210280 A6 B6 五、發明說明（2 ) 其整個製造流程大致如下： id/ Q Aa \ , 湖）—水煑〜脱駿—膽固醇孓包接—遠心分禅 -把色、脱臭_低膽闺醇積製褚油。 述斅适流耘’租油先在約册〜9Q t之温皮下水煑約 20〜30分·錄 > ’咏去水溶液後，按照粗油駿價計算而加入鹼液 (氧 4·^! 於約75〜8〇χ：：2：溫度下進行中和攬拌，乒所 形成 < 魯肤》以.上 逆心分離機加以分離，益進行水洗脱駿。再將 脱駿尿理得到之 J〈轉油洛加和水相混合之具包接作用多醣類（ 環糊精），褚, 、 延仃巴接膽固醇之反應，再經遠心分離；將環糊 精一膽闺醇肖Α ^ 呼匕接物予以去除。再接着進行脱色和脱臭而完 低膽固醇含| 7丛 ®里< 精製豬泗之製造。 本發fl月；^ # 玉上’所需疋攻備如後述：其中水盡與包接 取程需要波、、左 . 热式二重釜，而包接脱除之製程需要攬拌裴 置’其製程設備（請參閱第-闺）包括有：粗洵貯槽i、輸 送泵2、7、1〇、乜、14、16、2。、熱交捵器3、8脱酸混 合槽4、脱駿挽拌機5、遠心分離機6、9、13、包接反應 橫11、乾燥塔15、脱色槽17、蜃遽器18、脱臭槽19、成品；由 槽21及有闕之鹼液槽22、水槽23及環糊精水液槽24，其中如 既駿、脱色、脱臭之浆程與目前精I油廠相同〇由於錄油（ 粗洵）中所含中性油以外之物質，例如游離脂肪峻苓對包接 效果影響最大，為達到最值之包接脱裙效果，而又避免影響 精製過程太九，本發明選揮其中最逍當之步驟，即在脱駿風 理後，進行膽同醇芝包接脱除製程，亦即在脱駿恩理後之邵 分精装錄沖中加入經興水相混合之具包接作用多醣類（環糊 甲 4(210X297 公潑） (請先聞讀背面之注意事項再填寫本頁) .裝. .線. 210280 A6 B6 五、發明説明（4 ) 拌時間在15〜75分鐘，攬拌溫度在30〜90 C下，膽固醇之 包接脱觫岣可得到顯著之效果。 目前市售豬油叼經過水芡、脱破、脱色、脱臭等之精 製步驟，若以精製後之豬油來進行包接去故膽固醇反應， 則反應後需再重覆油脂精製之過程，並不符合賁際應用效 益’但若以未精製之耝；由直接進行包接去除反應，則由於 粗油雜質太多，無法得到最佳包接效果，茲以圖一及表二 説明不同精製過程後進行包接反應對膽固醇殘餘量之影響。 經濟部中央標準局S工消費合作社印製 圖一、不同之豬油精製流程 —舣豬油精製流程 豬湳之包接精製流程㈠ _ - f 褚;由之包接精裝流程㈡ 緒油 緒油 練i田 C粗i由） | C粗油） 1 C粗油） ! 水煑 ί 水^： 1 1 水煑 1 Υ 脱酸 添加環糊精包接 脱酸 ^~取樣,Si二 遠心分離 .R 3 —取樣，贴一 添加環糊精包接 R 1 脱酸 遠心分離 —取樣點二 —取樣姑四 1 R 2 R 4 脱色 脱色 脱色 脱*臭 晛臭 脱臭 精I豬油 低膽固醇 低膽瞒 精裝褚油 ! 精製緒油 C比較例一） c比較例二） j' C賁施例） 衣紙張尺度適用中國國家標準（CNS)甲4规格（210 X 297公釐） 81.9.20,000 〜6〜 A6 B6 R 4 :為脱駿後再行包接作用之豬油 一 -— ----- 210280 五、發明説明（5 ) 表二：褚油經不同之精製或包接處理後之膽固醇殘餘量 取樣點 原膽固醇含量 C毫克/100克油） 膽闺醇殘餘量 C毫克/100克油） 膽固醇殘> 餘量 百分比 R 1 86.8 42.5 — 49.0 R2 86.8 32.8 ...................—-—— 37.8 〜 R 3 86.8 70.0 _ --------- 80.6 R 4 86.8 7.9 9.1 〜4 ^饮I f /「4 <研两〇 R 2 :未經脱酸，即洛加環糊精進行包接作用後，再行脱駿之豬> R 3 :尚未包接之脱醆褚渖。 由表二顯示 得到最好的膽固醇去除效果。此乃由於粗油中所含中性^ 外疋物質，例如游離脂肪酸、蹲抵質等會和具包接作用之 醣類（環糊精）結合，降低包接膽固醇之效果，故本發明' 使用脱酸後之邵分精製豬油來進行 多之膽固醇。最後再經一般 1 ‘右又，可去除: 奴‘由％加工f界所熟悉之脱色、！ 臭步朦，料得到風味、色澤艮好之低膽 前…中膽固醇之，餘量係用“層析儀一= 化侦測器分析，從；由中膽固醇 液膽固W含量足以證明，褚3 =析，及包接分離水 之多酷類C環糊精）包接嚴理=膽固醇經過具包接作 實旅例—： 已破分離帶至水相中。 取豬油C粗油）150克，經 ，得脱酸油137克，另以4·8克乏阮駿等精製過程名 本紙張/Ut適用中國因家標準（CNS)^jT7^ — t ^糊精與68·5克水4 -------------------------裝------.玎------^ . ' (請先閱;A.i!r面之注*事喟再坫寫本I) 經 濟 部 中 央 標 準 負 工 消 作 社 印 製 210 g210280 A6 B6 V. Description of the invention (2) The entire manufacturing process is roughly as follows: id / Q Aa \, Lake) —Water 煑 ～ 脱 髑 —Cholesterol encapsulation—Telecentric separation Zen-color, deodorization_Low gall boudoir Accumulate Chu oil. Shu Yu Shi Liu Yun's rented oil was first submerged in the warm skin ~ 9Q t for about 20 ~ 30 minutes. Record> After removing the aqueous solution, add the lye (oxygen 4 · ^ according to the crude oil price calculation) ! At about 75 ~ 80x :: 2: Neutralize and mix at temperature, form ping < Lu Fu》 to separate with the upper centrifugal separator, and benefit from water elution. Then remove the urine Reasonable J <The conversion reaction of polysaccharides (cyclodextrin) mixed with oil and water and the inclusion of water, Chu, Yan Yanba and cholesterol, and then separated by telecentricity; Alcohol Xiao ^ ^ The dagger connection is removed. Then it is