TWI608176B - Rotation axis device - Google Patents

Rotation axis device Download PDF

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Publication number
TWI608176B
TWI608176B TW105120112A TW105120112A TWI608176B TW I608176 B TWI608176 B TW I608176B TW 105120112 A TW105120112 A TW 105120112A TW 105120112 A TW105120112 A TW 105120112A TW I608176 B TWI608176 B TW I608176B
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Taiwan
Prior art keywords
rotary shaft
rotating shaft
disposed
shaft member
cover
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TW105120112A
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Chinese (zh)
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TW201800673A (en
Inventor
Shih Wen Wen
Chung Ho Wu
Jia Long Liu
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Shih Wen Wen
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Priority to TW105120112A priority Critical patent/TWI608176B/en
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Publication of TWI608176B publication Critical patent/TWI608176B/en
Publication of TW201800673A publication Critical patent/TW201800673A/en

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

旋轉軸裝置Rotary shaft device

本發明相關於一種昇華純化設備,特別是相關於一種用以穿入昇華純化設備的一用於純化材料的內管容置構件的旋轉軸裝置。The present invention relates to a sublimation purification apparatus, and more particularly to a rotary shaft apparatus for inserting an inner tube housing member for purifying a material into a sublimation purification apparatus.

昇華(Sublimation)是指一種物質不經過液態而直接自固態轉化為氣態的過程,此種物態變化是發生在溫度和氣壓低於物質三相點的時候。因此,藉由調整到特定溫度、特定壓力,使不同的物質分別保持於固態或昇華為氣態,以分離出特定物質的昇華純化方式,已廣泛為人們所使用。Sublimation refers to the process in which a substance is directly converted from a solid to a gaseous state without passing through a liquid state. This change in state occurs when the temperature and pressure are lower than the triple point of the substance. Therefore, sublimation purification methods for separating different substances into a solid state or sublimating into a gaseous state by adjusting to a specific temperature and a specific pressure have been widely used.

在習知技術中,此種昇華純化方式是將原材料放入昇華純化設備內加熱,使原材料中的目標材料昇華為氣態而輸出。由於單一次的純化處理所能得到的純度有限,故往往還需要再做第二次、第三次的純化處理才能達到純度需求。為此,需要將經昇華過一次的材料先經過冷卻降溫(約花費3小時),才能再次放入昇華純化設備內進行下一次的純化處理。然而,此種作法的過程繁複,需將材料反覆移動以進行冷卻及昇華,所以會造成無法連續式作業,耗時又費工,從而增加成本。再者,其過程中需破真空(venting),不僅會使純化效果變差,甚至有使材料受到汙染的可能性。In the prior art, the sublimation purification method is to heat the raw material into a sublimation purification device, and the target material in the raw material is sublimated into a gaseous state and output. Since the purity that can be obtained by a single purification treatment is limited, it is often necessary to perform the second and third purification treatments to achieve the purity requirement. For this reason, it is necessary to cool the material once sublimated once (about 3 hours) before it can be put into the sublimation purification equipment again for the next purification treatment. However, the process of this method is complicated, and the material needs to be moved repeatedly for cooling and sublimation, so that continuous operation is impossible, time-consuming and labor-intensive, thereby increasing the cost. Furthermore, venting is required in the process, which not only deteriorates the purification effect, but also has the possibility of contaminating the material.

因此,為解決上述問題,本發明的目的即在提供一種用以穿入一昇華純化設備的一用於純化材料的內管容置構件的旋轉軸裝置,利用旋轉軸裝置在真空狀態下控制內管容置構件相對旋轉,從而使昇華純化設備能連續式作業且無需破真空。Therefore, in order to solve the above problems, an object of the present invention is to provide a rotary shaft device for inserting a sublimation purification device into an inner tube accommodating member for purifying a material, which is controlled by a rotary shaft device under a vacuum state. The tube housing member is relatively rotated so that the sublimation purification device can operate continuously without breaking the vacuum.

