的或可替代地,一或多個開口38也可位在至少一長形側構件36的側壁的下部之中。在第2圖至第5圖中描繪的實施例中,分配槽40相對於長形側構件36以平行方向排列,但基本上垂直於中央分配構件30定向。此外,在第2圖至第5圖中描繪的實施例中,長形側構件36比分配槽40的比例為1:1,使得各長形側構件被配置以饋送單一的分配槽40。 As shown particularly in FIG. 5, each of the elongated side members 36 includes a plurality of openings 38 for discharging liquid from the elongated side members 36 and entering one or more distribution grooves 40, which are located near but below The vertical height position of the elongated side member 36. The openings 38 are provided along the bottom of the elongated side member 36, but in addition or alternatively, one or more openings 38 may also be positioned in the lower portion of the sidewall of the at least one elongated side member 36. In the embodiments depicted in FIGS. 2 to 5, the distribution grooves 40 are aligned in parallel with respect to the elongated side member 36, but are oriented substantially perpendicular to the central distribution member 30. Further, in the embodiments depicted in FIGS. 2 to 5, the ratio of the elongated side members 36 to the distribution groove 40 is 1: 1, so that each of the elongated side members is configured to feed a single distribution groove 40.

各分配槽40包含一對長形側壁42a及42b,彼此橫向隔開且在其間定義液體接收空間44。液體接收空間44被配置以接收從長形側構件36的開口38排出的液體的至少一部分。分配槽40還包含一對相對的端壁46a及46b以及在側壁42a及42b之間延伸的基本上開放的底板區域48。如第3圖所示,各分配槽可包含沿分配槽40的長度間隔的一或多個側支撐元件47,其餘的底板區域48被開放且配置以排出離開各 分配槽40之液體。側支撐元件47的數量及間隔部份取決於構成材料及液體分配器18預期的作用,但也可藉由設置在分配槽40的液體接收空間44中的填料的類型及尺寸決定。 Each distribution tank 40 includes a pair of elongated side walls 42a and 42b that are laterally spaced from each other and define a liquid receiving space 44 therebetween. The liquid receiving space 44 is configured to receive at least a portion of the liquid discharged from the opening 38 of the elongated side member 36. The distribution slot 40 also includes a pair of opposing end walls 46a and 46b and a substantially open floor area 48 extending between the side walls 42a and 42b. As shown in FIG. 3, each distribution slot may include one or more side support elements 47 spaced along the length of the distribution slot 40, and the remaining floor area 48 is opened and configured to discharge away from each Liquid in the distribution tank 40. The number and spacing of the side support elements 47 depend in part on the materials and the intended function of the liquid distributor 18, but can also be determined by the type and size of the fillers provided in the liquid receiving space 44 of the distribution tank 40.

根據本發明,至少一部分,或每個分配槽40包含設置在液體接收空間44內的填料50的填料床49。當液體被引入液體接收空間44內,在透過底板區域48離開分配槽40之前,其向下通過填料50。饋送進入分配槽40之中之所有液體,或其之至少大部分,在被從液體分配器18排出且到底層的質量轉移床16(第1圖)上之前通過填料50的填料床49。功能性的,當液體通過各分配槽40流向下時,填料50的填料床49增強了液體的水平散佈。 According to the invention, at least a part, or each distribution tank 40 contains a packed bed 49 of packing 50 arranged in the liquid receiving space 44. When liquid is introduced into the liquid receiving space 44, it passes downward through the packing 50 before leaving the distribution tank 40 through the floor area 48. All the liquid fed into the distribution tank 40, or at least most of it, passes through the packed bed 49 of the packing 50 before being discharged from the liquid distributor 18 and onto the bottom mass transfer bed 16 (FIG. 1). Functionally, the packing bed 49 of the packing 50 enhances the horizontal spreading of the liquid as the liquid flows downward through each distribution tank 40.

在分配槽40中使用的填料50可為任何適合的填料種類,包含規整填料、隨機填料、及其組合。當填料50包含規整填料,如在第2圖至第5圖中大致地示出的,填料床49可包含二或多個(或至少三個)垂直延伸的波紋狀或網狀填料的片材。規整填料50的傾斜角度及捲曲尺寸可取決於散佈的液率與所需的程度而變化。填料可為織物或非織物且也可以或不可以為穿孔的。優選的,在填料床49中的填料50的下部邊緣的至少一部分是鋸齒狀的以產生鋸齒狀滴流邊緣且防止液體聚集在液體分配器18的下部。在填料床49內的填料50的片材的垂直方向產生排出跨越底層質量轉移床的表面液體的「線」,此些跨越底層質量轉移床的表面間隔之平行滴灌區提昇了來自分配器18的液體的分配均勻度。 The filler 50 used in the distribution tank 40 may be any suitable filler type, including structured filler, random filler, and combinations thereof. When the packing 50 contains structured packing, as shown generally in Figures 2 to 5, the packing bed 49 may contain two or more (or at least three) sheets of corrugated or mesh packing extending vertically . The angle of inclination and the size of the curl of the structured packing 50 may vary depending on the dispersion rate and the desired degree. The filler may be woven or non-woven and may or may not be perforated. Preferably, at least a portion of the lower edge of the packing 50 in the packing bed 49 is jagged to generate a jagged drip stream edge and prevent liquid from collecting in the lower portion of the liquid distributor 18. In the vertical direction of the sheet of filler 50 in the packed bed 49, a "line" is discharged that discharges the liquid across the surface of the underlying mass transfer bed. These parallel drip irrigation zones across the surface of the underlying mass transfer bed enhance the Even distribution of liquid.

