TW202338889A - Back-scatter electrons (bse) imaging with a sem in tilted mode using cap bias voltage - Google Patents

Back-scatter electrons (bse) imaging with a sem in tilted mode using cap bias voltage Download PDF

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TW202338889A
TW202338889A TW111111902A TW111111902A TW202338889A TW 202338889 A TW202338889 A TW 202338889A TW 111111902 A TW111111902 A TW 111111902A TW 111111902 A TW111111902 A TW 111111902A TW 202338889 A TW202338889 A TW 202338889A
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electrons
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葉胡達 哲
尹格爾 彼得羅夫
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以色列商應用材料以色列公司
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Abstract

A method of evaluating a region of a sample, the method comprising: positioning a sample within a vacuum chamber; generating an electron beam with a scanning electron microscope (SEM) column that includes an electron gun at one end of the column and a column cap at an opposite end of the column; focusing the electron beam on the sample and scanning the focused electron beam across the region of the sample, while the SEM column is operated in tilted mode, thereby generating secondary electrons and backscattered electrons from within the region; and during the scanning, collecting backscattered electrons with one or more detectors while applying a negative bias voltage to the column cap to alter a trajectory of the secondary electrons preventing the secondary electrons from reaching the one or more detectors.

Description

使用帽偏壓以傾斜模式的掃描式電子顯微鏡(SEM)作反散射電子(BSE)成像Scanning electron microscopy (SEM) in tilt mode using cap bias for backscattered electron (BSE) imaging

本申請案主張申請於2021年4月28日的美國申請案第17/243,478號的優先權。該案之揭示內容為了所有目的藉由引用之方式全部併入本文。This application claims priority from U.S. Application No. 17/243,478 filed on April 28, 2021. The disclosures of this case are incorporated herein by reference in their entirety for all purposes.

在電子材料及用於製造該等材料至電子結構中的製程的研究中,電子結構的樣本可用於微觀檢查,以便用於故障分析及裝置驗證的目的。例如,諸如矽晶圓的電子結構的樣本可在掃描式電子顯微鏡(scanning electron microscope; SEM)中得以分析以研究晶圓中的特定特性特徵。該特性特徵可包括製造的電路及在製造製程期間形成的任何缺陷。電子顯微鏡為一種用於分析半導體裝置的顯微結構的最有用的設備件之一者。In the study of electronic materials and processes used to fabricate such materials into electronic structures, samples of electronic structures may be used for microscopic examination for the purpose of failure analysis and device verification. For example, a sample such as the electronic structure of a silicon wafer can be analyzed in a scanning electron microscope (SEM) to study specific characteristics in the wafer. The characteristics may include the fabricated circuit and any defects formed during the manufacturing process. An electron microscope is one of the most useful pieces of equipment for analyzing the microstructure of semiconductor devices.

當使用來自SEM工具的電子束檢查樣品時,二次電極及反散射電子在電子束撞擊樣品時產生。二次電子源於樣品自身的原子並且為電子束與樣品之間的非彈性相互作用的結果。二次電子的能量相對較低(例如,0-20 eV)並且源於樣品表面或在樣品表面附近。在射束與樣品之間的彈性相互作用之後,反散射電子(backscattered electron; BSE)得以反射回。反散射電子可具有接近於電子束的能量位準的能量位準,並且從而可來自樣品的更深的區域。When a sample is examined using an electron beam from an SEM tool, secondary electrodes and backscattered electrons are created when the electron beam strikes the sample. Secondary electrons originate from the atoms of the sample itself and are the result of inelastic interactions between the electron beam and the sample. Secondary electrons have relatively low energy (e.g., 0-20 eV) and originate from or near the sample surface. After elastic interaction between the beam and the sample, backscattered electrons (BSE) are reflected back. The backscattered electrons may have an energy level close to that of the electron beam, and thus may originate from deeper regions of the sample.

因為該等及其他差異,二次電子及反散射電子可提供不同類型的資訊。二次電子可提供關於樣品的詳細表面資訊,而反散射電子顯示對原子序數差異的高靈敏度,且從而在使物體成像時用於提供材料對比度。Because of these and other differences, secondary electrons and backscattered electrons can provide different types of information. Secondary electrons can provide detailed surface information about the sample, while backscattered electrons show high sensitivity to differences in atomic number and are thus used to provide material contrast when imaging objects.

通常,二次電子產率比反散射電子產率高得多。因此,當收集反散射電子時,二次電子信號需要經抑制以準確地看到反散射電子信號。在典型SEM工具中,抑制二次電子信號可藉由在樣品與偵測器之間置放能量濾波器來完成,以便該能量濾波器阻止相對低能量的二次電子到達偵測器。雖然此方法已在過去成功地使用,但仍需要偵測反散射電子的新的方法。Typically, the secondary electron yield is much higher than the backscattered electron yield. Therefore, when backscattered electrons are collected, the secondary electron signal needs to be suppressed to accurately see the backscattered electron signal. In a typical SEM tool, suppression of secondary electron signals is accomplished by placing an energy filter between the sample and detector so that the energy filter prevents relatively low-energy secondary electrons from reaching the detector. Although this method has been used successfully in the past, new methods of detecting backscattered electrons are needed.

本案的一些實施例涉及當以掃描電子顯微鏡使樣品成像時,用於收集反散射電子的改良的方法及技術。經收集的電子可用於評估樣品的特性,諸如以提供材料對比度。Some embodiments of the present invention relate to improved methods and techniques for collecting backscattered electrons when imaging a sample with a scanning electron microscope. The collected electrons can be used to evaluate properties of the sample, such as to provide material contrast.

在一些實施例中,一種評估樣品的區域的方法包括:將樣品定位在真空腔室中;用掃描式電子顯微鏡(SEM)柱產生電子束,該掃描式電子顯微鏡柱包括在柱的一端處的電子槍及在該柱的相對端處的柱帽;將電子束聚焦在樣品上並且橫跨樣品區域掃描經聚焦的電子束,同時SEM柱以傾斜模式操作,從而自區域之內產生二次電子及反散射電子;並且在掃描期間,利用一或多個偵測器收集反散射電子,同時施加負偏壓至柱帽以改變二次電子的軌跡,從而防止二次電子到達一或多個偵測器。In some embodiments, a method of evaluating an area of a sample includes: positioning the sample in a vacuum chamber; generating an electron beam with a scanning electron microscope (SEM) column including at one end of the column Electron guns and column caps at opposite ends of the column; focus the electron beam on the sample and scan the focused electron beam across the sample area while the SEM column is operated in tilt mode, thereby generating secondary electrons from within the area and Anti-scattered electrons; and during scanning, use one or more detectors to collect anti-scattered electrons, while applying a negative bias to the column cap to change the trajectory of secondary electrons, thereby preventing secondary electrons from reaching one or more detectors device.