本發明為解決習知技術之問題所採用之技術手段係提供一種旋轉軸裝置,包含:一旋轉軸構件,沿一延伸方向延伸,該旋轉軸構件具有一插枵端,該插枵端用以穿入一昇華純化設備的一用於純化材料的內管容置構件; 一門蓋構件,包括一套設於該旋轉軸構件的蓋體,該蓋體的朝向該插枵端的一側用以蓋合該內管容置構件的一開口部;以及一插枵構件,包括一承載片及複數個插枵,該承載片套設於該旋轉軸構件的該插枵端,該複數個插枵分別以平行該延伸方向的方式設置於該承載片,其中該插枵端及該複數個插枵經設置而對應插入該內管容置構件內部的插槽,該旋轉軸構件經設置而於該旋轉軸構件的軸向方向旋轉該內管容置構件。The technical means for solving the problems of the prior art provides a rotary shaft device, comprising: a rotating shaft member extending along an extending direction, the rotating shaft member having a plug end, wherein the plug end is used for An inner tube receiving member for purifying material penetrated into a sublimation purification device; a door cover member comprising a cover body disposed on the rotating shaft member, the side of the cover body facing the insertion end for covering An opening portion of the inner tube accommodating member; and a splicing member, comprising a carrier sheet and a plurality of splicing sleeves, the carrier sheet is sleeved on the insertion end of the rotating shaft member, and the plurality of splicing portions respectively The carrier sheet is disposed in parallel with the extending direction, wherein the plug end and the plurality of plugs are disposed to correspondingly insert into the slot of the inner tube receiving member, and the rotating shaft member is disposed to rotate The inner tube housing member is rotated in the axial direction of the shaft member.

在本發明的一實施例中係提供一種旋轉軸裝置,該插枵構件更包括一調整件,設置於該旋轉軸構件且連接該承載片,該調整件經設置而在該旋轉軸構件上移動而調整該承載片與該旋轉軸構件的相對位置。In an embodiment of the invention, a rotary shaft device is further provided, the plug member further comprising an adjusting member disposed on the rotating shaft member and connected to the carrier sheet, the adjusting member being disposed to move on the rotating shaft member The relative position of the carrier sheet and the rotating shaft member is adjusted.

在本發明的一實施例中係提供一種旋轉軸裝置,該承載片以重心位置連接該旋轉軸構件。In an embodiment of the invention, there is provided a rotary shaft device that connects the rotary shaft member at a center of gravity.

在本發明的一實施例中係提供一種旋轉軸裝置,該旋轉軸構件係為可相對該蓋體而沿該延伸方向滑移。In an embodiment of the invention, a rotary shaft assembly is provided that is slidable relative to the cover in the direction of extension.

在本發明的一實施例中係提供一種旋轉軸裝置,更包括一限位構件,設置於該旋轉軸構件,該限位構件經設置而限制該旋轉軸構件相對該蓋體的滑移範圍。In an embodiment of the invention, a rotary shaft device is provided, further comprising a limiting member disposed on the rotating shaft member, the limiting member being disposed to limit a sliding range of the rotating shaft member relative to the cover.

在本發明的一實施例中係提供一種旋轉軸裝置,更包括一密封構件,設置於該旋轉軸構件且連接該蓋體,該密封構件密合於該旋轉軸構件及該蓋體之間的空隙而密封該內管容置構件。In an embodiment of the invention, a rotary shaft device is further provided, further comprising a sealing member disposed on the rotating shaft member and connected to the cover body, the sealing member being tightly engaged between the rotating shaft member and the cover body The inner tube housing member is sealed by a gap.

在本發明的一實施例中係提供一種旋轉軸裝置,更包括一握柄構件,設置於該旋轉軸構件的一相反於該插枵端的握柄端,該握柄構件的半徑大於該旋轉軸構件的截面的半徑。In an embodiment of the invention, a rotary shaft device is further provided, further comprising a handle member disposed on a handle end of the rotary shaft member opposite to the insertion end, the radius of the handle member being greater than the rotation axis The radius of the section of the component.

在本發明的一實施例中係提供一種旋轉軸裝置,該蓋體係呈圓形。In an embodiment of the invention, a rotary shaft device is provided, the cover system being circular.