現在轉到第6圖至第8圖,說明根據本發明另一實施例配置的液體分配器118。如第6圖至第8圖,液體分配器118包含槽狀的中央 分配構件130,中央分配構件130包含於實質上水平方向延伸之一對橫向地間隔的長形側壁131a及131b。長形側壁131a及131b藉由底板139連接在底部且藉由端壁137a及137b連接在端部。可選擇的,蓋體(未示出)可基本上覆蓋沿中央分配構件130的頂端的所有開放區域或至少一部分開放區域,取決於其中將使用液體分配器118的特定應用。雖然如示出僅包含單一分配構件130,也可構想出具有二或多個中央分配構件130或更多的實施例並落入本發明的範圍之內。 Turning now to FIGS. 6 to 8, a liquid dispenser 118 configured according to another embodiment of the present invention will be described. As shown in FIGS. 6 to 8, the liquid distributor 118 includes a groove-shaped center. The distribution member 130 and the central distribution member 130 include a pair of laterally spaced elongated side walls 131a and 131b extending in a substantially horizontal direction. The elongated side walls 131a and 131b are connected to the bottom by the bottom plate 139 and connected to the ends by the end walls 137a and 137b. Alternatively, the cover (not shown) may cover substantially all or at least a portion of the open area along the top end of the central distribution member 130, depending on the particular application in which the liquid dispenser 118 is to be used. Although shown as including only a single distribution member 130, embodiments having two or more central distribution members 130 or more are also contemplated and fall within the scope of the present invention.

中央分配構件130包含用於接收液體流的液體入口(未示出)及定義在中央分配構件130的側壁131a及131b中之用於從其排出液體之複數個液體出口135a及135b。在替代方案中,一或多個出口135a及135b可被沿中央分配構件130的底板139的長度定義。相似於先前詳細描述的液體分配器18,液體分配器118進一步包含從中央分配構件130在向外之方向上延伸的複數個長形側構件136。優選的,長形側構件136係垂直於中央分配構件130定向,如第6圖至第8圖中所示。液體分配器118之長形側構件136包含長形槽而非管道構件,長形槽各包含經由底板147於底部彼此連結及藉由一對端壁143a及143b連接在端部之一對橫向間隔開的長形側壁141a及141b。雖然於第6圖至第8圖中示出具有兩個通常為長方形之長形側構件136,液體分配器118可包含任何數量之具有包含半圓柱形或多邊形之任何剖面形狀之長形側構件136。 The central distribution member 130 includes a liquid inlet (not shown) for receiving a liquid flow and a plurality of liquid outlets 135a and 135b defined in the side walls 131a and 131b of the central distribution member 130 for discharging liquid therefrom. In the alternative, one or more of the outlets 135a and 135b may be defined along the length of the bottom plate 139 of the central distribution member 130. Similar to the liquid dispenser 18 described in detail previously, the liquid dispenser 118 further includes a plurality of elongated side members 136 extending from the central distribution member 130 in an outward direction. Preferably, the elongated side member 136 is oriented perpendicular to the central distribution member 130, as shown in Figs. 6 to 8. The elongated side member 136 of the liquid distributor 118 includes an elongated groove instead of a pipe member, each of which includes a pair of lateral spaces connected to each other via a bottom plate 147 at the bottom and connected to one end by a pair of end walls 143a and 143b. Open elongated side walls 141a and 141b. Although shown in FIGS. 6 to 8 with two generally rectangular elongated side members 136, the liquid dispenser 118 may include any number of elongated side members having any cross-sectional shape including a semi-cylindrical or polygonal shape 136.