decolorized and deodorized to complete the low cholesterol content | 7 Cong® Li < Manufacture of Refined Pig Si. This issue fl month; ^ # Yushang 'required preparations As described below: the water and the package pick-up process require a wave, and left. Thermal double kettle, and the process of removing the package requires the mixing of Pei Zhi's process equipment (please refer to the first-girl) includes: Storage tank i, delivery pumps 2, 7, 10, 乜, 14, 16, 2., heat exchanger 3, 8 deacidification mixing tank 4, dejun mixer 5, telecentric separator 6, 9, 13 ,package Reaction horizontal 11, drying tower 15, decolorizing tank 17, mirage 18, deodorizing tank 19, finished products; from tank 21 and alkaline liquid tank 22, water tank 23 and cyclodextrin water tank 24, of which The pulping process of decolorization and deodorization is the same as that of current Jingyi Oil Factory. Due to the substances other than neutral oil contained in the oil (coarse), such as free fat Junling has the greatest impact on the inclusion effect, it is the package that reaches the maximum value To take off the skirt effect, and to avoid affecting the refining process is too nine, the present invention chooses one of the most prudent steps, that is, after taking off the wind, carrying out the removal process of gallbladder and alcohol, that is, taking off the grace After the Shao Fen hardcover recording, the polysaccharides with inclusion effect mixed with Xing water (cyclodextrin 4 (210X297 public splash) are added (please read the precautions on the back and fill out this page). . Line. 210280 A6 B6 V. Description of the invention (4) Mixing time is 15 ~ 75 minutes, mixing temperature is 30 ~ 90 C, cholesterol can be obtained by decoupling and entrapment can get significant effects. Currently available lard After refining steps such as water hydrangea, depigmentation, decolorization, deodorization, etc. For sterol reaction, it is necessary to repeat the process of refining the oil after the reaction, which is not in line with the benefits of Benji application. But if it is not refined, the reaction will be removed by direct inclusion, because there are too many crude oil impurities, which cannot be obtained. For the best inclusion effect, the impact of the inclusion reaction on the residual cholesterol after different refining processes is illustrated in Figures 1 and 2. Figure 1 of the lard refining process by the Ministry of Economic Affairs Central Standards Bureau S Industry and Consumer Cooperative Printed Figure 1.