在本發明的一實施例中係提供一種旋轉軸裝置,該門蓋構件更包括一固定件,設置於該蓋體的外周緣,用以將該蓋體固定於該昇華純化設備的一殼體。In an embodiment of the present invention, a rotating shaft device is further provided, the door cover member further comprising a fixing member disposed on an outer circumference of the cover body for fixing the cover body to a casing of the sublimation purification device .

經由本發明所採用之技術手段,旋轉軸裝置可穿入一昇華純化設備的一用於純化材料的內管容置構件並密封該內管容置構件的一開口部,使旋轉軸裝置在真空狀態下控制內管容置構件相對旋轉,從而使昇華純化設備能連續式作業且無需破真空,降低材料受到汙染的可能性,而容易得到更佳的純化效果。Through the technical means adopted by the present invention, the rotating shaft device can penetrate an inner tube receiving member for purifying material of a sublimation purification device and seal an opening portion of the inner tube receiving member, so that the rotating shaft device is in a vacuum In the state, the inner tube accommodating member is controlled to rotate relatively, so that the sublimation purification device can operate continuously without breaking the vacuum, thereby reducing the possibility of contamination of the material, and it is easy to obtain better purification effect.

本發明所採用的具體實施例,將藉由以下之實施例及附呈圖式作進一步之說明。The specific embodiments of the present invention will be further described by the following examples and the accompanying drawings.

以下根據第1圖至第3圖,而說明本發明的實施方式。該說明並非為限制本發明的實施方式,而為本發明之實施例的一種。Hereinafter, embodiments of the present invention will be described with reference to Figs. 1 to 3 . This description is not intended to limit the embodiments of the invention, but is an embodiment of the invention.

如第1圖至第3圖所示,旋轉軸裝置100包含:一旋轉軸構件1、一門蓋構件2及一插枵構件3。As shown in FIGS. 1 to 3, the rotary shaft device 100 includes a rotary shaft member 1, a door cover member 2, and a plug member 3.

旋轉軸構件1沿一延伸方向L延伸。旋轉軸構件1具有一插枵端11,插枵端11用以穿入一昇華純化設備的一用於純化材料的內管容置構件T(繪於第3圖)。The rotating shaft member 1 extends in an extending direction L. The rotary shaft member 1 has a spigot end 11 for penetrating into an inner tube accommodating member T for purification material of a sublimation purification apparatus (drawn in Fig. 3).

門蓋構件2包括一套設於旋轉軸構件1的蓋體21,蓋體21的朝向插枵端11的一側用以蓋合內管容置構件T的一開口部。在本實施例中,蓋體係呈圓形。門蓋構件2更包括一固定件22,設置於蓋體21的外周緣,用以將蓋體21固定於昇華純化設備的一殼體。The door cover member 2 includes a cover body 21 provided on the rotary shaft member 1, and a side of the cover body 21 facing the insertion end 11 is used to cover an opening portion of the inner tube accommodation member T. In this embodiment, the lid system is circular. The door cover member 2 further includes a fixing member 22 disposed on the outer periphery of the cover body 21 for fixing the cover body 21 to a casing of the sublimation purification device.

插枵構件3包括一承載片31及複數個插枵32,承載片31套設於旋轉軸構件1的插枵端11,複數個插枵32分別以平行延伸方向L的方式設置於承載片31。在本實施例中,承載片31以重心位置連接旋轉軸構件1。插枵端11及複數個插枵32經設置而對應插入內管容置構件T內部的插槽,旋轉軸構件1經設置而於旋轉軸構件1的軸向方向旋轉內管容置構件T。The insertion member 3 includes a carrier 31 and a plurality of insertions 32. The carrier 31 is sleeved on the insertion end 11 of the rotating shaft member 1. The plurality of insertions 32 are respectively disposed on the carrier 31 in a parallel extending direction L. . In the present embodiment, the carrier sheet 31 is connected to the rotary shaft member 1 at the center of gravity. The insertion end 11 and the plurality of insertion holes 32 are provided to correspond to the slots inserted into the inside of the inner tube housing member T, and the rotary shaft member 1 is provided to rotate the inner tube accommodation member T in the axial direction of the rotary shaft member 1.