在如先前所描述的類似方式,中央分配構件130可以被佈置在相對於所述長形側構件136之上,如第6圖至第8圖中所示,或者,可替換地,可以共平面的位置設置,使中央分配構件130和長形側構件136 基本上處於同一水平面上。如具體顯示於第7圖,每個長形側構件136包括多個開口145a,多個開口145a定義於相應的側壁141a和141b,配置以從每個長形側構件136排出液體至一個或多個下方之分配槽140。 In a similar manner as previously described, the central distribution member 130 may be arranged above the elongated side member 136, as shown in Figures 6 to 8, or, alternatively, may be coplanar Position so that the central distribution member 130 and the elongated side member 136 Basically on the same horizontal plane. As specifically shown in FIG. 7, each of the elongated side members 136 includes a plurality of openings 145a, which are defined on the respective side walls 141a and 141b, and are configured to discharge liquid from each of the elongated side members 136 to one or more Lower distribution slot 140.

在第6圖至第8圖中所示的液體分配器118以垂直結構佈置,使得分配槽140以實質上垂直於相對於長形側構件136的延伸方向之方向延伸。因此,每個長形側構件136配置以通過沿每個長形側構件136之對置的側壁141a和141b的長度縱向間隔設置的排出開口145a和145b饋送至少兩個不同的分配槽140。如第6圖至第8圖所示,開口145a和145b以橫向間隔成對159設置,成對159中之一個開口145a係由側壁141a定義且成對159中之另一個開口145b係由相對的側壁141b定義。每個成對159之開口145a和145b可直接彼此對面地間隔,或開口145a與145b中的一個可自另一開口145b或145a水平和/或垂直方向地偏移(實施例中未示出)。儘管示出為定義於側壁部141a、141b之下部,一個或多個開口145a或145b亦可定義於側壁141a和141b內不同的位置或定義於長形側構件136之底板147中。 The liquid distributor 118 shown in FIGS. 6 to 8 is arranged in a vertical structure so that the distribution groove 140 extends in a direction substantially perpendicular to the extending direction with respect to the elongated side member 136. Therefore, each of the elongated side members 136 is configured to feed at least two different distribution grooves 140 through the discharge openings 145 a and 145 b which are longitudinally spaced along the length of the side walls 141 a and 141 b opposed to each of the elongated side members 136. As shown in FIGS. 6 to 8, the openings 145 a and 145 b are arranged in pairs 159 at lateral intervals. One opening 145 a in the pair 159 is defined by the side wall 141 a and the other opening 145 b in the pair 159 is opposed. The side wall 141b is defined. The openings 145a and 145b of each pair 159 may be directly opposite to each other, or one of the openings 145a and 145b may be horizontally and / or vertically offset from the other opening 145b or 145a (not shown in the embodiment). . Although shown as being defined below the side wall portions 141a, 141b, one or more openings 145a or 145b may also be defined in different positions within the side walls 141a and 141b or in the bottom plate 147 of the elongated side member 136.

當以垂直排列配置,如第6圖至第8圖中所示,成對159的各開口145a和145b可配置以饋送同一分配槽140。成對159之開口145a和145b的數目通常對應於配置以饋送每長形側構件136之分配槽140的數目。此外,一個以上的長形側構件136也可以被配置以饋送相同的分配槽146,如大致顯示於第6圖至第8圖。根據尺寸和特定的塔操作,合適地,至少兩個,至少三個,或至少四個長形側構件136可以被配置以饋送單一個分配槽146。 When arranged in a vertical arrangement, as shown in FIGS. 6 to 8, the openings 145 a and 145 b of the pair 159 may be arranged to feed the same distribution slot 140. The number of openings 145a and 145b of the pair 159 generally corresponds to the number of distribution slots 140 configured to feed each elongated side member 136. In addition, one or more elongated side members 136 may be configured to feed the same distribution groove 146 as shown generally in FIGS. 6 to 8. Depending on the size and particular tower operation, suitably at least two, at least three, or at least four elongated side members 136 may be configured to feed a single distribution slot 146.

