TW202040068A - Drying system and control method thereof - Google Patents
Drying system and control method thereof Download PDFInfo
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- TW202040068A TW202040068A TW108113172A TW108113172A TW202040068A TW 202040068 A TW202040068 A TW 202040068A TW 108113172 A TW108113172 A TW 108113172A TW 108113172 A TW108113172 A TW 108113172A TW 202040068 A TW202040068 A TW 202040068A
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
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Abstract
Description
本發明提供一種乾燥系統,以及適用於此乾燥系統的控制方法。The invention provides a drying system and a control method suitable for the drying system.
乾燥是一種工業上常見的單元操作流程。一般而言,操作員會將待乾燥物置於乾燥室,並且藉由加熱將固體中的水分汽化並自待乾燥物的內部或表面排出。然而,對於一些加熱後容易分解或氧化的材料,需要以減壓或抽氣的方式進行低溫乾燥,在這種環境中,由於乾燥室內的壓力較一般大氣為低,一般溼度計不易判斷乾燥物的濕度狀態,從而無從得知乾燥流程是否完成。Drying is a common unit operation process in industry. Generally speaking, the operator places the object to be dried in a drying chamber, and vaporizes the moisture in the solid by heating and discharges it from the inside or surface of the object to be dried. However, some materials that are easily decomposed or oxidized after heating need to be dried at low temperature by means of reduced pressure or air extraction. In this environment, because the pressure in the drying chamber is lower than the general atmosphere, it is difficult for general hygrometers to determine the dry matter. Therefore, it is impossible to know whether the drying process is completed.
本發明提供一種乾燥系統,以及適用於此乾燥系統的控制方法,可判斷待乾燥物的濕度狀態,並且控制乾燥流程持續進行或中止。The invention provides a drying system and a control method suitable for the drying system, which can judge the humidity state of the object to be dried and control the drying process to continue or stop.
本發明的乾燥系統,包括一控制模組、一抽氣模組以及一感測模組。抽氣模組電性連接於控制模組且連接於一腔體。感測模組電性連接於控制模組且連接於腔體。The drying system of the present invention includes a control module, an air extraction module and a sensing module. The air extraction module is electrically connected to the control module and connected to a cavity. The sensing module is electrically connected to the control module and connected to the cavity.
本發明的控制方法,適用於上述的乾燥系統,控制方法包括控制模組驅動抽氣模組將腔體內部的氣體抽出、感測模組將腔體內部的殘餘氣體離子化以取得一氣體資料,並將氣體資料傳遞至控制模組,以及控制模組判斷氣體資料是否符合一預定標準。當控制模組判斷氣體資料不符合預定標準時,控制模組控制抽氣模組繼續將腔體內部的殘餘氣體抽出;當控制模組判斷氣體資料符合預定標準時,控制模組終止抽氣模組運作。The control method of the present invention is suitable for the above-mentioned drying system. The control method includes the control module driving the air extraction module to extract the gas inside the cavity, and the sensing module ionizes the residual gas inside the cavity to obtain a gas data , And transfer the gas data to the control module, and the control module determines whether the gas data meets a predetermined standard. When the control module determines that the gas data does not meet the predetermined standard, the control module controls the air extraction module to continue to extract the residual gas inside the cavity; when the control module determines that the gas data meets the predetermined standard, the control module terminates the operation of the air extraction module .
在本發明的一實施例中,抽氣模組包括一氣體幫浦以及一抽氣管線,且抽氣管線連接於氣體幫浦與腔體。In an embodiment of the present invention, the pumping module includes a gas pump and a pumping pipeline, and the pumping pipeline is connected to the gas pump and the cavity.
在本發明的一實施例中,感測模組包括一微量氣體分析儀以及一壓力感測器。In an embodiment of the present invention, the sensing module includes a trace gas analyzer and a pressure sensor.
在本發明的一實施例中,控制方法更包括將氣體幫浦透過抽氣管線連接於腔體。In an embodiment of the present invention, the control method further includes connecting the gas pump to the cavity through an exhaust line.
在本發明的一實施例中,控制方法更包括微量氣體分析儀將腔體內部的殘餘氣體離子化並分析殘餘氣體的一氣體離子荷質比,以取得殘餘氣體的各組成氣體的分壓,壓力感測器感測殘餘氣體的一氣體壓力,以及控制模組根據氣體壓力及各組成氣體的分壓,計算組成各組成氣體的元素的一重量百分比,其中氣體資料包括重量百分比。In an embodiment of the present invention, the control method further includes ionizing the residual gas inside the cavity by a trace gas analyzer and analyzing a gas ion charge-to-mass ratio of the residual gas to obtain the partial pressure of each component gas of the residual gas. The pressure sensor senses a gas pressure of the residual gas, and the control module calculates a weight percentage of the elements constituting each component gas according to the gas pressure and the partial pressure of each component gas, wherein the gas data includes weight percentage.