進一步地,插枵構件3更包括一調整件33,設置於旋轉軸構件1且連接承載片31,調整件33經設置而在旋轉軸構件1上移動而調整承載片31與旋轉軸構件1的相對位置,以使複數個插枵32能對應匹配內管容置構件T內部的插槽。Further, the plug member 3 further includes an adjusting member 33 disposed on the rotating shaft member 1 and connected to the carrier sheet 31. The adjusting member 33 is disposed to move on the rotating shaft member 1 to adjust the carrier sheet 31 and the rotating shaft member 1. The relative positions are such that the plurality of plugs 32 can correspond to the slots inside the inner tube housing member T.

在本實施例中,旋轉軸裝置100更包括一限位構件4及一密封構件5。密封構件5設置於旋轉軸構件1且連接蓋體21,密封構件5用以密合於旋轉軸構件1及蓋體21之間的空隙而密封內管容置構件T。進一步地,旋轉軸構件1係為可相對蓋體21及密封構件5而沿延伸方向L滑移,因此當蓋體21透過固定件22固定於昇華純化設備的殼體時,可藉由將旋轉軸構件1沿延伸方向L滑移而使旋轉軸構件1配合內管容置構件T的長度。限位構件4設置於旋轉軸構件1,限位構件4經設置而限制旋轉軸構件1相對蓋體21的滑移範圍。In the embodiment, the rotating shaft device 100 further includes a limiting member 4 and a sealing member 5. The sealing member 5 is provided in the rotating shaft member 1 and is connected to the lid body 21, and the sealing member 5 is used to seal the gap between the rotating shaft member 1 and the lid body 21 to seal the inner tube housing member T. Further, the rotating shaft member 1 is slidable in the extending direction L with respect to the cover body 21 and the sealing member 5, so that when the cover body 21 is fixed to the housing of the sublimation purification device through the fixing member 22, it can be rotated The shaft member 1 is slid in the extending direction L such that the rotating shaft member 1 is fitted to the length of the inner tube accommodating member T. The stopper member 4 is provided to the rotating shaft member 1, and the stopper member 4 is provided to restrict the slip range of the rotating shaft member 1 with respect to the lid body 21.

在本實施例中,旋轉軸裝置100更包括一握柄構件6。握柄構件6設置於旋轉軸構件1的一相反於插枵端11的握柄端12,握柄構件6的半徑大於旋轉軸構件1的截面的半徑,用以方便使用者施力而以旋轉軸構件1的軸向方向旋轉內管容置構件T。In the present embodiment, the rotary shaft device 100 further includes a grip member 6. The handle member 6 is disposed on a handle end 12 of the rotating shaft member 1 opposite to the insertion end 11 , and the radius of the handle member 6 is larger than the radius of the section of the rotating shaft member 1 for facilitating the user to apply force to rotate The inner tube housing member T is rotated in the axial direction of the shaft member 1.

綜上所述,本發明提供的旋轉軸裝置可在軸向方向旋轉內管容置構件,以控制內管容置構件相對旋轉,使昇華純化設備能連續式作業且無需破真空,降低材料受到汙染的可能性,而容易得到更佳的純化效果。除此之外,調整件可調整承載片與旋轉軸構件的相對位置,以使插枵能對應匹配內管容置構件內部的插槽;旋轉軸構件可相對蓋體而沿延伸方向滑移,因此可使旋轉軸構件配合內管容置構件長度。In summary, the rotating shaft device provided by the present invention can rotate the inner tube accommodating member in the axial direction to control the relative rotation of the inner tube accommodating member, so that the sublimation purification device can be continuously operated without breaking the vacuum and reducing the material receiving. The possibility of contamination, and easy to get better purification results. In addition, the adjusting member can adjust the relative position of the carrier sheet and the rotating shaft member, so that the insertion slot can correspondingly match the slot inside the inner tube receiving member; the rotating shaft member can slide along the extending direction with respect to the cover body, Therefore, the rotating shaft member can be fitted to the inner tube accommodating member length.