液體分配器118還可包括用以促進長形側構件136和分配槽140之間的液體的流動之多個側臂分配器170。如第6圖至第8圖所示,側臂分配器170包括一對間隔開的側壁部174a和174b,及設置在側臂分配器170的外端的單個端壁176。長形側構件136的側壁141a和141b與側臂分配器170的側壁部174a及174b在其另一端連接。通常情況下,如第8圖所示,側臂分配器170在頂部開口,並包括底板178,底板178用於允許液體從長形側構件136流入每個分配槽140。如第8圖所示,各個側臂分配器170的底板178包括用於將液體排出至分配槽140的多個孔175。每個側臂分配器170用以使排出側臂分配器170之液體在大致垂直於每個分配槽140的延伸方向的方向散佈遍及分配槽140。在底板178中定義的孔175(或,可替代的,在側壁174a及174b的下部)為了提供需要的量的液體到分配槽140,以一預定距離間隔開,且在槽140內期望的位置。 The liquid distributor 118 may further include a plurality of side arm distributors 170 to facilitate the flow of liquid between the elongated side member 136 and the distribution tank 140. As shown in FIGS. 6 to 8, the side arm distributor 170 includes a pair of spaced apart side wall portions 174 a and 174 b, and a single end wall 176 provided at an outer end of the side arm distributor 170. The side walls 141 a and 141 b of the elongated side member 136 are connected to the side walls 174 a and 174 b of the side arm distributor 170 at the other ends thereof. Generally, as shown in FIG. 8, the side arm distributor 170 is opened at the top and includes a bottom plate 178 for allowing liquid to flow from the elongated side member 136 into each of the distribution grooves 140. As shown in FIG. 8, the bottom plate 178 of each side arm distributor 170 includes a plurality of holes 175 for discharging liquid to the distribution tank 140. Each side arm distributor 170 is used to spread the liquid discharged from the side arm distributor 170 throughout the distribution groove 140 in a direction substantially perpendicular to the extending direction of each distribution groove 140. The holes 175 defined in the bottom plate 178 (or, alternatively, the lower portions of the side walls 174a and 174b) are spaced at a predetermined distance to provide the required amount of liquid to the distribution tank 140, and at desired positions within the tank 140 .

如第6圖至第8圖中所示,每個分配槽140包括彼此橫向間隔開的一對長形側壁142a和142b,以限定其間的液體接收空間144。分配槽140還包括設置在液體接收空間144的大致相對的兩端的一對端壁146a及146b。分配槽140的頂部是開放的,且底板區域148也可以是基本上敞開的,除了用於維持分配槽140的形狀及/或支撐在其中的填料之在沿著槽的長度以預先決定的距離在側壁142a及142b之間延伸的一些側向支架(未示出)。 As shown in FIGS. 6 to 8, each distribution groove 140 includes a pair of elongated side walls 142 a and 142 b laterally spaced from each other to define a liquid receiving space 144 therebetween. The distribution tank 140 further includes a pair of end walls 146 a and 146 b provided at substantially opposite ends of the liquid receiving space 144. The top of the distribution tank 140 is open, and the bottom plate area 148 may also be substantially open, except for maintaining the shape of the distribution tank 140 and / or the filler supported therein at a predetermined distance along the length of the tank. Some lateral supports (not shown) extend between the side walls 142a and 142b.

如第6圖至第8圖中所示,液體分配器118還包括設置在液體接收空間144內的填料150的填料床149。填料床149被配置使得液體在離開實質上開放的分配槽140的底板區域148之前,通過填料150中 的至少一部分饋送進入分配槽140。如上所述,填料150可以是規整或隨機填料,並且可以包括金屬絲網或紗布型填料,如概括地描繪在第6圖至第8圖中。或者,任何先前描述的其他類型的填料或填充安排也可以用在分配槽140中。類似於液體分配器18,分配器118的分配槽140是包括填料150的分配器118的唯一組件。中央分配構件130及長形側構件136兩者定義實質上中空的液體收容空間,該液體收容空間不包含任何類型的填料設置在其中。 As shown in FIGS. 6 to 8, the liquid distributor 118 further includes a packing bed 149 of the packing 150 provided in the liquid receiving space 144. Packed bed 149 is configured such that the liquid passes through the packing 150 before leaving the floor area 148 of the substantially open distribution tank 140. At least a portion of the feed is fed into the distribution tank 140. As described above, the filler 150 may be a regular or random filler, and may include a wire mesh or gauze-type filler, as generally depicted in FIGS. 6 to 8. Alternatively, any other type of filler or filling arrangement previously described may be used in the distribution tank 140. Similar to the liquid distributor 18, the distribution tank 140 of the distributor 118 is the only component of the distributor 118 that includes the filler 150. Both the central distribution member 130 and the elongated side member 136 define a substantially hollow liquid storage space, and the liquid storage space does not include any type of filler disposed therein.

現在轉到第9圖至第11圖,液體分配器118的變型,被表示為液體分配器218,被示為包括中央分配構件230及靠近,但高於長形分配槽240的垂直高度設置的複數個長形側構件236。如先前第6圖至第8圖中所示的實施例所為之描述,中央分配構件230包括具有一對側壁231a及231b、一對相對的端壁237a和237b、以及複數個液體出口235的開放端槽,用於饋送容納到中央分配構件230中的液體進入到各長形側構件236中。中央分配構件230可以被放置在比各長形側構件236更高的垂直高度,如約略地在第9圖及第10圖中所示,但是其中中央分配構件230及長形側構件236配置在共平面配置之實施例也在本發明設想的範圍之內。 Turning now to FIGS. 9 to 11, a modification of the liquid distributor 118 is shown as a liquid distributor 218, and is shown as including a central distribution member 230 and a close, but higher vertical height than the elongated distribution slot 240. A plurality of elongated side members 236. As described in the previous embodiments shown in FIGS. 6 to 8, the central distribution member 230 includes an opening having a pair of side walls 231a and 231b, a pair of opposite end walls 237a and 237b, and a plurality of liquid outlets 235 End grooves for feeding the liquid accommodated in the central distribution member 230 into each of the elongated side members 236. The central distribution member 230 may be placed at a higher vertical height than each of the elongated side members 236, as shown approximately in Figs. 9 and 10, but the central distribution member 230 and the elongated side members 236 are disposed at Embodiments of a coplanar configuration are also within the scope of the present invention.