舣 Lard oil refining process 湳 湳 Inclusion refining process ㈠ _-f Chu; from which to encapsulate the hardcover process ㈡ Xuyou Xuyou Liani Tian C crude i) | C crude oil) 1 C crude oil)! ί water ^: 1 1 water hydration 1 Υ Deacidification with cyclodextrin inclusion deacidification ^ ~ Sampling, Si two telecentric separation. R 3-Sampling, paste one with cyclodextrin inclusion R 1 Deacidification telecentric separation-sampling Point 2-Sampling 4 1 R 2 R 4 Decolorization Decolorization Decolorization Deodorization Deodorant Deodorant I Lard Low Cholesterol Low Bile Concealed Hardcover Chu Oil! Refined Xu Oil C Comparative Example 1) c Comparative Example 2) j 'C Ben Example) Appropriate size of clothing and paper China National Standard (CNS) A4 specifications (210 X 297 mm) 81.9.20,000 ～ 6 ~ A6 B6 R 4: lard for the purpose of wrapping after taking off the horse ----------- 210280 V. Description of the invention (5) Table 2: Cholesterol residue after different refining or encapsulation treatment. Cholesterol content (C mg / 100g oil) Cholesterol residue C mg / 100g oil) Cholesterol residue> ; Percentage remaining R 1 86.8 42.5 — 49.0 R2 86.8 32.8 ...................----- 37.8 ~ R 3 86.8 70.0 _ ------- -80.6 R 4 86.8 7.9 9.1 ～ 4 ^ Drinking I f / "4 < Ganliang 〇R 2: without deacidification, that is, after the inclusion effect of Luojia cyclodextrin, then take off the pigs who are off the horses > R 3: Chu Cheng who has not yet taken over. Table 2 shows the best cholesterol removal effect. This is because the neutral ^ scabby substances contained in the crude oil, such as free fatty acids, squatting mass, etc., will combine with the encapsulated sugar (cyclodextrin) to reduce the effect of encapsulating cholesterol, so the present invention ' Use demineralized lard refined lard to carry out excess cholesterol. Finally, after the general 1 ‘Right again, can be removed: Slave‘ Decoloration familiar from the% processing f world! Stinky step, expect to get a good flavor and color, low cholesterol before ... middle cholesterol, the remaining amount is analyzed by "chromatograph one = chemical detector, from; from the cholesterol content in the cholesterol liquid is sufficient to prove, Chu 3 = Analysis, and how much cool C cyclodextrin is included in the separation of water) Encapsulation is strict = Cholesterol is taken as an example after being encased: The broken separation is taken to the aqueous phase. Take lard C crude oil) 150 grams, 137 grams of deacidified oil, and 4.8 grams of dried Ruan Jun, etc. Refined process name paper / Ut applies to the China National Standards (CNS) ^ jT7 ^ — t ^ dextrin and 68.5 grams Water 4 ------------------------- installed ------. 玎 ------ ^. '(Please read first; Ai! R surface note * Then I will write it again I) Printed by the Ministry of Economic Affairs, Central Standard Workers' Press, 210 g
五、發明説明（6 ) 經 部 t 央 m 準 局 消 作 社 印 製 拌混合後，再將上述…徐徐加入，進行包接挽拌 中攬样速凌為測啊，溫度維持心，攬拌時間心鐘c 接後ϋ[接在常溫下以遠心離心c 匕 k 1800 Xg，10分鐘）分離， 反應液分成上下油水相兩層，上層 ‘價构知分離薏為123克。 此_接褚油，繼續以一般脱色、阮臭條件精製成低膽闺 醇精製豬油121克。從粗油膽闲醇含量86.8宅克/踟克由 經脱破步騄降至70毫克/肌“，再經包接脱色、脱臭:至 8.5毫^耽克油，其間膽阁醇〈去献半為9〇.7%。而脱色、 脱臭製程並未改變膽固醇含量。 實施例二： 取耝油C豬油”50克，經過水烫、脱駿等精製過程後 ，得脱酸泗137克。另以2·7克</Θ型環糊精與68.5克水攬 拌，混合後再將上述脱蛟拥徐徐加入，以進行包接挽持反應 。反應中，攬拌速度為1100 rpm，溫度維持3〇 Ό挽拌時間叨分 鐘，包接後’反應液ii:接在常溫下，以遠心離心〔woo xg， ίο分鐘）分離，將反應液分成上下油、水相兩層。上層油脂分 離所得量約為123克。將此晚駿包接績油，繼增以一般脱色 、脱臭條件精製成低膽固醇精軚鞴油，其膽固醇含量為 14.5毫克/伽克汩，膽闺醇；^去除率約為83 3 %。 