在本發明的一實施例中,控制方法更包括控制模組根據氣體壓力及各組成氣體的分壓,計算各組成氣體的一碳元素的重量百分比、一氫元素的重量百分比、一氧元素的重量百分比以及一水分子的重量百分比,其中預定標準包括碳元素的重量百分比、氫元素的重量百分比、氧元素的重量百分比以及水分子的重量百分比的至少其中之一。In an embodiment of the present invention, the control method further includes the control module calculating the weight percentage of one carbon element, the weight percentage of one hydrogen element, and the weight percentage of one oxygen element in each component gas according to the gas pressure and the partial pressure of each component gas. The weight percentage and the weight percentage of a water molecule, wherein the predetermined standard includes at least one of the weight percentage of carbon element, the weight percentage of hydrogen element, the weight percentage of oxygen element, and the weight percentage of water molecule.
在本發明的一實施例中,碳元素的重量百分比為0.05%、氫元素的重量百分比為0.05%、氧元素的重量百分比為0.005%以及水分子的重量百分比為0.0001%。In an embodiment of the present invention, the weight percentage of carbon element is 0.05%, the weight percentage of hydrogen element is 0.05%, the weight percentage of oxygen element is 0.005%, and the weight percentage of water molecule is 0.0001%.
為讓本發明的上述特徵和優點能更明顯易懂,下文特舉實施例,並配合所附圖式作詳細說明如下。In order to make the above-mentioned features and advantages of the present invention more comprehensible, the following specific embodiments are described in detail in conjunction with the accompanying drawings.
第1圖是本發明的一實施例的乾燥系統的方塊圖,第2圖是本發明的一實施例的控制方法的步驟流程圖,請參考第1圖以及第2圖。本實施例的控制方法適用於一乾燥系統10,乾燥系統10包括一抽氣模組100、一控制模組200以及一感測模組300,其中抽氣模組100、控制模組200以及感測模組300彼此電性連接,且抽氣模組100連接於一腔體400。Fig. 1 is a block diagram of a drying system according to an embodiment of the present invention, and Fig. 2 is a flow chart of steps of a control method according to an embodiment of the present invention. Please refer to Figs. 1 and 2. The control method of this embodiment is applicable to a
具體而言,抽氣模組100包括一氣體幫浦120以及一抽氣管線140,其中抽氣管線140用以連接於氣體幫浦120與腔體400。當使用者想要乾燥一待乾燥物,或是想要降低腔體400內的濕度時,可以將待乾燥物置入腔體400內,並且將氣體幫浦120透過抽氣管線140連接於腔體400,再啟動乾燥系統10,此時控制模組200會驅動抽氣模組100將腔體400內部的氣體抽出(步驟S01)。在抽氣的過程當中,腔體400內部的氣體分子會逐漸變少,待抽氣經過一定時間後,感測模組300會將腔體400內部的氣體離子化以取得一氣體資料,並將氣體資料傳遞至控制模組200(步驟S02)。Specifically, the
詳細而言,本實施例的感測模組300包括一微量氣體分析儀(Residual Gas Analyzer, RGA) 320,其中微量氣體分析儀320能將腔體400內部的殘餘氣體離子化,並且分析殘餘氣體的氣體離子荷質比。由於殘餘氣體中不同組成氣體的荷質比彼此相異,因此可進一步地取得殘餘氣體的各組成氣體的分壓。當腔體400內部的壓力降低的同時,壓力露點也會隨之降低,因此待乾燥物或是腔體400內部的細小水滴會更容易氣化成為水氣,並且隨著一般空氣離子化進而被微量氣體分析儀320分析偵測。此時,控制模組200根據氣體壓力以及各組成氣體的分壓,計算各組成氣體的碳元素的重量百分比、氫元素的重量百分比、氧元素的重量百分比以及水分子的重量百分比,並判斷此氣體資料是否符合一預定標準(步驟S03)。其中,預定標準包括碳元素的重量百分比、氫元素的重量百分比、氧元素的重量百分比以及水分子的重量百分比的至少其中之一,在本實施例中設定各個元素或分子成份的重量百分比閾值:碳元素0.05%、氫元素0.05%、氧元素0.05%以及水分子0.0001%,上述比例雖然是經過多次實驗後得到的最佳化結果,但本發明並不以此為限,依據所需要的目標乾燥程度,上述的重量百分比閾值也可調整為其它的數值。In detail, the
當控制模組200判斷氣體資料不符合預定標準,也就是各個元素或分子的成份未低於各別設定的閾值時,控制模組200將控制抽氣模組100繼續將腔體400內部的殘餘氣體抽出,使腔體400內部的細小水滴繼續揮發成水氣,進而達到乾燥的效果;當控制模組200判斷氣體資料符合預定標準,也就是各個元素或分子的成份低於各別設定的閾值時,代表此時腔體400內部的乾燥度已達到預定的目標,此時控制模組200將終止抽氣模組100運作(步驟S04),並完成整個乾燥流程。When the
