TWI612997B - 萃取反應器及用於從顆粒材料萃取之方法 - Google Patents
萃取反應器及用於從顆粒材料萃取之方法 Download PDFInfo
- Publication number
- TWI612997B TWI612997B TW102139683A TW102139683A TWI612997B TW I612997 B TWI612997 B TW I612997B TW 102139683 A TW102139683 A TW 102139683A TW 102139683 A TW102139683 A TW 102139683A TW I612997 B TWI612997 B TW I612997B
- Authority
- TW
- Taiwan
- Prior art keywords
- extraction
- heat exchanger
- temperature
- patent application
- scope
- Prior art date
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 287
- 239000008187 granular material Substances 0.000 title claims abstract description 9
- 239000000284 extract Substances 0.000 claims abstract description 21
- 239000011236 particulate material Substances 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims description 115
- 239000002245 particle Substances 0.000 claims description 61
- 238000000034 method Methods 0.000 claims description 22
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims description 20
- 238000009835 boiling Methods 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 8
- 230000002706 hydrostatic effect Effects 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 229920000393 Nylon 6/6T Polymers 0.000 claims description 2
- 230000008859 change Effects 0.000 claims description 2
- 239000004952 Polyamide Substances 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 8
- 229920002647 polyamide Polymers 0.000 abstract description 8
- 238000006068 polycondensation reaction Methods 0.000 abstract description 3
- 239000000178 monomer Substances 0.000 description 11
- 229920002292 Nylon 6 Polymers 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 9
- 229920000642 polymer Polymers 0.000 description 7
- 239000012530 fluid Substances 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002826 coolant Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229920000768 polyamine Polymers 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 230000005465 channeling Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000011026 diafiltration Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000013529 heat transfer fluid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0207—Control systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0219—Fixed bed of solid material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/46—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Automation & Control Theory (AREA)
- Extraction Or Liquid Replacement (AREA)
- Polyamides (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12191455.0A EP2727637B1 (de) | 2012-11-06 | 2012-11-06 | Extraktionsreaktor sowie verfahren zur extraktion von granulärem material |
| ??12191455.0 | 2012-11-06 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201424819A TW201424819A (zh) | 2014-07-01 |
| TWI612997B true TWI612997B (zh) | 2018-02-01 |
Family
ID=47115619
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW102139683A TWI612997B (zh) | 2012-11-06 | 2013-11-01 | 萃取反應器及用於從顆粒材料萃取之方法 |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP2727637B1 (OSRAM) |
| JP (1) | JP6359021B2 (OSRAM) |
| KR (1) | KR102097290B1 (OSRAM) |
| CN (2) | CN203474700U (OSRAM) |
| ES (1) | ES2747448T3 (OSRAM) |
| IN (1) | IN2015DN02955A (OSRAM) |
| PL (1) | PL2727637T3 (OSRAM) |
| SI (1) | SI2727637T1 (OSRAM) |
| TW (1) | TWI612997B (OSRAM) |
| WO (1) | WO2014072167A1 (OSRAM) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3727626A1 (de) | 2017-12-22 | 2020-10-28 | Uhde High Pressure Technologies GmbH | Vorrichtung und verfahren zum hochdruckbehandeln von schüttgut durch extrahieren und/oder imprägnieren sowie verwendung |
| CN111330309B (zh) * | 2020-03-30 | 2021-09-21 | 浙江温兄机械阀业有限公司 | 物料分层式动态提取设备及其提取方法 |
| CN112430498B (zh) * | 2020-11-20 | 2024-09-03 | 湖南和广生物科技有限公司 | 一种多料篮梯级分步超临界流体萃取釜 |
| CN116036645B (zh) * | 2022-11-28 | 2025-10-21 | 福建省力恒锦纶实业有限公司 | 一种低熔点共聚酰胺的连续萃取方法 |