〔註〕精製油脂之一舣條件： ⑴水煑：加30 %水（以油量計量）、85 X：加热25分鐘。 ⑵脱鲅：鹼量依油脂中游離脂昉酸量計异，脱破加熱通部Ό ，攬捽15分鐘，再以遠心分離宦脚。 ⑶脱色：加1.5 %之活性白土，在120 Ό下真空攬掉，冷却 本紙張尺度通用中國囲家標準（CNS)甲4规格（2i〇 X 2耵公釐）〜g 81.9.20,(V. Description of the invention (6) After printing and mixing by the Ministry of Industry and Information Technology, the above ... is added slowly, and the speed of the sample is measured during the package and pull mixing. The temperature is maintained. After the time clock c is connected, it is separated by [centrifuged at room temperature and centrifuged c dk 1800 Xg for 10 minutes]. The reaction solution is divided into upper and lower oil and water phases. The upper layer has a valence of 123 grams. After this, take Chu oil and continue to refine 121 grams of low-cholesterol lard under general decolorization and Ruan odor conditions. From crude oil cholesterol content of 86.8 gram / gram to 70 mg / muscle from depilation step, and then decolorization and deodorization by enveloping: to 8.5 milligrams of dying oil. The half is 90.7%. The decolorization and deodorization process does not change the cholesterol content. Example 2: Taking 50 grams of argan oil C lard, after refining processes such as blanching and dehydration, 137 grams of deacidification is obtained . Another 2.7 g < / Θ-type cyclodextrin was mixed with 68.5 g of water. After mixing, the above-mentioned decapitation was slowly added to carry out the inclusion-holding reaction. During the reaction, the stirring speed was 1100 rpm, and the temperature was maintained at 30 ° C. The stirring time was 10 minutes. After the inclusion, the reaction solution ii: connected at room temperature, separated by centrifugal centrifugation (woo xg, ίο min), and the reaction solution was divided into Upper and lower oil and water layers. The amount of oil separated from the upper layer was about 123 grams. This evening junbao package oil, followed by general decolorization, deodorization conditions refined into low-cholesterol refined naphtha oil, its cholesterol content is 14.5 mg / gak, cholesterol; ^ removal rate is about 83 3%. 〔Note〕 One of the conditions of refined oil: ⑴ water: add 30% water (measured by the amount of oil), 85 X: heat for 25 minutes. ⑵ Degumming: The amount of alkali varies according to the amount of free fatty acid in the oil. Remove the heating passage Ό, hold it for 15 minutes, and then separate the feet by telecentricity. (3) Decolorization: add 1.5% of activated clay, take it under vacuum at 120 ° C, and cool it. The paper size is in accordance with China National Standard (CNS) A 4 specifications (2i〇 X 2 mm) ~ g 81.9.20, (