以上之敘述以及說明僅為本發明之較佳實施例之說明,對於此項技術具有通常知識者當可依據以下所界定申請專利範圍以及上述之說明而作其他之修改,惟此些修改仍應是為本發明之發明精神而在本發明之權利範圍中。The above description and description are only illustrative of the preferred embodiments of the present invention, and those of ordinary skill in the art can make other modifications in accordance with the scope of the invention as defined below and the description above, but such modifications should still be It is within the scope of the invention to the invention of the invention.

100‧‧‧旋轉軸裝置
1‧‧‧旋轉軸構件
11‧‧‧插枵端
12‧‧‧握柄端
2‧‧‧門蓋構件
21‧‧‧蓋體
22‧‧‧固定件
3‧‧‧插枵構件
31‧‧‧承載片
32‧‧‧插枵
33‧‧‧調整件
4‧‧‧限位構件
5‧‧‧密封構件
6‧‧‧握柄構件
L‧‧‧延伸方向
T‧‧‧內管容置構件
100‧‧‧Rotary shaft device
1‧‧‧Rotary shaft members
11‧‧‧plug end
12‧‧‧ grip end
2‧‧‧door cover components
21‧‧‧ cover
22‧‧‧Fixed parts
3‧‧‧Insert components
31‧‧‧ Carrying film
32‧‧‧Insert
33‧‧‧Adjustment
4‧‧‧Limited components
5‧‧‧ Sealing member
6‧‧‧Handle member
L‧‧‧ Extension direction
T‧‧‧ inner tube housing member

第1圖為顯示根據本發明一實施例的旋轉軸裝置之立體圖。 第2圖為顯示根據本發明的實施例的旋轉軸裝置之剖面圖。 第3圖為顯示根據本發明的實施例的旋轉軸裝置及內管容置構件之示意圖。Fig. 1 is a perspective view showing a rotary shaft device according to an embodiment of the present invention. Fig. 2 is a cross-sectional view showing a rotary shaft device according to an embodiment of the present invention. Fig. 3 is a schematic view showing a rotary shaft device and an inner tube accommodating member according to an embodiment of the present invention.

100‧‧‧旋轉軸裝置 100‧‧‧Rotary shaft device

1‧‧‧旋轉軸構件 1‧‧‧Rotary shaft members

11‧‧‧插枵端 11‧‧‧plug end

2‧‧‧門蓋構件 2‧‧‧door cover components

21‧‧‧蓋體 21‧‧‧ cover

22‧‧‧固定件 22‧‧‧Fixed parts

3‧‧‧插枵構件 3‧‧‧Insert components

31‧‧‧承載片 31‧‧‧ Carrying film

32‧‧‧插枵 32‧‧‧Insert

33‧‧‧調整件 33‧‧‧Adjustment

4‧‧‧限位構件 4‧‧‧Limited components

5‧‧‧密封構件 5‧‧‧ Sealing member

6‧‧‧握柄構件 6‧‧‧Handle member

L‧‧‧延伸方向 L‧‧‧ Extension direction

Claims (9)