| CN117225004B (zh) * | 2023-11-14 | 2024-01-26 | 湖南禧又多油脂有限公司 | 一种基于物联网的植物油低温萃取处理自动控制系统 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4002430A (en) * | 1974-01-31 | 1977-01-11 | Basf Aktiengesellschaft | Extraction tube for polyamides |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2248220A (en) * | 1938-05-26 | 1941-07-08 | Mid Continent Petroleum Corp | Method of separating constituents of mineral oils |
| US2578670A (en) * | 1946-08-12 | 1951-12-18 | Robert A Carleton | Method of deodorizing and stabilizing soybean oil |
| DE1012479B (de) | 1952-06-07 | 1957-07-18 | Hessische Berg Und Huettenwerk | Verfahren zur Messung der Gaszusammensetzung von zwei oder mehr regenerativ beheizten Systemen, z. B. Hochofen-Winderhitzern |
| DE2242642C3 (de) * | 1972-08-30 | 1980-06-19 | Basf Ag, 6700 Ludwigshafen | Verfahren zum kontinuierlichen Extrahieren von Polylactamen |
| US4160647A (en) * | 1975-08-02 | 1979-07-10 | Chimkombinat | Continuous operation extractor |
| DD206999A1 (de) * | 1981-09-04 | 1984-02-15 | Peter Kramer | Kontinuierliches extraktionsverfahren fuer kunststoff-granulat |
| JPS5925803A (ja) * | 1982-08-03 | 1984-02-09 | Mitsui Toatsu Chem Inc | 向流洗浄塔および合成樹脂スラリ−の洗浄方法 |
| DE19752183A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur kontinuierlichen Extraktion von Polyamid |
| DE19752182A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur kontinuierlichen Extraktion von Polyamid |
| DE19801267B4 (de) * | 1998-01-15 | 2005-03-24 | Inventa-Fischer Gmbh | Verfahren zur Herstellung von PA-6 Granulat und dessen Verwendung |
| DE19808442A1 (de) * | 1998-02-27 | 1999-09-02 | Basf Ag | Verfahren zur Extraktion von Polyamidteilchen |
| DE10124579A1 (de) | 2001-05-21 | 2002-12-05 | Bayer Ag | Verfahren und Vorrichtung zur Extraktion von Polyamid |
| US6479620B1 (en) * | 2001-06-01 | 2002-11-12 | E. I. Du Pont De Nemours And Company | Process for converting caprolactam to nylon 6 |
| JP2008080267A (ja) * | 2006-09-28 | 2008-04-10 | Toray Ind Inc | 複合式熱交換型反応器およびそれを用いたポリカプロアミドプレポリマーの製造方法 |
| DE102007061136A1 (de) * | 2007-12-19 | 2009-06-25 | Glatt Ingenieurtechnik Gmbh | Verfahren und Vorrichtung zur mehrstufigen Behandlung von dispersen Feststoffen |
| DE102008044452A1 (de) | 2008-08-19 | 2010-02-25 | Lurgi Zimmer Gmbh | Kontinuierliches Verfahren zur Extraktion von Polyamid-6 |
| US8425655B2 (en) * | 2010-07-09 | 2013-04-23 | Carbon Capture Scientific, Llc | Gas pressurized separation column and process to generate a high pressure product gas |
-
2012
- 2012-11-06 SI SI201231667T patent/SI2727637T1/sl unknown
- 2012-11-06 EP EP12191455.0A patent/EP2727637B1/de active Active
- 2012-11-06 PL PL12191455T patent/PL2727637T3/pl unknown
- 2012-11-06 ES ES12191455T patent/ES2747448T3/es active Active
- 2012-11-21 CN CN201220757326.5U patent/CN203474700U/zh not_active Expired - Lifetime
-
2013
- 2013-10-21 IN IN2955DEN2015 patent/IN2015DN02955A/en unknown
- 2013-10-21 KR KR1020157010916A patent/KR102097290B1/ko active Active
- 2013-10-21 JP JP2015540093A patent/JP6359021B2/ja not_active Expired - Fee Related
- 2013-10-21 WO PCT/EP2013/071987 patent/WO2014072167A1/de not_active Ceased
- 2013-10-21 CN CN201380058137.6A patent/CN104780988B/zh active Active
- 2013-11-01 TW TW102139683A patent/TWI612997B/zh active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4002430A (en) * | 1974-01-31 | 1977-01-11 | Basf Aktiengesellschaft | Extraction tube for polyamides |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6359021B2 (ja) | 2018-07-18 |
| IN2015DN02955A (OSRAM) | 2015-09-18 |
| SI2727637T1 (sl) | 2019-11-29 |
| TW201424819A (zh) | 2014-07-01 |
| WO2014072167A1 (de) | 2014-05-15 |
| KR102097290B1 (ko) | 2020-04-06 |
| CN203474700U (zh) | 2014-03-12 |
| EP2727637A1 (de) | 2014-05-07 |
| PL2727637T3 (pl) | 2020-02-28 |
| EP2727637B1 (de) | 2019-08-28 |
| KR20150105293A (ko) | 2015-09-16 |
| ES2747448T3 (es) | 2020-03-10 |
| CN104780988B (zh) | 2017-06-16 |
| CN104780988A (zh) | 2015-07-15 |
| JP2016502458A (ja) | 2016-01-28 |
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