TW202235833A - Method for finding the properest kilning temperature of ceramics by laser sintering - Google Patents

Method for finding the properest kilning temperature of ceramics by laser sintering Download PDF

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TW202235833A
TW202235833A TW110108746A TW110108746A TW202235833A TW 202235833 A TW202235833 A TW 202235833A TW 110108746 A TW110108746 A TW 110108746A TW 110108746 A TW110108746 A TW 110108746A TW 202235833 A TW202235833 A TW 202235833A
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李子介
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Abstract

The present invention related to a method for finding the properest kilning temperature of ceramics by laser sintering. Its procedure including allocating the ingredients formula of the ceramics first. Next, using laser to illuminate the ingredients with different light point moving speed to find the highest speed which can sinter the ingredients. Afterwards, calculating a energy value by the acquired speed. Then matching the energy value with a relation curve of the light point moving speed and the energy value to find the necessary real kilning temperature of the ingredients.

Description

運用雷射燒成量測陶瓷最適窯燒溫度之方法Method of Measuring the Optimum Kiln Firing Temperature of Ceramics Using Laser Firing

本發明係有關一種運用雷射燒成量測陶瓷最適窯燒溫度之方法,係一種工業製造技術者。The invention relates to a method for measuring the optimum kiln firing temperature of ceramics by using laser firing, and is an industrial manufacturing technique.

在製作陶瓷作品時,不同配方的陶瓷原料可能需要實際經過多次窯燒後,才能確定適合的窯燒溫度,而如果窯燒溫度不適合,即可能出現釉藥融流或未燒結等情況,而需要再調整下次的溫度;When making ceramic works, the ceramic raw materials of different formulas may need to be kilned several times before the suitable kiln temperature can be determined. If the kiln temperature is not suitable, the glaze may melt or not be sintered, and Need to adjust the temperature next time;

但窯燒時除了需耗費許多陶瓷原料與加熱燃料外,每次窯燒也都需時至少十幾小時以上,若失敗時也得清理善後,因此以實際窯燒來試誤相當不經濟且浪費。However, in addition to consuming a lot of ceramic raw materials and heating fuel during kiln firing, each kiln firing also takes at least ten hours or more. If it fails, it must be cleaned up, so trial and error with actual kiln firing is quite uneconomical and wasteful. .

有鑑於上述缺失弊端,本發明人認為具有改正之必要,遂以從事相關技術以及產品設計製造之多年經驗,秉持優良設計理念,針對以上不良處加以研究創作,在經過不斷的努力後,終乃推出本發明運用雷射燒成量測陶瓷最適窯燒溫度之方法,期以更正產品結構以提升產品優良之功效。In view of the above shortcomings, the inventor believes that it is necessary to correct it. Based on his many years of experience in related technologies and product design and manufacturing, and adhering to the excellent design concept, he researched and created the above shortcomings. After continuous efforts, he finally achieved Introduced the method of measuring the optimum kiln firing temperature of ceramics by using laser firing in the present invention, hoping to correct the product structure and improve the excellent efficacy of the product.

本發明運用雷射燒成量測陶瓷最適窯燒溫度之方法之主要目的,係提供一種能以雷射燒結來推算出陶瓷所需要的實際窯燒溫度的方法者。The main purpose of the present invention for measuring the optimum kiln firing temperature of ceramics by laser sintering is to provide a method that can calculate the actual kiln firing temperature required by ceramics by laser sintering.