一種旋轉軸裝置,包含: 一旋轉軸構件,沿一延伸方向延伸,該旋轉軸構件具有一插枵端,該插枵端用以穿入一昇華純化設備的一用於純化材料的內管容置構件; 一門蓋構件,包括一套設於該旋轉軸構件的蓋體,該蓋體的朝向該插枵端的一側用以蓋合該內管容置構件的一開口部;以及 一插枵構件,包括一承載片及複數個插枵,該承載片套設於該旋轉軸構件的該插枵端,該複數個插枵分別以平行該延伸方向的方式設置於該承載片, 其中該插枵端及該複數個插枵經設置而對應插入該內管容置構件內部的插槽,該旋轉軸構件經設置而於該旋轉軸構件的軸向方向旋轉該內管容置構件。A rotary shaft device comprising: a rotating shaft member extending along an extending direction, the rotating shaft member having a plug end for penetrating into a inner tube of a sublimation purification device for purifying material a cover member comprising a cover body disposed on the rotating shaft member, a side of the cover body facing the insertion end for covering an opening of the inner tube receiving member; and a plug The component includes a carrier sheet and a plurality of inserts, the carrier sheet is sleeved on the insertion end of the rotating shaft member, and the plurality of inserts are respectively disposed on the carrier sheet in a manner parallel to the extending direction, wherein the inserting piece The end and the plurality of inserts are disposed to correspond to slots inserted into the inner tube housing member, and the rotary shaft member is disposed to rotate the inner tube housing member in the axial direction of the rotary shaft member. 如請求項1所述之旋轉軸裝置,其中該插枵構件更包括一調整件,設置於該旋轉軸構件且連接該承載片,該調整件經設置而在該旋轉軸構件上移動而調整該承載片與該旋轉軸構件的相對位置。The rotary shaft device of claim 1, wherein the insertion member further comprises an adjusting member disposed on the rotating shaft member and connected to the carrier sheet, the adjusting member being disposed to move on the rotating shaft member to adjust the The relative position of the carrier sheet to the rotating shaft member. 如請求項1所述之旋轉軸裝置,其中該承載片以重心位置連接該旋轉軸構件。A rotary shaft device according to claim 1, wherein the carrier sheet is coupled to the rotary shaft member at a center of gravity. 如請求項1所述之旋轉軸裝置,其中該旋轉軸構件係為可相對該蓋體而沿該延伸方向滑移。The rotary shaft device of claim 1, wherein the rotary shaft member is slidable in the extending direction relative to the cover. 如請求項4所述之旋轉軸裝置,更包括一限位構件,設置於該旋轉軸構件,該限位構件經設置而限制該旋轉軸構件相對該蓋體的滑移範圍。The rotary shaft device according to claim 4, further comprising a limiting member disposed on the rotating shaft member, the limiting member being disposed to limit a sliding range of the rotating shaft member relative to the cover. 如請求項1所述之旋轉軸裝置,更包括一密封構件,設置於該旋轉軸構件且連接該蓋體,該密封構件密合於該旋轉軸構件及該蓋體之間的空隙而密封該內管容置構件。The rotary shaft device of claim 1, further comprising a sealing member disposed on the rotating shaft member and connected to the cover, the sealing member being tightly fitted to a gap between the rotating shaft member and the cover to seal the The inner tube houses the member. 如請求項1所述之旋轉軸裝置,更包括一握柄構件,設置於該旋轉軸構件的一相反於該插枵端的握柄端,該握柄構件的半徑大於該旋轉軸構件的截面的半徑。The rotary shaft device according to claim 1, further comprising a grip member disposed on a grip end of the rotary shaft member opposite to the plug end, the grip member having a radius larger than a cross section of the rotary shaft member radius. 如請求項1所述之旋轉軸裝置,其中該蓋體係呈圓形。The rotary shaft device of claim 1, wherein the cover system has a circular shape. 如請求項1所述之旋轉軸裝置,其中該門蓋構件更包括一固定件,設置於該蓋體的外周緣,用以將該蓋體固定於該昇華純化設備的一殼體。The rotary shaft device of claim 1, wherein the door cover member further comprises a fixing member disposed on an outer circumference of the cover body for fixing the cover body to a casing of the sublimation purification device.
TW105120112A 2016-06-27 2016-06-27 Rotation axis device TWI608176B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1611366A1 (en) * 1988-01-26 1990-12-07 Всесоюзный Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ Sublimation-desublimation still
CN101721835A (en) * 2008-10-21 2010-06-09 沈善明 Continuous vacuum dynamic sublimating and condensing machine
CN102512843A (en) * 2012-01-04 2012-06-27 天津大学 Vacuum sublimation device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1611366A1 (en) * 1988-01-26 1990-12-07 Всесоюзный Научно-Исследовательский Институт Химических Реактивов И Особо Чистых Химических Веществ Sublimation-desublimation still
CN101721835A (en) * 2008-10-21 2010-06-09 沈善明 Continuous vacuum dynamic sublimating and condensing machine
CN102512843A (en) * 2012-01-04 2012-06-27 天津大学 Vacuum sublimation device

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