本文所述的實施例的各種實施可包括一或多個以下特徵。從經偵測的反散射電子產生區域的至少一部分的影像。施加負50伏及負1000伏的負偏壓至柱帽。施加負100伏與負500伏之間的負偏壓至柱帽。柱帽可具有在其尖端有開口的錐形形狀,並且電子束可經引導穿過該開口。反散射電子可利用透鏡內偵測器及頂部偵測器來收集。反散射電子可利用外部偵測器來收集。Various implementations of the embodiments described herein may include one or more of the following features. An image of at least a portion of the area is generated from the detected backscattered electrons. Negative bias voltages of minus 50 volts and minus 1000 volts were applied to the column caps. Apply a negative bias voltage between minus 100 volts and minus 500 volts to the post cap. The column cap may have a tapered shape with an opening at its tip, and the electron beam may be directed through the opening. Backscattered electrons can be collected using in-lens detectors and top detectors. Backscattered electrons can be collected using external detectors.

一些實施例涉及儲存指令的非暫態電腦可讀媒體,該等指令用於根據上文或本文中的任何方法對樣本的區域進行X射線光譜表面材料分析。例如,藉由以下方法:將樣品定位在真空腔室中;用掃描式電子顯微鏡(SEM)柱產生電子束,該掃描式電子顯微鏡柱包括在柱的一端處的電子槍及在該柱的相對端處的柱帽;將電子束聚焦在樣品上並且橫跨樣品區域掃描經聚焦的電子束,同時SEM柱以傾斜模式操作,從而自區域之內產生二次電子及反散射電子;並且在掃描期間,利用一或多個偵測器收集反散射電子,同時施加負偏壓至柱帽以改變二次電子的軌跡,從而防止二次電子到達一或多個偵測器。Some embodiments relate to a non-transitory computer-readable medium storing instructions for performing X-ray spectroscopic surface material analysis of a region of a sample according to any method above or herein. For example, by positioning the sample in a vacuum chamber and generating an electron beam with a scanning electron microscope (SEM) column including an electron gun at one end of the column and an electron gun at an opposite end of the column. the column cap at , using one or more detectors to collect backscattered electrons, while applying a negative bias to the column cap to change the trajectory of secondary electrons, thereby preventing secondary electrons from reaching one or more detectors.

一些實施例涉及用於根據上文或本文所述的任何方法對樣品的區域進行X射線光譜表面材料分析的系統。例如,該系統可包括:真空腔室;樣品支撐件,經配置以在樣品評估過程期間將樣品保持在真空腔室內;掃描電子顯微鏡(SEM)柱,經配置以將帶電粒子束朝向樣品引導至真空腔室中,該SEM柱包括在柱的一端處的電子槍及在柱的相對端處的柱帽;偵測器,經配置以偵測反散射電子;及處理器和耦合至處理器的記憶體。該記憶體可包括複數個電腦可讀指令,當該等指令由處理器執行時,使得系統以:將樣品定位在真空腔室中;用掃描式電子顯微鏡(SEM)柱產生電子束,該掃描式電子顯微鏡柱包括在柱的一端處的電子槍及在該柱的相對端處的柱帽;將電子束聚焦在樣品上並且橫跨樣品區域掃描經聚焦的電子束,同時SEM柱以傾斜模式操作,從而自區域之內產生二次電子及反散射電子;並且利用一或多個偵測器收集反散射電子,同時施加負偏壓至柱帽以改變二次電子的軌跡,從而防止二次電子到達一或多個偵測器。Some embodiments relate to systems for X-ray spectroscopic surface material analysis of a region of a sample according to any of the methods described above or herein. For example, the system may include: a vacuum chamber; a sample support configured to maintain the sample within the vacuum chamber during the sample evaluation process; and a scanning electron microscope (SEM) column configured to direct a charged particle beam toward the sample. In a vacuum chamber, the SEM column includes an electron gun at one end of the column and a column cap at an opposite end of the column; a detector configured to detect backscattered electrons; and a processor and memory coupled to the processor body. The memory may include a plurality of computer-readable instructions that, when executed by the processor, cause the system to: position a sample in a vacuum chamber; generate an electron beam using a scanning electron microscope (SEM) column; and the scanning An electron microscope column includes an electron gun at one end of the column and a column cap at an opposite end of the column; an electron beam is focused on a sample and the focused electron beam is scanned across the sample area while the SEM column is operated in a tilt mode , thereby generating secondary electrons and backscattered electrons from within the area; and using one or more detectors to collect backscattered electrons, while applying a negative bias to the column cap to change the trajectory of secondary electrons, thereby preventing secondary electrons Reach one or more detectors.

為了更好地理解本案之性質及優點,應對以下描述及附圖進行參考。然而,應理解,每一附圖僅是提供用於說明之目的,並且並不意欲作為本案範圍的限制的定義。此外,作為一般規則,且除非從描述中明顯相反,在不同附圖中的元件使用相同元件符號的情況下,該等元件通常是相同的或至少在功能或用途上相似。In order to better understand the nature and advantages of this case, reference should be made to the following description and accompanying drawings. It is to be understood, however, that each drawing is provided for the purpose of illustration only and is not intended as a definition of the limits of the scope of the invention. Furthermore, as a general rule, and unless the contrary is apparent from the description, where the same reference numerals are used for elements in different figures, such elements will generally be identical or at least similar in function or purpose.

本案的實施例涉及當以掃描電子顯微鏡使樣品成像時,用於收集反散射電子的改良的方法及技術。 示例性樣品評估工具 Embodiments of the present application relate to improved methods and techniques for collecting backscattered electrons when imaging a sample with a scanning electron microscope. Exemplary Sample Evaluation Tool

為了更好地理解和瞭解本案,首先參考第1圖,該圖為根據本案的一些實施例的樣品評估系統100的簡化示意圖。除了其他操作之外,樣品評估系統100可尤其用於形成在樣品(諸如半導體晶圓)上的結構的缺陷檢查及分析。In order to better understand and understand this case, first refer to Figure 1 , which is a simplified schematic diagram of a sample evaluation system 100 according to some embodiments of this case. Sample evaluation system 100 may be used, among other operations, for defect inspection and analysis of structures formed on samples, such as semiconductor wafers.

系統100可包括真空腔室110以及掃描電子顯微鏡(SEM)柱120。支撐元件150可在處理操作期間支撐腔室110內的樣品145(例如,半導體晶圓),在該處理操作中,樣品145(在本文中有時稱為「物體」或「樣本」)受到來自SEM柱的帶電粒子束126的影響。System 100 may include a vacuum chamber 110 and a scanning electron microscope (SEM) column 120 . Support element 150 may support sample 145 (eg, a semiconductor wafer) within chamber 110 during processing operations in which sample 145 (sometimes referred to herein as an "object" or "sample") is subjected to Effect of charged particle beam 126 on the SEM column.