爲達到前揭之目的,本發明運用雷射燒成量測陶瓷最適窯燒溫度之方法包括有以下步驟:In order to achieve the purpose disclosed above, the method for measuring the optimum kiln firing temperature of ceramics by using laser firing in the present invention includes the following steps:

原料調配,即調配出欲製作成陶瓷成品的成份原料;Raw material blending, that is, the blending of ingredients and raw materials to be made into ceramic products;

雷射燒結,以一雷射裝置所產生的雷射光照射調配好的原料,並依序以不同的光點移動速度來照射原料,照射後觀察原料的狀態以找出能夠讓原料燒結的最快光點移動速度;Laser sintering, the prepared raw materials are irradiated with laser light generated by a laser device, and the raw materials are irradiated with different light spot moving speeds in sequence, and the state of the raw materials is observed after irradiation to find out the fastest way to sinter the raw materials. Speed of spot movement;

比對程序,以所得的最快光點移動速度計算出一能量值後,再將該能量值與一光點移動速度-能量值曲線進行比對,即可得出該原料實際進行窯燒時所需的溫度。The comparison program calculates an energy value based on the obtained fastest light spot moving speed, and then compares the energy value with a light spot moving speed-energy value curve to obtain the actual kiln burning time of the raw material. desired temperature.

而與以往需耗費大量成本來進行實際窯燒試誤後,才能找出不同配方原料的合適窯燒溫度相比,本發明則利用雷射燒結再配合比對法,即可得出原料所需的可能實際窯燒溫度,進而達到節省成本的效果,其對於陶瓷製作的未來發展有極大的助益潛力,而可見本發明之進步性。Compared with the past, which required a large amount of cost to carry out actual kiln firing trial and error, to find out the suitable kiln temperature of raw materials with different formulas, the present invention uses laser sintering and matching comparison method to obtain the required kiln temperature for raw materials. The possible actual kiln firing temperature, and then achieve the effect of cost saving, which has great potential to help the future development of ceramic production, and it can be seen that the progress of the present invention.

為完成本發明之方法的先行實驗中,先以一雷射裝置來對多種已知所需窯燒溫度的陶瓷原料進行燒結實驗,所用的雷射光功率為20W,光點半徑為0.2mm,並從1mm/sec的光點移動速度開始,以每次增加1mm/sec速度的來逐次照射原料,後觀察原料以找出能夠讓原料產生燒結現象的最快光點移動速度,而此些實驗原料與其所需的窯燒溫度分別為瓷土1240~1280℃、陶土1210~1260℃、透明釉1100~1245℃、窯燒測溫錐600~800℃,[請參閱第一圖與第二圖]而實驗結果之一請參考第一與二圖,其為透明釉的雷射燒結實驗結果,可看出能夠讓透明釉表面產生波浪紋燒結的最快光點移動速度為14mm/sec,超過後即會因光點移動過快,而無法提供照射處足夠的能量來造成燒結;In the preceding experiment for completing the method of the present invention, a laser device is used to carry out sintering experiments on a variety of ceramic raw materials with known required kiln firing temperatures. The laser light power used is 20W, and the light spot radius is 0.2mm. Starting from the light spot moving speed of 1mm/sec, the raw material is irradiated successively by increasing the speed of 1mm/sec each time, and then observing the raw material to find out the fastest light spot moving speed that can cause the sintering phenomenon of the raw material, and these experimental raw materials The required kiln firing temperatures are respectively 1240-1280°C for china clay, 1210-1260°C for pottery clay, 1100-1245°C for transparent glaze, and 600-800°C for kiln firing temperature cones, [please refer to the first and second pictures] For one of the experimental results, please refer to the first and second pictures, which are the laser sintering test results of the transparent glaze. It can be seen that the fastest light spot moving speed that can produce wave patterns on the transparent glaze surface is 14mm/sec. Because the light spot moves too fast, it cannot provide enough energy to irradiate to cause sintering;

得知最快光點移動速度後再計算出其能量值,能量值的計算公式如下:

Figure 02_image001
After knowing the moving speed of the fastest light spot, calculate its energy value. The formula for calculating the energy value is as follows:
Figure 02_image001