在第9圖至第11圖中所示之液體分配器218被配置成平行排列,使得分配槽240在基本平行相對於長形側構件236延伸方向的方向延伸。各長形側構件236被配置為饋送二或多個不同的分配槽240,但各分配槽240係從單一個長形側構件236饋送。然而,當平行排列配置如第9圖及第10圖所示,設置在給定的側壁241a或241b的其中之一的排放開口可被配置以饋送液體進入單一個分配槽240,如第9圖及第 10圖中所示。因此,在這種配置中,各分配槽240被配置成從單一個長形側構件236接收液體。 The liquid distributors 218 shown in FIGS. 9 to 11 are arranged in parallel so that the distribution grooves 240 extend in a direction substantially parallel to the extending direction of the elongated side member 236. Each elongated side member 236 is configured to feed two or more different distribution slots 240, but each distribution slot 240 is fed from a single elongated side member 236. However, when the parallel arrangement is shown in FIGS. 9 and 10, the discharge opening provided on one of the given side walls 241a or 241b may be configured to feed liquid into a single distribution tank 240, as shown in FIG. 9 And first Figure 10 shows. Therefore, in this configuration, each distribution tank 240 is configured to receive liquid from a single elongated side member 236.

在長形側構件236和分配槽240之間的液體流,也可被定位於靠近每個排放開口245的複數個側臂分配器270促進。適合於使用在本實施例中的側臂分配器270,在第11圖中提供的特寫圖特別示出且包含頂部開放的長形構件288,具有相對的側壁288a及288b,其延伸通過分配槽240的側壁242b並進入液體接收空間244。長形構件的一部分288a可被定位在比長形構件的另一部分288b更低的垂直高度,從而給予側臂分配器270大致為階梯狀之輪廓。當液體從長形側構件236的排放開口245通過,其進入長形構件288且穿過側壁242b進入分配槽240的液體接收空間244。此後,液體在通過底板區域(未示出)排出分配槽240之前,通過填料250的填料床249下降。分配槽240可藉由側臂分配器270經由從長形構件288的上邊緣水平地延伸的側臂片280物理性的連接到長形側構件236,且被配置用於插入到在分配槽240的側壁242a內的對應槽。此附接部件是例示性的,且其他裝置或結構可以在本發明的範圍內被使用。 The liquid flow between the elongated side member 236 and the distribution tank 240 may also be facilitated by a plurality of side arm distributors 270 positioned close to each discharge opening 245. Suitable for use with the side arm distributor 270 in this embodiment, the close-up view provided in Figure 11 is particularly shown and includes an elongated member 288 with an open top, with opposing side walls 288a and 288b, which extend through the distribution slot The side wall 242b of 240 also enters the liquid receiving space 244. One portion 288a of the elongated member may be positioned at a lower vertical height than the other portion 288b of the elongated member, thereby giving the side arm distributor 270 a substantially stepped profile. When the liquid passes through the discharge opening 245 of the elongated side member 236, it enters the elongated member 288 and passes through the side wall 242b into the liquid receiving space 244 of the distribution groove 240. Thereafter, the liquid falls through the packing bed 249 of the packing 250 before being discharged out of the distribution tank 240 through a floor area (not shown). The distribution slot 240 may be physically connected to the elongated side member 236 by a side arm distributor 270 via a side arm piece 280 extending horizontally from the upper edge of the elongated member 288 and configured to be inserted into the distribution slot 240. Corresponding grooves in the sidewall 242a. This attachment member is exemplary, and other devices or structures may be used within the scope of the present invention.

如第9圖至第11圖所示,液體分配器218示出為在填料250的填料床249中利用隨機填料。另外或在替代方案中,規整或金屬絲網填料,也可以使用,並且對於填料250的細節類似於前面所述。 As shown in FIGS. 9 to 11, the liquid distributor 218 is shown to utilize random packing in a packed bed 249 of the packing 250. Additionally or in the alternative, structured or wire mesh fillers may be used, and the details of the filler 250 are similar to those previously described.