SEM柱120連接到真空腔室110,以便由該柱產生的帶電粒子束在撞擊樣品145之前傳播穿過在真空腔室110內形成的真空環境。SEM柱120可藉由用帶電粒子束126照射樣本、偵測歸因於照射而發射的粒子並基於偵測到的粒子產生帶電粒子影像來產生樣本145的一部分的影像。為此,SEM柱120可包括電子束源122(亦即「電子槍」)、限定電子束漂移空間的陽極管128、聚光透鏡裝置124、一或多個偏轉透鏡(諸如透鏡130、132)、一或多個聚焦透鏡134及柱帽136。SEM column 120 is connected to vacuum chamber 110 so that the charged particle beam generated by the column propagates through the vacuum environment created within vacuum chamber 110 before impacting sample 145 . SEM column 120 can produce an image of a portion of sample 145 by illuminating the sample with charged particle beam 126, detecting particles emitted due to the illumination, and generating a charged particle image based on the detected particles. To this end, SEM column 120 may include an electron beam source 122 (i.e., an "electron gun"), an anode tube 128 that defines the electron beam's drift space, a condenser lens assembly 124, one or more deflection lenses (such as lenses 130, 132), One or more focusing lenses 134 and column cap 136.

在成像製程中,電子束源122產生電子束126,該電子束126傳遞穿過聚光透鏡124並最初由聚光透鏡124會聚,然後在撞擊樣品145之前由透鏡134聚焦。聚光透鏡124定義了與解析度直接相關的電子束的數值孔徑和電流(連同最終孔徑),同時聚焦透鏡134將電子束聚焦到樣品上。位於陽極管128(第一電極)的下端與样品145(第二電極)之間的柱帽136可為系統中的第三電極,其調節在晶圓附近產生的電場。During the imaging process, electron beam source 122 generates electron beam 126 that passes through and is initially focused by condenser lens 124 and then by lens 134 before impacting sample 145 . The condenser lens 124 defines the numerical aperture and current of the electron beam (together with the final aperture) which are directly related to the resolution, while the focusing lens 134 focuses the electron beam onto the sample. Post cap 136 located between the lower end of anode tube 128 (first electrode) and sample 145 (second electrode) can be a third electrode in the system that regulates the electric field generated near the wafer.

粒子成像製程通常包括在經成像的樣品的特定區域上來回掃描帶電粒子束(例如,以光柵或其他掃描圖案)。可為磁透鏡、靜電透鏡或電透鏡與磁透鏡的組合的偏轉透鏡130、132,可實現熟習該項技術者已知的掃描圖案。經掃描的區域典型地為樣品的整體區域的非常小一部分。例如,樣品可為直徑為200 mm或300 mm的半導體晶圓,而晶圓上掃描的每一區域可為具有以微米或數十微米測量的寬度及/或長度的矩形區域。Particle imaging processes typically involve scanning a charged particle beam back and forth (eg, in a raster or other scanning pattern) over a specific area of the imaged sample. Deflection lenses 130, 132, which may be magnetic lenses, electrostatic lenses, or a combination of electrolenses and magnetic lenses, may achieve scanning patterns known to those skilled in the art. The scanned area is typically a very small portion of the overall area of the sample. For example, the sample may be a 200 mm or 300 mm diameter semiconductor wafer, and each area scanned on the wafer may be a rectangular area having a width and/or length measured in microns or tens of microns.

SEM柱120亦可包括一或多個偵測器以在成像製程期間偵測自樣品產生的帶電粒子。例如,SEM柱120可包括透鏡內偵測器162及頂部偵測器144,該等偵測器可經配置以偵測由於帶電粒子束126照射樣品的結果發射的二次電子及反散射電子。透鏡內偵測器142可包括中心孔,該中心孔允許帶電粒子束126穿過偵測器並允許進入帶電粒子柱120的二次電子及反散射電子穿過偵測器142到達頂部偵測器144。在一些實施例中,樣品評估系統120亦可包括外部偵測器(下文關於第6圖所論述),該外部偵測器亦可經配置以偵測二次和反散射電子。SEM column 120 may also include one or more detectors to detect charged particles generated from the sample during the imaging process. For example, SEM column 120 may include an in-lens detector 162 and a top detector 144 that may be configured to detect secondary electrons and backscattered electrons emitted as a result of charged particle beam 126 illuminating a sample. The in-lens detector 142 may include a central aperture that allows the charged particle beam 126 to pass through the detector and allows secondary electrons and backscattered electrons entering the charged particle column 120 to pass through the detector 142 to the top detector. 144. In some embodiments, sample evaluation system 120 may also include an external detector (discussed below with respect to Figure 6), which may also be configured to detect secondary and backscattered electrons.

另外,系統100可包括電壓供應源160及一或多個控制器170,諸如處理器或其他硬體單元。電壓供應源可經操作以提供所需的柱的有效電壓,以從而提高影像解析度。此舉可藉由在第一電極與第二電極之間(亦即,在陽極管與樣品之間)適當分配電壓供應來達成。控制器170可藉由執行儲存於一或多個電腦可讀記憶體180中的電腦指令來控制系統(包括電壓供應源160)的操作,如將由一般技藝人士所知。舉例而言,電腦可讀記憶體可包括固態記憶體(諸如隨機存取記憶體(random access memory; RAM)及/或唯讀記憶體(read-only memory; ROM),該記憶體可為可程式化的、可快閃記憶體更新的及/或其類似者)、磁碟驅動器、光學儲存裝置或類似的非暫態電腦可讀儲存媒體。Additionally, system 100 may include a voltage supply 160 and one or more controllers 170, such as a processor or other hardware unit. The voltage supply can be operated to provide a desired effective voltage of the column to thereby enhance image resolution. This can be achieved by appropriately distributing the voltage supply between the first and second electrodes (ie, between the anode tube and the sample). Controller 170 may control the operation of the system, including voltage supply 160, by executing computer instructions stored in one or more computer-readable memories 180, as will be known to those of ordinary skill in the art. For example, computer-readable memory may include solid-state memory (such as random access memory (RAM) and/or read-only memory (ROM)), which may be programmable, flash-updatable and/or the like), disk drives, optical storage devices or similar non-transitory computer-readable storage media.

如第1圖中所示,實施例允許SEM柱120相對於樣品145以非垂直角度傾斜。例如,如第1圖中所示,柱120可相對於樣品145的上部大體上平坦表面以45度的角度傾斜。為了使柱120能夠傾斜,帽136可具有使柱能夠非常靠近樣品145定位而不使柱帽136與樣品碰撞的錐形形狀。此外,且如下文所述,在一些實施例中,SEM柱120不包括能量濾波器,該能量濾波器由一些SEM工具使用以防止二次電子到達透鏡內偵測器142。或者,在一些實施例中,SEM柱120可包括能量濾波器,但可用於在不啟動能量濾波器的情況下評估樣品。 在收集反散射電子中的挑戰 As shown in Figure 1, embodiments allow the SEM column 120 to be tilted at non-vertical angles relative to the sample 145. For example, as shown in Figure 1, post 120 may be tilted at a 45 degree angle relative to the upper generally flat surface of sample 145. To enable tilting of column 120, cap 136 may have a tapered shape that enables the column to be positioned very close to sample 145 without colliding column cap 136 with the sample. Additionally, and as described below, in some embodiments, SEM column 120 does not include an energy filter used by some SEM tools to prevent secondary electrons from reaching in-lens detector 142 . Alternatively, in some embodiments, the SEM column 120 may include an energy filter but may be used to evaluate samples without activating the energy filter. Challenges in collecting backscattered electrons