其中W為雷射功率(W),r為光點半徑(mm),V為光點移動速度(mm/sec),而對上述原料完成實驗並計算整理後,[請一併參閱第三圖]可以光點移動速度為橫軸並以能量值為縱軸繪製出一光點移動速度-能量值曲線而如第三圖所示,並瓷土等各原料的座標點之縱軸值也同時代表自身所需的最低窯燒溫度,因此要對一新配方的原料進行窯燒前,可先對該原料進行雷射燒結以找出能產生燒結現象的最快光點移動速度,接著再以該最快光點移動速度計算出能量值,後再以該能量值找出該原料於上述曲線的座標值後,即可得出該原料所需的實際窯燒溫度。Where W is the laser power (W), r is the spot radius (mm), V is the moving speed of the spot (mm/sec), and after completing the experiment and calculation of the above raw materials, [please also refer to the third figure ] A light spot moving speed-energy value curve can be drawn with the moving speed of the light spot on the horizontal axis and the energy value on the vertical axis, as shown in the third figure, and the vertical axis values of the coordinate points of various raw materials such as porcelain clay also represent The minimum kiln firing temperature required by itself, so before kilning a raw material with a new formula, laser sintering can be performed on the raw material to find out the fastest light spot moving speed that can produce sintering phenomenon, and then use this The energy value is calculated by the fastest moving speed of the light spot, and then the coordinate value of the raw material on the above curve is found by the energy value, and the actual kiln firing temperature required by the raw material can be obtained.

[請參閱第四圖]因此本發明運用雷射燒成量測陶瓷最適窯燒溫度之方法,其步驟包括:[Please refer to the fourth picture] Therefore, the present invention uses laser firing to measure the optimum firing temperature of ceramics. The steps include:

原料調配(1),即調配出欲製作成陶瓷成品的成份原料;Raw material blending (1), that is, the blending of ingredients and raw materials to be made into finished ceramic products;

雷射燒結(2),以一雷射裝置所產生的雷射光照射調配好的原料,並依序以不同的光點移動速度來照射原料,照射後觀察原料的狀態以找出能夠讓原料燒結的最快光點移動速度;Laser sintering (2): The prepared raw materials are irradiated with laser light generated by a laser device, and the raw materials are irradiated with different moving speeds of light spots in sequence, and the state of the raw materials is observed after irradiation to find out the materials that can be sintered. The fastest light spot moving speed;

比對程序(3),以所得的最快光點移動速度計算出能量值後,再將該能量值與一光點移動速度-能量值曲線進行比對,即可得出該原料實際進行窯燒時所需的溫度。Comparing procedure (3), after calculating the energy value based on the obtained fastest light spot moving speed, and then comparing the energy value with a light spot moving speed-energy value curve, it can be obtained that the raw material is actually used in the kiln. The temperature required for burning.

原料調配(1)步驟為一般陶瓷工作者欲製作陶瓷作品時的例行工作,故不多加贅述;Raw material preparation (1) is the routine work of ordinary ceramic workers when they want to make ceramic works, so I won’t repeat them here;

雷射燒結(2)步驟中,此處的雷射裝置所產生的雷射光功率為20W,光點直徑0.2mm,並從1mm/sec的光點移動速度開始,以每次增加1mm/sec速度的來逐次照射原料以找出可燒結原料的最快光點移動速度。In the laser sintering (2) step, the laser light power generated by the laser device here is 20W, the light spot diameter is 0.2mm, and the moving speed of the light spot starts from 1mm/sec, and the speed is increased by 1mm/sec each time. To irradiate the raw material successively to find out the fastest light spot moving speed of the sinterable raw material.

本發明透過先以雷射進行燒結,而找出可讓原料燒結的最快光點移動速度,再計算出能量值並比對光點移動速度-能量值曲線後,即可得出該原料所需的實際窯燒溫度,而無須再像以往需要進行多次窯燒試誤才能找出合適的窯燒溫度,藉此可節省大量的人力、物料與時間成本。The present invention first sinters with laser to find out the fastest moving speed of the light spot that can sinter the raw material, and then calculates the energy value and compares the light spot moving speed-energy value curve, then the raw material can be obtained. The actual kiln firing temperature required, instead of the need to go through multiple trial and error kiln firing to find out the appropriate kiln firing temperature, which can save a lot of manpower, material and time costs.