綜上所述,本發明的乾燥系統以及控制方法,藉由將腔體內部的氣體抽出、離子化腔體內部的殘餘氣體進而取得氣體資料,並判斷氣體資料是否符合預定標準,可在低溫乾燥的環境下取代溼度計確實掌握待乾燥物或腔體內部的乾燥度,大幅增加了乾燥流程的應用範圍以及準確度。 以上所述僅為本發明之較佳實施例,凡依本發明申請專利範圍所做之均等變化與修飾,皆應屬本發明之涵蓋範圍。In summary, the drying system and control method of the present invention can obtain gas data by extracting the gas inside the cavity and ionizing the residual gas inside the cavity, and determine whether the gas data meets the predetermined standard, and can be dried at low temperature. In an environment where the hygrometer is replaced, the dryness of the object to be dried or the cavity is accurately grasped, which greatly increases the application range and accuracy of the drying process. The foregoing descriptions are only preferred embodiments of the present invention, and all equivalent changes and modifications made in accordance with the scope of the patent application of the present invention shall fall within the scope of the present invention.
10:乾燥系統 100:抽氣模組 120:氣體幫浦 140:抽氣管線 200:控制模組 300:感測模組 320:微量氣體分析儀 340:壓力感測器 400:腔體 S01、S02、S03、S04:步驟10: Drying system 100: Air extraction module 120: Gas pump 140: suction line 200: control module 300: Sensing module 320: Trace gas analyzer 340: Pressure sensor 400: Cavity S01, S02, S03, S04: steps
第1圖是本發明的一實施例的乾燥系統的方塊圖。 第2圖是本發明的一實施例的控制方法的步驟流程圖。Figure 1 is a block diagram of a drying system according to an embodiment of the present invention. Figure 2 is a flow chart of the control method of an embodiment of the present invention.
10:乾燥系統 10: Drying system
100:抽氣模組 100: Air extraction module
120:氣體幫浦 120: Gas pump
140:抽氣管線 140: suction line
200:控制模組 200: control module
300:感測模組 300: Sensing module
320:微量氣體分析儀 320: Trace gas analyzer
340:壓力感測器 340: Pressure sensor
400:腔體 400: Cavity
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TW108113172A TWI687630B (en) | 2019-04-16 | 2019-04-16 | Drying system and control method thereof |
CN201910373109.2A CN111829333A (en) | 2019-04-16 | 2019-05-06 | Drying system and control method |
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JP3062990B2 (en) * | 1994-07-12 | 2000-07-12 | キヤノン株式会社 | Electron emitting device, method of manufacturing electron source and image forming apparatus using the same, and device for activating electron emitting device |
JP3077602B2 (en) * | 1996-03-06 | 2000-08-14 | 三浦工業株式会社 | Vacuum cooling device |
JP5461223B2 (en) * | 2010-02-22 | 2014-04-02 | 株式会社松井製作所 | Vacuum drying equipment for granular materials |
CN102012148B (en) * | 2010-11-19 | 2013-03-20 | 何天青 | Vacuum drying control method |
TWI654695B (en) * | 2012-12-06 | 2019-03-21 | 英福康公司 | Vacuum tool and method for measuring an atomsphere in a guest vacuum chamber of the vacuum tool |
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WO2018194925A1 (en) * | 2017-04-21 | 2018-10-25 | Mks Instruments, Inc. | End point detection for lyophilization |
CN107014156B (en) * | 2017-04-26 | 2019-03-29 | 常州广建仪器科技有限公司 | Dried object moisture measurement method, Minton dryer and its control method |
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