如上所述,一些實施例在不使用能量濾波器來抑制二次離子信號的情況下收集反散射電子。為了更好地瞭解一些實施例的優點及益處,現參考第2圖,該圖為與樣品245間隔開的SEM柱200的一部分的簡化示意圖。SEM柱200可表示第1圖中所示的SEM柱120。為了便於圖示,在第2圖中僅圖示了SEM柱200的所選元件。如圖所示,SEM柱200包括在柱遠端的柱帽236、透鏡內偵測器242及頂部偵測器244。亦圖示了陽極管210的一部分。As discussed above, some embodiments collect backscattered electrons without using energy filters to suppress secondary ion signals. To better understand the advantages and benefits of some embodiments, reference is now made to Figure 2, which is a simplified schematic illustration of a portion of SEM column 200 spaced apart from sample 245. SEM column 200 may represent SEM column 120 shown in Figure 1 . For ease of illustration, only selected elements of the SEM column 200 are illustrated in Figure 2 . As shown, SEM column 200 includes a column cap 236 at the distal end of the column, an in-lens detector 242, and a top detector 244. A portion of anode tube 210 is also shown.

在成像操作期間,SEM柱200產生電子束(未圖示)並引導電子束,以使得電子束撞擊樣品245。電子束與樣品245的相互作用產生各種二次電子及反散射電子,該等電子在所有方向上行進遠離樣品。一些產生之電子的路徑圖示為路徑250、路徑252及路徑254。如圖所示,一些產生的電子沿著路徑250行進遠離SEM柱並且因此無法到達偵測器242或244中的任一者;一些產生的電子沿著路徑252行進,該路徑252在使得電子撞擊在透鏡內偵測器242上的軌跡進入SEM柱;且一些產生的電子沿著路徑254行進,該路徑在使電子能夠傳遞穿過透鏡內偵測器242的中心開口到達頂部偵測器244的軌跡上進入SEM柱。During imaging operations, SEM column 200 generates an electron beam (not shown) and directs the electron beam such that the electron beam strikes sample 245 . The interaction of the electron beam with the sample 245 produces various secondary electrons and backscattered electrons that travel away from the sample in all directions. The paths of some of the generated electrons are illustrated as path 250, path 252, and path 254. As shown, some of the generated electrons travel along path 250 away from the SEM column and therefore fail to reach either detector 242 or 244; some of the generated electrons travel along path 252 which causes the electrons to impact The trajectory on the in-lens detector 242 enters the SEM column; and some of the generated electrons travel along a path 254 that enables the electrons to pass through the central opening of the in-lens detector 242 to the top detector 244 Enter the SEM column on the track.

在設定為收集反散射電子的一些先前已知的SEM工具中,SEM柱包括如第3圖中所示的能量濾波器310。可藉由防止低於預定能量位準的電子傳過濾波器來將反散射電子與二次電子分離的能量濾波器310,該濾波器通常正好位於頂部偵測器244之前。因此,包括SEM柱300的評估系統僅可看到沿著路徑254並到達頂部偵測器244的反散射電子。沿路徑252行進並到達偵測器242的電子將包括二次電子及反散射電子。由於偵測器242無法區分不同類型的電子,因此透鏡內偵測器242不能用於將反散射電子信號與二次電子信號隔離。此外,沿路徑250的反散射電子將不會到達偵測器242或244中的任一者。 將負偏壓施加至柱帽 In some previously known SEM tools configured to collect backscattered electrons, the SEM column includes an energy filter 310 as shown in Figure 3. An energy filter 310 that can separate backscattered electrons from secondary electrons by preventing electrons below a predetermined energy level from passing through the filter. This filter is typically located just before the top detector 244. Therefore, an evaluation system including SEM column 300 will only see backscattered electrons that follow path 254 and reach top detector 244 . Electrons traveling along path 252 and reaching detector 242 will include secondary electrons and backscattered electrons. Since detector 242 cannot distinguish between different types of electrons, in-lens detector 242 cannot be used to isolate backscattered electron signals from secondary electron signals. Furthermore, backscattered electrons along path 250 will not reach either detector 242 or 244. Apply negative bias to column cap

根據本文揭示的一些實施例,SEM柱(例如,柱120或200)可在傾斜模式下操作(例如,與樣品成45度角或其他非垂直角)並且負偏壓可在成像過程中經施加至柱帽以抑制二次電子到達任何電子偵測器(包括比柱帽離樣品更遠的透鏡內偵測器142、242及頂部偵測器144、244)。According to some embodiments disclosed herein, a SEM column (eg, column 120 or 200) can be operated in a tilted mode (eg, at a 45 degree angle or other non-vertical angle to the sample) and a negative bias can be applied during imaging. to the column cap to inhibit secondary electrons from reaching any electronic detectors (including in-lens detectors 142, 242 and top detectors 144, 244 that are farther from the sample than the column cap).

第4圖為根據一些實施例的圖示與使樣品成像的方法400相關聯的步驟的簡化流程圖。方法400藉由將樣品定位在樣品評估系統的處理腔室之內開始(步驟410)。可為例如腔室110的處理腔室可包括,可以傾斜模型操作的SEM柱及一或多個電子偵測器,諸如透鏡內偵測器142或頂部偵測器144。步驟410可包括將樣品(諸如樣品145)定位在真空腔室之內的樣品支撐件(諸如支撐件150)上。Figure 4 is a simplified flowchart illustrating steps associated with a method 400 of imaging a sample, in accordance with some embodiments. Method 400 begins by positioning a sample within a processing chamber of a sample evaluation system (step 410). A processing chamber, such as chamber 110, may include a SEM column that can be operated with a tilt model and one or more electronic detectors, such as an in-lens detector 142 or a top detector 144. Step 410 may include positioning the sample, such as sample 145, on a sample support, such as support 150, within the vacuum chamber.

接下來,將負偏壓施加至柱帽(步驟420),且SEM柱可經啟動以產生電子束(步驟430),該電子束經聚焦並掃描跨過樣品的感興趣區域(步驟440)。電子束可經由諸如透鏡134之類的聚焦透鏡聚焦,並且電子束可用諸如透鏡130和132之類的一或多個偏轉透鏡來掃描跨過基板的一區域。Next, a negative bias voltage is applied to the column cap (step 420), and the SEM column can be activated to generate an electron beam (step 430) that is focused and scanned across the region of interest of the sample (step 440). The electron beam may be focused via a focusing lens, such as lens 134, and the electron beam may be scanned across an area of the substrate using one or more deflection lenses, such as lenses 130 and 132.