再次參考第1圖,當下降的液體從液體分配器18的分配槽40排出,其落在質量轉移床16的上表面上。雖然如示出的是包含關於第2圖至第5圖所示之液體分配器18,其應被理解質量轉移塔10可包含如關於第6圖至第8圖的描述設置的液體分配器118或包含關於第9圖至 第11圖的描述設置的液體分配器218。額外的,當質量轉移塔10包含二或多個質量轉移床16,其也可包含配置以類似的方式接收及排出液體流至各質量轉移床16的上表面上的二或多個液體分配器18、118、218。 Referring again to FIG. 1, when the lowered liquid is discharged from the distribution tank 40 of the liquid distributor 18, it falls on the upper surface of the mass transfer bed 16. Although shown as including the liquid distributor 18 shown in FIGS. 2 to 5, it should be understood that the mass transfer tower 10 may include the liquid distributor 118 provided as described in relation to FIGS. 6 to 8. Or contain images about 9 to FIG. 11 illustrates the liquid distributor 218 provided. Additionally, when the mass transfer tower 10 includes two or more mass transfer beds 16, it may also include two or more liquid distributors configured to receive and discharge liquid flow to the upper surface of each mass transfer bed 16 in a similar manner. 18, 118, 218.

綜上所述,將可見本發明可良好適於達成上文中所述結果與目的以及所述及所揭露之結構固有的其他優勢。 In summary, it will be seen that the present invention is well adapted to achieve the results and objectives described above and other advantages inherent to the structures described and disclosed.

應當理解的是,某些特徵和子組合是有用的,且可以單獨地且不參考其他特徵和子組合地使用。這是本發明之專利申請範圍所設想到且在本發明之專利申請範圍之內。 It should be understood that certain features and sub-combinations are useful and can be used individually and without reference to other features and sub-combinations. This is contemplated by the scope of the patent application of the present invention and is within the scope of the patent application of the present invention.

由於許多可能的實施例可以本文揭露之發明進行,而不脫離本文所公開的本發明的範疇被完成,但應當理解,本文中所闡述或在附圖中所示的所有內容都將被解釋為說明性的,而不是限制的意義 Since many possible embodiments can be made with the invention disclosed herein without departing from the scope of the invention disclosed herein, it should be understood that everything described herein or shown in the drawings will be interpreted as Descriptive rather than restrictive meaning

Claims (20)