(請先閱¾背面之iit.本5?再項^本頁J 丨裝. 訂_ .線- 210280 A6 五、發明説明（7 ) 後將白土濾去卽可。 ⑷脱臭：以蒸汽加熱主24〇 X：，在真空狀锚 ^ ’利用高壓茨汽 蒸餾脱除#發物，约1小時後令却。 “·、八 綜上所述，本發明於精製褚油的裳造 艰各·中選择脱駿後 之步驟加入經和水混合具包接作用 < 多醣麵 7邮颊C敁糊精）與油 中膽固醇包接結合，再以遠心分離機將包接物分離去除而製 成低膽固醇精製豬油的方法，不僅具有新頴性且具賓直業上 疋利用償值，合於發明專利要件。 圖式簡單説明： 第一阖為本發明製造流程設備闺。 {請先聞:*背面之ίχϊ承項Λ-^ϊίτ 本π) 裝. 訂' -線- 經濟部中央標準局R工消费合作社印製 衣纸張尺度通用中因國家標準（CNS〉甲4规格UlO X 297公货） 81.9.20,000 210280(Please read ¾ iit on the back. This 5? Then item ^ This page J 丨 Install. Order _. Line-210280 A6 5. Description of the invention (7) After filtering the white clay to remove it. ⑷ Deodorization: heating the main with steam 24〇X :, in a vacuum-like anchor ^ 'removal of # hairs using high-pressure Ci steam distillation, about 1 hour later ordered. "·, Eight summary As mentioned above, the present invention is difficult to make the refined Chu oil Choose the step after the dehydration, add the inclusion effect of mixed with water < polysaccharide noodle 7 post buccal C dextrin) and combine with cholesterol in the oil, and then separate and remove the inclusion with a telecentric separator The method for refining lard with low cholesterol is not only new but also has a direct utilization value, which is in accordance with the requirements of the invention patent. Brief description of the diagram: The first switch is the manufacturing process equipment of this invention. {Please first Smell: * The back side of the item Λ- ^ ϊίτ this π) installed. Order '-line-Ministry of Economic Affairs Central Standards Bureau R Industrial and Consumer Cooperatives printed clothing paper scales common in the national standard (CNS> A 4 specifications UlO X 297 public goods) 81.9.20,000 210280
AG HG 經濟部中央標準局β:工消费合作社印製 五、發明説明（1 ) 發明背景： 本發明係有關於一種低膽固醇精製褚油的t i^法， 尤指一種籍着多酿類的包接作用，而把豬油中大邯份（膽 固醇分離去除，並將此包接脱除技衡適當的結合;田脂精練 技衡，而製成低膽固醇精製褚油的方法。 錄油係從肥緒肉塊中經高溫炸出，以往家庭多半瓦接 使用炸出之耝油，近年食品加工業者甚至將粗初進一步精 製，以除去粗油中㈣離脂肪駿，〔磷脂質）和其他 中性油以外的雜質，而達到史安定衛吐仏 』文弋術生的油脂品質，惟這 種精製緒湳仍含有高量的膽固醇，食用 玉用過多，仍嘗對人妞 健康造成威脅。 發明概述： 本發明之目的係在提供一種低膽固 、 、呢M岭精製褚油的製造 才法，亦係在褚油的精装過程中，選 & $阢騣後的步驟，加 入經和水相混合《具包接作用多酿類c環糊精）與油中膽 固醇包接結合，再以遠心分離機將包接物分離去除，而製 成低膽固醇精製豬；·田。 發明的詳細説明： 本發明之製造才法及流程進一步 7文》f細説明如下. 本發明係在豬油的精製過程中加入經和水混4包接 作用〈多醣類（環糊精）興油中膽阁醇包接結合：存將此 包接物脱陳而製成低膽闺醇精製锖油的才法，其策糕包括 有—股褚油精製所需之：水支，、脱色、脱臭及消關 本發明尤包接脱除等流程。 表紙張λ賴用中_家標準祕（21〇 X 297 1 -------I-----------------裝------.玎------線 <請先閱^背面之注*事碣再瑣寫本頁)AG HG Ministry of Economic Affairs Central Standards Bureau β: Printed by the Industrial and Consumer Cooperatives V. Description of the invention (1) Background of the invention: The present invention relates to a ti ^ method for refining Chu oil with low cholesterol, especially a bag with multiple brews The method is to separate the large portion of the lard from the lard (cholesterol is separated and removed, and the entrapment is removed to properly combine the technical balance; Tian Zhi refines the technical balance, and a method of making low cholesterol refined Chu oil. The fat pieces of the fat are fried at high temperature. In the past, most families used frying oil. In recent years, the food processing industry has even further refined the crude oil to remove the fat from the crude oil (phospholipid) and other Impurities other than sexual oils achieve the quality of oils and fats produced by Wen Yizhu, Shi'an Dingwei, but this refined