當電子束掃描跨過感興趣的區域時,負偏壓經施加至柱帽上。負偏壓應該足夠高以抑制二次電子,但它不應該高到影響電子束126,這將對成像過程的解析度產生不利影響。在向柱帽施加負偏壓的時,且當電子束掃描跨過感興趣區域時,可用適當的偵測器收集反散射電子,該偵測器諸如透鏡內偵測器142或頂部偵測器144(步驟450)。在實際實施中,步驟430、440及450可以基本上同時發生並且可非常快。As the electron beam scans across the area of interest, a negative bias voltage is applied to the column cap. The negative bias should be high enough to suppress secondary electrons, but it should not be high enough to affect the electron beam 126, which would adversely affect the resolution of the imaging process. When a negative bias is applied to the column cap, and as the electron beam scans across the region of interest, the backscattered electrons can be collected with an appropriate detector, such as an in-lens detector 142 or a top detector. 144 (step 450). In an actual implementation, steps 430, 440, and 450 may occur substantially simultaneously and may be very fast.

在一些實施例中,負偏壓可為抑制二次電子所需的最小電壓。負偏壓的適當值將部分地取決於柱帽的幾何形狀,並且可穿過如可由熟習該項技術者容易地確定的模擬或實驗來確定。在一些實施例中,偏壓可在負50與負1000伏之間;並且在其他實施例中,偏壓可在負100與負500伏之間。In some embodiments, the negative bias voltage may be the minimum voltage required to suppress secondary electrons. The appropriate value of negative bias will depend in part on the geometry of the pillar cap and can be determined through simulation or experimentation as can be readily determined by one skilled in the art. In some embodiments, the bias voltage may be between negative 50 and negative 1000 volts; and in other embodiments, the bias voltage may be between negative 100 and negative 500 volts.

第5A圖及第5B圖為圖示根據一些實施例的將負偏壓施加至SEM柱500的帽的影響的簡化圖。SEM柱500可表示上文論述的SEM柱120或200。特定而言,第5A圖圖示向SEM柱500的帽236施加200伏的負電壓對在成像操作期間產生的二次電子510的影響,且第5B圖圖示將相同的負電壓(200伏)施加至帽236對反散射電子520的影響。在第5A圖及第5B圖的每一者中,SEM柱500在成像過程期間產生1 kV的電子束。Figures 5A and 5B are simplified diagrams illustrating the effects of applying a negative bias voltage to the cap of SEM column 500 in accordance with some embodiments. SEM column 500 may represent SEM column 120 or 200 discussed above. Specifically, Figure 5A illustrates the effect of applying a negative voltage of 200 volts to cap 236 of SEM column 500 on secondary electrons 510 produced during imaging operations, and Figure 5B illustrates applying the same negative voltage (200 volts ) applied to the effect of cap 236 on backscattered electrons 520 . In each of Figures 5A and 5B, SEM column 500 generates a 1 kV electron beam during the imaging process.

從基於模擬結果的第5A圖及第5B圖的比較可看出,負電壓排斥較低能量的二次電子,以便無二次電子510進入SEM柱500。因此,施加負帽電壓確保沒有二次電子510可到達柱500內的透鏡內或頂部偵測器(第5A圖或第5B圖中未示出)。相反,向帽236施加負電壓對較高能量的反散射電子520的影響最小。因此,一些反散射電子沿著進入SEM柱的路徑行進,到達透鏡內偵測器或頂部偵測器之一者,並使柱內倍的透鏡內偵測器能夠在不使用單獨的濾波器的情況下提供反散射信號。From a comparison of Figure 5A and Figure 5B based on simulation results, it can be seen that the negative voltage repels lower energy secondary electrons so that no secondary electrons 510 enter the SEM column 500. Therefore, applying a negative cap voltage ensures that no secondary electrons 510 can reach the in-lens or top detector within column 500 (not shown in Figure 5A or Figure 5B). In contrast, applying a negative voltage to cap 236 has minimal effect on higher energy backscattered electrons 520. Therefore, some of the backscattered electrons travel along the path into the SEM column, reaching either the in-lens detector or the top detector, and enable in-lens detectors within the column without the use of a separate filter. Provides backscattered signal.

第6A圖及第6B圖是SEM柱500的一部分的簡化圖,其圖示了當沒有偏壓(即,0伏的偏壓)經施加至電子帽時於成像期間產生的電子的示例性路徑。特定而言,第6A圖圖示當沒有偏壓經施加至帽236時的二次電子610的示例性軌跡,且第6B圖圖示當沒有偏壓施加至帽236時的反散射電子620的示例性軌跡。如第6B圖中可見,當200伏負偏壓施加至帽時,反散射電子620的軌跡與第5B圖中所示的反散射電子520的軌跡大體上相同。然而,如第6A圖中所示,在帽上無負偏壓的情況下,進入SEM柱500的一些二次電子610可從而到達透鏡內或頂部偵測器中的一者。由於偵測器無法區分二次電子與反散射電子,因此二次電子會污染偵測器處的信號,從而防止獲得準確的反散射信號。 利用外部偵測器的樣品評估工具 Figures 6A and 6B are simplified diagrams of a portion of SEM column 500 illustrating exemplary paths of electrons generated during imaging when no bias (i.e., a bias of 0 volts) is applied to the electron cap. . Specifically, Figure 6A illustrates an exemplary trajectory of secondary electrons 610 when no bias is applied to cap 236, and Figure 6B illustrates an example trajectory of backscattered electrons 620 when no bias is applied to cap 236. Example trajectories. As can be seen in Figure 6B, when a negative bias of 200 volts is applied to the cap, the trajectory of backscattered electrons 620 is substantially the same as the trajectory of backscattered electrons 520 shown in Figure 5B. However, as shown in Figure 6A, without a negative bias on the cap, some secondary electrons 610 entering the SEM column 500 may thereby reach one of the in-lens or top detectors. Since the detector cannot distinguish between secondary electrons and backscattered electrons, secondary electrons can contaminate the signal at the detector, preventing an accurate backscattered signal from being obtained. Sample evaluation tool using external detector

根據一些實施例的樣品評估工具可包括可用於偵測反散射電子的外部偵測器。外部偵測器可為上述透鏡內偵測器和頂部偵測器之一者或兩者的補充或替代。第7圖為根據本案的一些實施例的樣品評估系統700的簡化示圖。樣品評估系統700可類似於評估系統100,除了其包括外部偵測器710。為方便起見,與評估系統100類似的評估系統700的其他元件已用相同的元件符號標記並且在下文不再論述。Sample evaluation tools according to some embodiments may include an external detector that may be used to detect backscattered electrons. The external detector may be in addition to or in place of either or both of the in-lens detector and the top detector described above. Figure 7 is a simplified diagram of a sample evaluation system 700 according to some embodiments of the present invention. Sample evaluation system 700 may be similar to evaluation system 100 except that it includes an external detector 710 . For convenience, other elements of evaluation system 700 that are similar to evaluation system 100 have been labeled with the same element symbols and are not discussed below.