唯以上所述者,僅為本發明之一較佳實施例而已,當不能以之限定本發明之範圍。即大凡依申請專利範圍所作之均等變化與修飾,皆應仍屬本創作專利涵蓋之範圍內。What is described above is only a preferred embodiment of the present invention, and should not be used to limit the scope of the present invention. That is to say, all equivalent changes and modifications made according to the scope of the patent application should still fall within the scope covered by this creation patent.

綜上所述,當知本發明具有新穎性、進步性,且本發明未見之於任何刊物,當符合專利法第22條之規定。To sum up, if the invention is novel and progressive, and the invention has not been published in any publication, it shall comply with the provisions of Article 22 of the Patent Law.

1:原料調配 2:雷射燒結 3:比對程序 1: Raw material deployment 2: Laser sintering 3: Comparison program

第一圖係雷射燒結實驗中的透明釉之實驗結果圖。 第二圖係第一圖中光點移動速度為14mm/sec之組別的放大圖。 第三圖係光點移動速度-能量值曲線之示意圖。 第四圖係本發明運用雷射燒成量測陶瓷最適窯燒溫度之方法的步驟流程圖。 The first picture is the experimental result picture of the transparent glaze in the laser sintering experiment. The second picture is an enlarged picture of the group whose moving speed of the light spot is 14mm/sec in the first picture. The third figure is a schematic diagram of the light spot moving speed-energy value curve. Figure 4 is a flow chart of the steps of the method of measuring the optimum firing temperature of ceramics by using laser firing in the present invention.

none

1:原料調配 1: Raw material deployment

2:雷射燒結 2:Laser sintering

3:比對程序 3: Comparison program

Claims (2)

一種運用雷射燒成量測陶瓷最適窯燒溫度之方法,其步驟包括: 原料調配,調配出欲製作成陶瓷成品的成份原料; 雷射燒結,以一雷射裝置所產生的雷射光照射調配好的原料,並依序以不同的光點移動速度來照射原料,照射後觀察原料的狀態以找出能夠讓原料燒結的最快光點移動速度; 比對程序,以所得的最快光點移動速度計算出一能量值後,再將該能量值與一光點移動速度-能量值曲線進行比對,即可得出該原料實際進行窯燒時所需的溫度者。 A method for measuring the optimum kiln firing temperature of ceramics by using laser firing, the steps of which include: Allocation of raw materials, the allocation of raw materials to be made into ceramic products; Laser sintering, the prepared raw materials are irradiated with laser light generated by a laser device, and the raw materials are irradiated with different light spot moving speeds in sequence, and the state of the raw materials is observed after irradiation to find out the fastest way to sinter the raw materials. Speed of spot movement; The comparison program calculates an energy value based on the obtained fastest light spot moving speed, and then compares the energy value with a light spot moving speed-energy value curve to obtain the actual kiln burning time of the raw material. the desired temperature. 如請求項1所述之運用雷射燒成量測陶瓷最適窯燒溫度之方法,其中,在該雷射燒結步驟中,雷射光功率為20W,光點直徑0.2mm,並從1mm/sec的光點移動速度開始,以每次增加1mm/sec速度的來逐次照射原料以找出可燒結原料的最快光點移動速度者。The method of using laser sintering to measure the optimum kiln firing temperature of ceramics as described in claim 1, wherein, in the laser sintering step, the laser light power is 20W, the light spot diameter is 0.2mm, and the temperature is increased from 1mm/sec Starting from the moving speed of the light spot, the raw material is irradiated successively by increasing the speed by 1mm/sec each time to find out the fastest moving speed of the light spot that can sinter the raw material.
TW110108746A 2021-03-11 2021-03-11 Method for finding the properest kilning temperature of ceramics by laser sintering TWI750055B (en)

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