syrup still contains high amounts of cholesterol. Too much consumption of jade is still a threat to human health. Summary of the invention: The purpose of the present invention is to provide a method for manufacturing low-solid, refined, and M Ling refined Chu oil, and also to select the steps after the selection of & $ 阢 騣 in the refined process of Chu oil. Aqueous mixture "multi-brewed c cyclodextrin with entrapment effect" is combined with cholesterol entrapment in oil, and then the inclusions are separated and removed with a telecentric separator to make a low-cholesterol refined pig; Tian. Detailed description of the invention: The manufacturing method and process of the present invention are further described in Article 7 "f. The detailed description is as follows. The present invention is in the process of lard refining by adding and mixing with water 4 inclusion effect <polysaccharides (cyclodextrin) The combination of choline alcohol in Xingyou: The method of making this low-cholesterol refined oil by de-aging the inclusions, the strategy includes the one needed for the refining of Chu oil: Shuizhi ,, Decolorization, deodorization and elimination of the process of the present invention, especially including removal and removal. Table paper λ relying on _ home standard secret (21〇X 297 1 ------- I ----------------- installed ------. 玎------ Line < Please read ^ Notes on the back ^ * Just write this page)
210280 五、發明說明（3 ) …一 3.5%，而水約 /约30〜 用里为砀间脂量灸〇·5主0.75倍），並 〜骀Ό之溫度下攪拌约15〜75分θ <α κ λ, <多酷類c環糊精）… 具包接作用 包接結n〈中而f中之膽固醇 丹乂*恤达心分離機將此包接物脱 《膽固稃即被分離去徐而辑 接作用 < 多醣類c環糊精） 、匕 .^ 禾i接扠除锖油中膽闺醇，包 接反應<各項條件C包括環糊精用量，攪 匕 間）均會影響心中膽固 θ 〜’挽拌時 猜油（、…不二Π '，兹…説明未精製 …接條件作用後，膽固醇锋餘之情形 f%先閲讀背面之注念事Jfl再場寫本頁> 經濟部中央標準局員工消費合作社印製 膽固醇蜂餘量 _ — τ供。妖脒f 環糊精用210280 V. Description of the invention (3)… a 3.5%, and the water is about / about 30 ~ with the amount of moxibustion moxibustion (5 times 0.75 times), and ~ 15 ~ 75 minutes θ at the temperature of 骀 Ό < α κ λ, < Duoku class c cyclodextrin)… With the inclusion effect, the inclusion junction n <in the middle and f in the cholesterol Dan ** Tarson separator removes the inclusions from the ‘gules That is, it is separated from the Xu Erji connection < polysaccharide c cyclodextrin), dagger. ^ Wo i joint fork to remove gallbladder alcohol in the oil, inclusion reaction < each condition C includes the amount of cyclodextrin, Stirring the dagger) will affect the heart's guts θ ~ 'Guess the oil when mixing (、 ... 不二 Π', here ... explain the unrefined ... after the condition is applied, the cholesterol front excess f% first read the note on the back Thing Jfl writes this page again> The Ministry of Economic Affairs Central Standards Bureau employee consumer cooperatives print cholesterol bee margin _ — τ for. Yaoxuan f cyclodextrin use
由表一顯示，具包^ ^ ^ c * 參紙張认適用中咖家惊準（CN’S>甲4悦格（训χ 297公货）—As shown in Table 1, the package ^ ^ ^ c * can be used in the Chinese papers (CN ’S > A 4 Yuege (Xun 297 public goods) —