在樣品評估過程期間,評估系統700中的SEM柱120可相對於樣品145傾斜,如上文關於第1圖所論述。如第7圖中所示,外部偵測器710可與SEM柱的帽136間隔開並且定位成當樣品被電子束126轟擊時收集從樣品145產生的電子。雖然透鏡內偵測器142和頂部偵測器144限於偵測穿過帽136的開口進入SEM柱的反散射電子,但外部偵測器710可偵測具有將電子帶離SEM柱的軌跡的反散射電子。實施例可在成像過程期間向帽136施加負電壓以抑制二次電子信號(亦即,防止二次電子到達外部偵測器710)並確保外部偵測器710收集主要或僅包括反散射電子的信號。 待成像 的樣品實例 During the sample evaluation process, the SEM column 120 in the evaluation system 700 may be tilted relative to the sample 145 as discussed above with respect to FIG. 1 . As shown in FIG. 7 , external detector 710 may be spaced apart from cap 136 of the SEM column and positioned to collect electrons generated from sample 145 when the sample is bombarded by electron beam 126 . While in-lens detector 142 and top detector 144 are limited to detecting backscattered electrons entering the SEM column through the opening of cap 136, external detector 710 can detect backscattered electrons with trajectories that carry electrons away from the SEM column. Scattered electrons. Embodiments may apply a negative voltage to cap 136 during the imaging process to suppress secondary electron signals (i.e., prevent secondary electrons from reaching external detector 710) and ensure that external detector 710 collects primarily or only backscattered electrons. signal. Sample sample to be imaged

為了向本案中闡述的實施例的一些態樣提供上下文,現參考第8圖,該圖為根據一些實施例的半導體晶圓上的區域的簡化圖示,該區域可包括晶圓上不同位置處的多個區域,可從該等區域收集反散射電子以評估樣品。特定而言,第8圖包括晶圓800的俯視圖以及晶圓800的特定部分的兩個展開圖。晶圓800可為例如200 mm或300 mm的半導體晶圓,並且可包括形成在其上的多個積體電路810(在所示實例中為52個)。積體電路810可處於製造的中間階段,並且本文描述的樣品評估技術可用於評估和分析積體電路的一或多個區域820。例如,第8圖的展開圖A圖示了可根據本文所述的技術評估和分析的積體電路810之一者的多個區域820。展開圖B圖示了包括形成在其中的不同特徵的彼等區域820之一者。To provide context for some aspects of the embodiments described herein, reference is now made to FIG. 8, which is a simplified illustration of a region on a semiconductor wafer that may include various locations on the wafer in accordance with some embodiments. Multiple regions from which backscattered electrons can be collected to evaluate the sample. Specifically, FIG. 8 includes a top view of wafer 800 and two expanded views of specific portions of wafer 800 . Wafer 800 may be, for example, a 200 mm or 300 mm semiconductor wafer, and may include a plurality of integrated circuits 810 (52 in the example shown) formed thereon. The integrated circuit 810 may be in an intermediate stage of manufacturing, and the sample evaluation techniques described herein may be used to evaluate and analyze one or more areas 820 of the integrated circuit. For example, Expansion A of FIG. 8 illustrates multiple regions 820 of one of the integrated circuits 810 that may be evaluated and analyzed according to techniques described herein. Expansion B illustrates one of the regions 820 including different features formed therein.

本案的實施例可使用例如上文關於第4圖論述的方法400來分析和評估區域820。評估可藉由根據光柵圖案在區域820內來回掃描SEM束來完成,該光柵圖案諸如在第8圖的展開圖B中以簡化格式示出的掃描圖案830。 額外的實施例 Embodiments of the present invention may analyze and evaluate region 820 using, for example, method 400 discussed above with respect to FIG. 4 . Evaluation may be accomplished by scanning the SEM beam back and forth within area 820 according to a raster pattern, such as scan pattern 830 shown in simplified format in Expansion B of Figure 8. Additional Examples

出於說明和描述的目的,呈現本文描述的特定實施例的前述描述。該描述不意欲窮舉或將實施例限制為所揭示的精確形式。此外,雖然上文揭示了本案的不同實施例,但是可在不脫離本案實施例的精神和範疇的情況下以任何合適的方式組合特定實施例的具體細節。此外,對於一般技藝人士顯而易見的是,鑒於上述教示,許多修改和變化是可能的。The foregoing descriptions of the specific embodiments described herein have been presented for the purposes of illustration and description. This description is not intended to be exhaustive or to limit the embodiments to the precise forms disclosed. Furthermore, while different embodiments of the present invention are disclosed above, the specific details of the particular embodiments may be combined in any suitable manner without departing from the spirit and scope of the embodiments of the invention. Furthermore, it will be apparent to those of ordinary skill in the art that many modifications and variations are possible in light of the above teachings.

上述說明書中對方法的任何引用皆應加以必要變更適用於能夠執行該方法的系統,並且應加以必要變更適用於儲存指令的電腦程式產品,該等指令一旦執行就導致該方法的執行。類似地,上述規範中對系統的任何引用應加以必要變更適用於可由系統執行的方法,該系統應加以必要變更適用於儲存可由該系統執行的指令的電腦程式產品;並且說明書中對電腦程式產品的任何引用皆應加以必要變更適用於在執行儲存於電腦程式產品中的指令時可執行的方法,並且應加以必要變更適用於經配置為執行儲存在電腦程式產品中的指令的系統。Any reference in the above specification to a method shall apply mutatis mutandis to a system capable of executing the method, and shall apply mutatis mutandis to a computer program product storing instructions that, when executed, cause the execution of the method. Similarly, any reference in the above specification to a system shall apply mutatis mutandis to a method executable by the system, which shall apply mutatis mutandis to a computer program product storing instructions executable by that system; and references in the specification to a computer program product shall apply mutatis mutandis to a method executable by the system. Any reference to shall apply mutatis mutandis to a method executable in the execution of instructions stored in a computer program product, and shall apply mutatis mutandis to a system configured to execute instructions stored in a computer program product.

在本申請案的所示實施例可以使用本領域技藝人士已知的電子元件和電路來實施的範圍內,為了理解和瞭解本申請案的基本概念並且為了不混淆或分散本案的教示,該等細節不會以比上述認為必要的程度更大的程度來解釋。To the extent that the illustrated embodiments of the present application can be implemented using electronic components and circuits known to those skilled in the art, in order to understand and understand the basic concepts of the present application and in order not to obscure or distract from the teachings of the present application, such Details will not be explained to a greater extent than is deemed necessary above.