一種用於在一垂直長形處理塔中之下降液體之流量分配器,該流量分配器包含:一中央分配構件,係包含用於接收液體流之至少一入口及用於從該中央分配構件排出該液體流之一部份之一或多個液體出口;複數個長形側構件,係設置以接收從該中央分配構件之該液體出口排出之液體之至少一部分,其中該複數個長形側構件係沿該中央分配構件之長度縱向的彼此間隔隔開且包含用於從其排出液體之一或多個開口;複數個分配槽,係位在靠近該長形側構件,該複數個分配槽中的每一個包含一對長形側壁,其中該對長形側壁橫向地彼此間隔以在其間定義一液體接收空間及一實質上開放的底板區域,其中該液體接收空間係設置以接收自該長形側構件之該開口排出之液體且透過該底板區域自該分配槽排出該液體;及規整(structured)填料之二或多個片材,其位於各該等液體接收空間中,用於在該液體被容置於該液體接收空間中時且在該液體透過該底板區域自該分配槽被排出之前增強該液體的水平散佈(horizontal spreading),該規整(structured)填料之各該等二或多個片材定義該液體之一下部滴液邊緣(lower drip edge)。A flow distributor for a falling liquid in a vertical elongated processing tower, the flow distributor comprising: a central distribution member including at least one inlet for receiving a liquid flow and for discharging from the central distribution member One or more liquid outlets as part of the liquid flow; a plurality of elongated side members arranged to receive at least a portion of the liquid discharged from the liquid outlet of the central distribution member, wherein the plurality of elongated side members Are spaced apart from each other longitudinally along the length of the central distribution member and contain one or more openings for discharging liquid therefrom; a plurality of distribution grooves are positioned near the elongated side member in the plurality of distribution grooves Each includes a pair of elongated side walls, where the pair of elongated side walls are laterally spaced apart from each other to define a liquid receiving space and a substantially open floor area therebetween, wherein the liquid receiving space is configured to receive from the elongated Liquid discharged from the opening of the side member and discharged from the distribution tank through the bottom plate area; and two or more sheets of structured filler, located at The liquid receiving spaces are used to enhance the horizontal spreading of the liquid when the liquid is contained in the liquid receiving space and before the liquid is discharged from the distribution tank through the bottom plate area, the structure is regular Each of the two or more sheets of structured material defines a lower drip edge of one of the liquids. 如申請專利範圍第1項所述之分配器,其中該複數個長形側構件包含至少一第一長形側構件及一第二長形側構件,且該複數個分配槽包含至少一第一分配槽及一第二分配槽,其中該第一長形側構件係配置以排出液體進入各該第一分配槽及該第二分配槽。The distributor according to item 1 of the scope of patent application, wherein the plurality of elongated side members include at least a first elongated side member and a second elongated side member, and the plurality of distribution slots include at least one first A distribution tank and a second distribution tank, wherein the first elongated side member is configured to discharge liquid into each of the first distribution tank and the second distribution tank. 如申請專利範圍第2項所述之分配器,其中該第二長形側構件係配置以排出液體進入各該第一分配槽及該第二分配槽。The dispenser according to item 2 of the scope of patent application, wherein the second elongated side member is configured to discharge liquid into each of the first distribution tank and the second distribution tank. 如申請專利範圍第2項所述之分配器,其中該第一長形側構件包含一第一對液體出口及一第二對液體出口,其中該第一對液體出口係配置以排出液體進入該第一分配槽及該第二對液體出口係配置以排出液體進入該第二分配槽。The dispenser according to item 2 of the patent application scope, wherein the first elongated side member includes a first pair of liquid outlets and a second pair of liquid outlets, wherein the first pair of liquid outlets are configured to discharge liquid into the The first distribution tank and the second pair of liquid outlets are configured to discharge liquid into the second distribution tank. 如申請專利範圍第2項所述之分配器,其中該第一長形側構件包含設置在該長形側構件之相對側上之至少一第一對液體出口,其中該第一對液體出口其中之一係設置以排出液體進入該第一分配槽及該第一對液體出口其中之另一係設置以排出液體進入該第二分配槽。The dispenser according to item 2 of the scope of patent application, wherein the first elongated side member includes at least one first pair of liquid outlets disposed on opposite sides of the elongated side member, wherein the first pair of liquid outlets therein One is arranged to discharge liquid into the first distribution tank and the other is arranged to discharge liquid into the second distribution tank. 如申請專利範圍第2項所述之分配器,進一步包含一第三分配槽及一第四分配槽,其中該第一長形側構件係設置以排出液體進入該第一分配槽及該第二分配槽且該第二長形側構件係設置以排出液體進入該第三分配槽及該第四分配槽。The dispenser according to item 2 of the scope of patent application, further comprising a third distribution tank and a fourth distribution tank, wherein the first elongated side member is arranged to discharge liquid into the first distribution tank and the second distribution tank. The distribution groove and the second elongated side member are arranged to discharge liquid into the third distribution groove and the fourth distribution groove. 如申請專利範圍第2項所述之分配器,進一步包含一第三分配槽及一第四分配槽,其中各該第一長形側構件及該第二長形側構件係設置以排出液體進入各該第一分配槽、該第二分配槽、該第三分配槽、及該第四分配槽。The dispenser according to item 2 of the scope of patent application, further comprising a third distribution tank and a fourth distribution tank, wherein each of the first elongated side member and the second elongated side member are arranged to discharge liquid into Each of the first distribution slot, the second distribution slot, the third distribution slot, and the fourth distribution slot. 如申請專利範圍第2項所述之分配器,其中該第一長形側構件及該第二長形側構件之伸長軸係實質上平行彼此且該第一長形側構件及該第二長形側構件係實質上垂直於該中央分配構件之伸長軸。The dispenser according to item 2 of the scope of patent application, wherein the elongated shafts of the first elongated side member and the second elongated side member are substantially parallel to each other and the first elongated side member and the second long The shaped side member is substantially perpendicular to the elongation axis of the central distribution member. 如申請專利範圍第8項所述之分配器,其中該第一分配槽及該第二分配槽之伸長軸係實質上平行於該第一長形側構件及該第二長形側構件之伸長軸。The distributor according to item 8 of the scope of patent application, wherein the elongation axes of the first and second distribution grooves are substantially parallel to the elongation of the first elongated side member and the second elongated side member axis. 如申請專利範圍第8項所述之分配器,其中該第一分配槽及該第二分配槽之伸長軸係實質上垂直於該第一長形側構件及該第二長形側構件之伸長軸。The distributor according to item 8 of the scope of patent application, wherein the elongation axes of the first and second distribution grooves are substantially perpendicular to the elongation of the first elongated side member and the second elongated side member axis. 如申請專利範圍第1項所述之分配器,其中該中央分配構件係位在垂直高度高於該長形側構件之至少一部分處。The distributor according to item 1 of the scope of patent application, wherein the central distribution member is located at least a part of the vertical height higher than the elongated side member. 如申請專利範圍第1項所述之分配器,其中該中央分配構件係實質上與該長形側構件之至少一部分在同一垂直平面上。The dispenser according to item 1 of the patent application scope, wherein the central distribution member is substantially on the same vertical plane as at least a part of the elongated side member. 如申請專利範圍第1項所述之分配器,其中各該長形側構件自該中央分配構件以在約30°至150°之範圍內之一角度向外延伸。The distributor according to item 1 of the patent application range, wherein each of the elongated side members extends outward from the central distribution member at an angle within a range of about 30 ° to 150 °. 如申請專利範圍第1項所述之分配器,其中各該規整填料之該等二或多個片材係垂直延伸及波紋狀。The distributor according to item 1 of the scope of patent application, wherein the two or more sheets of each of the structured packings extend vertically and are corrugated. 如申請專利範圍第1項所述之分配器,其中該規整填料包含至少二個垂直延伸的紗網狀填料片材。The dispenser according to item 1 of the patent application scope, wherein the structured packing comprises at least two vertically extending gauze-like packing sheets. 如申請專利範圍第1項所述之分配器,其中規整填料包含織物之規整填料。The dispenser according to item 1 of the patent application range, wherein the structured packing comprises the structured packing of the fabric. 如申請專利範圍第1項所述之分配器,其中規整填料包含多孔的規整填料。The distributor according to item 1 of the patent application range, wherein the structured packing comprises a porous structured packing. 如申請專利範圍第1項所述之分配器,其中該下部滴液邊緣之至少一部分係為鋸齒的。The dispenser according to item 1 of the patent application scope, wherein at least a part of the lower drip edge is serrated. 如申請專利範圍第14項所述之分配器,其中當該液體自該分配槽被排出時該等滴液邊緣產生多條液體平行線(parallel lines of liquid)。The dispenser according to item 14 of the scope of patent application, wherein when the liquid is discharged from the distribution tank, a plurality of parallel lines of liquid are generated at the edges of the drops. 一種流量分配器,係用於在一垂直長形處理塔中之下降液體,該流量分配器包含:一中央分配構件,係包含用於接收液體流之至少一入口及用於從該中央分配構件排出該液體流之一部份之一或多個液體出口;複數個長形側構件,係設置以接收從該中央分配構件之該液體出口排出之液體之至少一部分,其中該複數個長形側構件係沿該中央分配構件之長度縱向的彼此間隔隔開且包含用於從其排出液體之一或多個開口;複數個分配槽,係位在靠近該長形側構件,該複數個分配槽中的每一個包含一對長形側壁,其中該對長形側壁橫向地彼此間隔以在其間定義一液體接收空間及一實質上開放的底板區域,其中該液體接收空間係設置以接收自該長形側構件之該開口排出之液體且透過該底板區域自該分配槽排出該液體,其中該複數個長形側構件包含至少一第一長形側構件及一第二長形側構件,且該複數個分配槽包含至少一第一分配槽及一第二分配槽,其中該第一長形側構件係配置以排出液體進入各該第一分配槽及該第二分配槽;及複數個垂直延伸的波紋狀規整填料片材,其位於各該第一分配槽及該第二分配槽之該液體接收空間中,用於在該液體被容置於該液體接收空間中時且在該液體透過該底板區域自該第一或第二分配槽被排出之前增強該液體的水平散佈,其中該等規整填料片材之各者均定義一下部滴液邊緣,該等滴液邊緣使得該液體沿著多條平行線自各該第一及第二分配槽被排出。A flow distributor for descending liquid in a vertically elongated processing tower, the flow distributor includes: a central distribution member including at least one inlet for receiving a liquid flow and for distributing from the central distribution member One or more liquid outlets that discharge a portion of the liquid stream; a plurality of elongated side members arranged to receive at least a portion of the liquid discharged from the liquid outlet of the central distribution member, wherein the plurality of elongated sides The members are longitudinally spaced from each other along the length of the central distribution member and contain one or more openings for discharging liquid therefrom; a plurality of distribution grooves, which are located near the elongate side member, the plurality of distribution grooves Each of the two includes a pair of elongated side walls, where the pair of elongated side walls are laterally spaced apart from each other to define a liquid receiving space therebetween and a substantially open floor area, wherein the liquid receiving space is configured to receive from the long The liquid discharged from the opening of the side member and the liquid is discharged from the distribution tank through the bottom plate area, wherein the plurality of elongated side members include at least a first length A side member and a second elongated side member, and the plurality of distribution slots include at least a first distribution slot and a second distribution slot, wherein the first elongated side member is configured to discharge liquid into each of the first distributions Tank and the second distribution tank; and a plurality of vertically extending corrugated structured packing sheets, which are located in the liquid receiving space of each of the first distribution tank and the second distribution tank, and are used for containing the liquid Enhance the horizontal spread of the liquid while in the liquid receiving space and before the liquid is discharged from the first or second distribution tank through the floor area, wherein each of the structured packing sheets defines a lower drip Edges, the drip edges make the liquid discharged from each of the first and second distribution grooves along a plurality of parallel lines.
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