100:樣品評估系統 110:真空腔室 120:掃描電子顯微鏡(SEM)柱 122:電子束源 124:聚光透鏡裝置 126:電子束 128:陽極管 130:偏轉透鏡 132:偏轉透鏡 134:聚焦透鏡 136:柱帽 142:透鏡內偵測器 144:頂部偵測器 145:樣品 150:支撐件 160:電壓供應源 170:控制器 180:電腦可讀記憶體 200:SEM柱 210:陽極管 236:柱帽 242:透鏡內偵測器 244:頂部偵測器 245:樣品 250:路徑 252:路徑 254:路徑 300:SEM柱 310:能量濾波器 400:方法 410:步驟 420:步驟 430:步驟 440:步驟 450:步驟 500:SEM柱 510:二次電子 520:反散射電子 610:二次電子 620:反散射電子 700:樣品評估系統 710:外部偵測器 800:晶圓 810:積體電路 820:區域 830:掃描圖案 100:Sample Evaluation System 110: Vacuum chamber 120: Scanning electron microscope (SEM) column 122: Electron beam source 124: Converging lens device 126:Electron beam 128:Anode tube 130:Deflection lens 132:Deflection lens 134:Focusing lens 136: Column cap 142:In-lens detector 144:Top detector 145:Sample 150:Support 160:Voltage supply source 170:Controller 180: Computer readable memory 200:SEM column 210:Anode tube 236: Column cap 242: In-lens detector 244:Top detector 245:Sample 250:Path 252:Path 254:Path 300:SEM column 310:Energy filter 400:Method 410: Steps 420: Steps 430: Steps 440: Steps 450: steps 500:SEM column 510: Secondary electrons 520: Anti-scattered electrons 610: Secondary electrons 620: Anti-scattered electrons 700:Sample Evaluation System 710:External detector 800:wafer 810:Integrated circuits 820:Area 830:Scan pattern

第1圖為根據本案的一些實施例的樣品評估系統的簡化示圖。Figure 1 is a simplified diagram of a sample evaluation system according to some embodiments of the present invention.

第2圖為圖示當由SEM柱產生的電子束撞擊樣品時,由樣品產生的反散射電子的示例性路徑的簡化示圖。Figure 2 is a simplified diagram illustrating an exemplary path of backscattered electrons generated by a sample when an electron beam generated by the SEM column strikes the sample.

第3圖為圖示在先前已知的SEM柱的實例中的能量濾波器的置放的簡化示圖;Figure 3 is a simplified diagram illustrating placement of an energy filter in an example of a previously known SEM column;

第4圖為圖示與根據本案的一些實施例相關聯的步驟的簡化流程圖。Figure 4 is a simplified flowchart illustrating steps associated with some embodiments in accordance with the present invention.

第5A圖為圖示根據一些實施例的當負偏壓施加至柱帽時對二次電子軌跡的影響的實例的簡化圖;Figure 5A is a simplified diagram illustrating an example of the impact on secondary electron trajectories when a negative bias is applied to a pillar cap, in accordance with some embodiments;

第5B圖為圖示根據一些實施例的當負偏壓施加至柱帽時對反散射電子軌跡的影響的實例的簡化圖;Figure 5B is a simplified diagram illustrating an example of the impact on backscattered electron trajectories when a negative bias is applied to a column cap, in accordance with some embodiments;

第6A圖為圖示當無偏壓施加至柱帽時的二次電子的示例性軌跡的簡化圖;Figure 6A is a simplified diagram illustrating exemplary trajectories of secondary electrons when no bias voltage is applied to the pillar cap;

第6B圖為圖示當無偏壓施加至柱帽時的反散射電子的示例性軌跡的簡化圖;Figure 6B is a simplified diagram illustrating exemplary trajectories of backscattered electrons when no bias voltage is applied to the pillar cap;

第7圖為根據本案的一些實施例的包括外部偵測器的樣品評估系統的簡化示圖;及Figure 7 is a simplified diagram of a sample evaluation system including an external detector according to some embodiments of the present case; and

第8圖為根據一些實施例的可自其收集反散射電子的半導體晶圓上的區域的簡化示圖。Figure 8 is a simplified illustration of a region on a semiconductor wafer from which backscattered electrons may be collected in accordance with some embodiments.

國內寄存資訊(請依寄存機構、日期、號碼順序註記) 無 國外寄存資訊(請依寄存國家、機構、日期、號碼順序註記) 無 Domestic storage information (please note in order of storage institution, date and number) without Overseas storage information (please note in order of storage country, institution, date, and number) without

400:方法 400:Method

410:步驟 410: Steps

420:步驟 420: Steps

430:步驟 430: Steps

440:步驟 440: Steps

450:步驟 450: steps

Claims (20)

一種評估一樣品的一區域的方法,該方法包含以下步驟: 將一樣品定位在一真空腔室之內; 用一掃描式電子顯微鏡(SEM)柱產生一電子束,該掃描式電子顯微鏡柱包括在該柱的一端處的一電子槍及在該柱的一相對端處的一柱帽; 將該電子束聚焦在該樣品上並且橫跨該樣品區域掃描該經聚焦的電子束,同時該SEM柱以傾斜模式操作,從而自該區域之內產生二次電子及反散射電子;以及 在該掃描期間,利用一或多個偵測器收集反散射電子,同時施加一負偏壓至該柱帽以改變該二次電子的一軌跡,從而防止該二次電子到達該一或多個偵測器。 A method of evaluating an area of a sample that consists of the following steps: Position a sample within a vacuum chamber; Generating an electron beam using a scanning electron microscope (SEM) column including an electron gun at one end of the column and a column cap at an opposite end of the column; focusing the electron beam on the sample and scanning the focused electron beam across the sample area while the SEM column is operated in a tilt mode, thereby generating secondary electrons and backscattered electrons from within the area; and During the scan, one or more detectors are used to collect backscattered electrons, and a negative bias voltage is applied to the column cap to change a trajectory of the secondary electrons, thereby preventing the secondary electrons from reaching the one or more Detector. 如請求項1所述之評估一樣品區域的方法,進一步包含以下步驟:從該經收集的反散射電子產生該區域的至少一部分的一影像。The method of evaluating a sample area as claimed in claim 1, further comprising the step of generating an image of at least a portion of the area from the collected backscattered electrons. 如請求項1所述之評估一樣品區域的方法,其中施加一負偏壓至該柱帽之步驟包含以下步驟:施加在負50伏與負1000伏之間的一偏壓。The method of evaluating a sample area as claimed in claim 1, wherein the step of applying a negative bias voltage to the pillar cap includes the following steps: applying a bias voltage between negative 50 volts and negative 1000 volts. 如請求項1所述之評估一樣品區域的方法,其中該柱帽具有在其尖端有一開口的一錐形形狀,並且該電子束經引導穿過該開口。The method of evaluating a sample area as claimed in claim 1, wherein the column cap has a tapered shape with an opening at its tip, and the electron beam is directed through the opening. 如請求項1所述之評估一樣品區域的方法,其中該一或多個偵測器包括一透鏡內偵測器及一頂部偵測器。The method of evaluating a sample area as claimed in claim 1, wherein the one or more detectors include an in-lens detector and a top detector. 如請求項1所述之評估一樣品區域的方法,其中收集反散射電子之步驟包括以下步驟:利用一外部偵測器收集該等反散射電子。The method of evaluating a sample area as described in claim 1, wherein the step of collecting backscattered electrons includes the following steps: using an external detector to collect the backscattered electrons. 如請求項1至6中任一項所述之評估一樣品區域的方法,其中施加一負偏壓至該柱帽之步驟包含以下步驟:施加在負100伏與負500伏之間的一偏壓。The method of evaluating a sample area as claimed in any one of claims 1 to 6, wherein the step of applying a negative bias voltage to the column cap includes the following steps: applying a bias voltage between negative 100 volts and negative 500 volts. pressure. 一種用於評估一樣品的一區域的系統,該系統包含: 一真空腔室; 一樣品支撐件,經配置以在一樣品評估過程期間將一樣品保持在該真空腔室內; 一掃描電子顯微鏡(SEM)柱,經配置以將一帶電粒子束朝向該樣品引導至該真空腔室中,該SEM柱包括在該柱的一端處的一電子槍及在該柱的一相對端處的一柱帽; 一偵測器,經配置以偵測反散射電子;以及 一處理器及耦接至該處理器的一記憶體,該記憶體包括複數個電腦可讀指令,當該等指令由該處理器執行時,使得該系統進行以下操作: 將一樣品定位在一真空腔室之內; 用該掃描式電子顯微鏡(SEM)柱產生一電子束; 將該電子束聚焦在該樣品上並且橫跨該樣品區域掃描該經聚焦的電子束,同時該SEM柱以傾斜模式操作,從而自該區域之內產生二次電子及反散射電子;以及 利用一或多個偵測器收集反散射電子,同時該電子束掃描跨過該區域,且同時施加一負偏壓至該柱帽以改變該二次電子的一軌跡,從而防止該二次電子到達該一或多個偵測器。 A system for evaluating an area of a sample that includes: a vacuum chamber; a sample support configured to maintain a sample within the vacuum chamber during a sample evaluation process; A scanning electron microscope (SEM) column configured to direct a charged particle beam into the vacuum chamber toward the sample, the SEM column including an electron gun at one end of the column and an opposite end of the column a pillar cap; a detector configured to detect backscattered electrons; and A processor and a memory coupled to the processor. The memory includes a plurality of computer-readable instructions. When executed by the processor, the instructions cause the system to perform the following operations: Position a sample within a vacuum chamber; Using the scanning electron microscope (SEM) column to generate an electron beam; focusing the electron beam on the sample and scanning the focused electron beam across the sample area while the SEM column is operated in a tilt mode, thereby generating secondary electrons and backscattered electrons from within the area; and One or more detectors are used to collect backscattered electrons while the electron beam scans across the area, and a negative bias voltage is applied to the column cap to change a trajectory of the secondary electrons, thereby preventing the secondary electrons from Reach the one or more detectors. 如請求項8所述之系統,其中該複數個電腦可讀指令進一步使該系統在由該處理器執行時,從該偵測到的反散射電子產生該區域的至少一部分的一影像。The system of claim 8, wherein the plurality of computer-readable instructions further causes the system, when executed by the processor, to generate an image of at least a portion of the area from the detected backscattered electrons. 如請求項8所述之系統,其中施加一負偏壓至該柱帽包含施加在負50伏與負1000伏之間的一偏壓。The system of claim 8, wherein applying a negative bias to the pillar cap includes applying a bias between negative 50 volts and negative 1000 volts. 如請求項8所述之系統,其中施加一負偏壓至該柱帽包含施加在負100伏與負500伏之間的一偏壓。The system of claim 8, wherein applying a negative bias to the pillar cap includes applying a bias between negative 100 volts and negative 500 volts. 如請求項8所述之系統,其中該柱帽具有在其尖端有一開口的一錐形形狀,並且該電子束經引導穿過該開口。The system of claim 8, wherein the column cap has a tapered shape with an opening at its tip, and the electron beam is directed through the opening. 如請求項8所述之系統,其中該一或多個偵測器包括一透鏡內偵測器及一頂部偵測器。The system of claim 8, wherein the one or more detectors include an in-lens detector and a top detector. 如請求項8至13中任一項所述之系統,其中該系統包含一外部偵測器。The system of any one of claims 8 to 13, wherein the system includes an external detector. 一種非暫態電腦可讀記憶體,其儲存用於藉由以下方式評估一樣品區域的複數個電腦可讀指令: 將一樣品定位在一真空腔室之內; 用一掃描式電子顯微鏡(SEM)柱產生一電子束,該掃描式電子顯微鏡柱包括在該柱的一端處的一電子槍及在該柱的一相對端處的一柱帽; 將該電子束聚焦在該樣品上並且橫跨該樣品區域掃描該經聚焦的電子束,同時該SEM柱以傾斜模式操作,從而自該區域之內產生二次電子及反散射電子;以及 在該掃描期間,利用一或多個偵測器收集反散射電子,同時施加一負偏壓至該柱帽以改變該二次電子的一軌跡,從而防止該二次電子到達該一或多個偵測器。 A non-transitory computer-readable memory storing a plurality of computer-readable instructions for evaluating a region of a sample by: Position a sample within a vacuum chamber; Generating an electron beam using a scanning electron microscope (SEM) column including an electron gun at one end of the column and a column cap at an opposite end of the column; focusing the electron beam on the sample and scanning the focused electron beam across the sample area while the SEM column is operated in a tilt mode, thereby generating secondary electrons and backscattered electrons from within the area; and During the scan, one or more detectors are used to collect backscattered electrons, and a negative bias voltage is applied to the column cap to change a trajectory of the secondary electrons, thereby preventing the secondary electrons from reaching the one or more Detector. 如請求項15所述之非暫態電腦可讀記憶體,其中用於評估一樣品區域的該複數個電腦可讀指令進一步包括從該經收集的反散射電子產生該區域的至少一部分的一影像的指令。The non-transitory computer-readable memory of claim 15, wherein the plurality of computer-readable instructions for evaluating a sample area further includes generating an image of at least a portion of the area from the collected backscattered electrons. instructions. 如請求項15所述之非暫態電腦可讀記憶體,其中施加一負偏壓至該柱帽包含施加在負50伏與負1000伏之間的一偏壓。The non-transitory computer readable memory of claim 15, wherein applying a negative bias voltage to the pillar cap includes applying a bias voltage between negative 50 volts and negative 1000 volts. 如請求項15所述之非暫態電腦可讀記憶體,其中施加一負偏壓至該柱帽包含施加在負100伏與負500伏之間的一偏壓。The non-transitory computer readable memory of claim 15, wherein applying a negative bias voltage to the pillar cap includes applying a bias voltage between negative 100 volts and negative 500 volts. 如請求項15所述之非暫態電腦可讀記憶體,其中該柱帽具有在其尖端有一開口的一錐形形狀,並且該電子束經引導穿過該開口。The non-transitory computer readable memory of claim 15, wherein the pillar cap has a tapered shape with an opening at its tip, and the electron beam is guided through the opening. 如請求項15至19中任一項所述之非暫態電腦可讀記憶體,其中該一或多個偵測器包括一透鏡內偵測器及一頂部偵測器。The non-transitory computer-readable memory of any one of claims 15 to 19, wherein the one or more detectors include an in-lens detector and a top detector.
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