TW201430074A - Heat dissipation nano-coating material and preparation method thereof - Google Patents
Heat dissipation nano-coating material and preparation method thereof Download PDFInfo
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本發明係有關一種奈米散熱塗料及製備方法,尤指一種以氟碳樹脂為基料而混合具有孔隙結構之填料,而利用填料之孔隙結構提升散熱性之設計者。The invention relates to a nano heat-dissipating paint and a preparation method thereof, in particular to a designer who mixes a filler having a pore structure based on a fluorocarbon resin and uses a pore structure of the filler to improve heat dissipation.
按,諸如金屬散熱片與熱管等散熱元件,散熱效果固然好,但是價格昂貴且不適用於輕巧化之產品設計,因而有散熱塗料之發展與應用。然而,現有之散熱塗料於散熱面固化形成散熱層後,因使用之基料之耐候性、耐熱性、耐低溫性及耐化學藥品性等抗污染性不佳,致使固化後所形之散熱層之散熱性易因汙染物附著而降低;再者,現有之散熱塗料所使用之填料因不具孔隙結構,故所能展現之散熱性並不高。According to heat dissipation components such as metal heat sinks and heat pipes, the heat dissipation effect is good, but it is expensive and not suitable for light-weight product design, so there is the development and application of heat-dissipating coatings. However, the existing heat-dissipating coating is cured on the heat-dissipating surface to form a heat-dissipating layer, and the heat-resistant layer formed after curing due to poor weather resistance, heat resistance, low-temperature resistance, and chemical resistance of the base material used. The heat dissipation is easily reduced by the adhesion of contaminants; in addition, the filler used in the existing heat-dissipating coatings does not have a pore structure, so the heat dissipation which can be exhibited is not high.
本發明之主要目的,係欲提供一種奈米散熱塗料及製備方法,而具有抗污染性佳及高散熱性之功效。The main object of the present invention is to provide a nano heat-dissipating paint and a preparation method thereof, which have the effects of good anti-pollution and high heat dissipation.
本發明之另一目的,則具有利於填料均勻分散之功效。Another object of the present invention is to facilitate the uniform dispersion of the filler.
為達上述功效,本發明之奈米散熱塗料結構特徵,係以氟碳樹脂為基料而混合具有孔隙結構之填料,該基料與該填料之重量比為3至5倍者。In order to achieve the above effects, the nano heat-dissipating coating structure of the present invention is characterized in that a filler having a pore structure is mixed with a fluorocarbon resin as a base, and the weight ratio of the base material to the filler is 3 to 5 times.
此外,該填料選自奈米竹炭、奈米碳管、奈米氧化鋅、奈米氧化鍺或前述填料之組合;該基料與該填料之混合溶劑選自天拿水、醋酸乙酯、無水乙醇、蒸餾水或前述混合溶劑之組合;該基料與混合溶劑之重量比為0.9至1.4倍,該填料與混合溶劑之重量比為0.3至0.6倍。In addition, the filler is selected from the group consisting of nano bamboo charcoal, carbon nanotubes, nano zinc oxide, nano cerium oxide or a combination of the foregoing fillers; the mixed solvent of the base material and the filler is selected from the group consisting of natural water, ethyl acetate, and anhydrous Ethanol, distilled water or a combination of the foregoing mixed solvents; the weight ratio of the base material to the mixed solvent is from 0.9 to 1.4 times, and the weight ratio of the filler to the mixed solvent is from 0.3 to 0.6 times.
本發明之奈米散熱塗料製備方法,係包括下列步驟:a.將氟碳樹脂做為基料溶於混合溶劑中,而得到基料混合液;b.將重量比為該基料0.2至0.33倍之具有孔隙結構之填料溶於混合溶劑中,而得到填料混合液;c.將經過步驟a得到之基料混合液與經過步驟b得到之填料混合液進行過濾;以及d.將經過步驟c過濾後之基料混合液與填料混合液攪拌混合均勻者。The preparation method of the nano heat dissipating paint of the present invention comprises the following steps: a. dissolving the fluorocarbon resin as a base material in a mixed solvent to obtain a base material mixture; b. adding a weight ratio of the base material to 0.2 to 0.33 a filler having a pore structure is dissolved in a mixed solvent to obtain a filler mixture; c. filtering the base mixture obtained in the step a and the filler mixture obtained in the step b; and d. The filtered mixture of the base material and the filler mixture are stirred and mixed uniformly.
然而,步驟a之基料與混合溶劑之重量比為0.9至1.4倍,步驟b之填料與混合溶劑之重量比為0.3至0.6倍,步驟c係利用350目篩網過濾,步驟d係利用剪切乳化機高速攪拌混合均勻。However, the weight ratio of the binder of the step a to the mixed solvent is 0.9 to 1.4 times, the weight ratio of the filler of the step b to the mixed solvent is 0.3 to 0.6 times, the step c is filtered by a 350 mesh sieve, and the step d is by using a shear. The emulsifier is stirred and mixed at high speed.
【00010】 首先,請參閱「圖1」所示,本發明之奈米散熱塗料製備方法,係包括下列步驟:a.將氟碳樹脂做為基料溶於混合溶劑中,而得到基料混合液,且令基料與混合溶劑之重量比為0.9至1.4倍;b.將重量比為該基料0.2至0.33倍之具有孔隙結構之填料溶於混合溶劑中,而得到填料混合液,且令填料與混合溶劑之重量比為0.3至0.6倍;c.將經過步驟a得到之基料混合液與經過步驟b得到之填料混合液利用350目篩網進行過濾;以及d.將經過步驟c過濾後之基料混合液與填料混合液利用剪切乳化機高速攪拌混合均勻者。【00011】 再者,本發明之奈米散熱塗料第一實施例,係將120g氟碳樹脂溶於120g醋酸乙脂中得到基料混合液,另將30g奈米竹炭溶於80g無水乙醇中得到填料混合液,而用350目篩網進行過濾該基料混合液與該填料混合液,然後用剪切乳化機高速攪拌該基料混合液與該填料混合液10分鐘,而混合均勻為奈米散熱塗料(參閱「圖2」所示)。【00012】 另者,本發明之奈米散熱塗料第二實施例,係將120g氟碳樹脂溶於100g天拿水中得到基料混合液,另將30g奈米竹炭溶於60g醋酸乙脂中得到填料混合液,而用350目篩網進行過濾該基料混合液與該填料混合液,然後用剪切乳化機高速攪拌該基料混合液與該填料混合液10分鐘,而混合均勻為奈米散熱塗料。【00013】 此外,本發明之奈米散熱塗料第三實施例,係將120g氟碳樹脂溶於100g醋酸乙脂中得到基料混合液,另將30g奈米竹炭溶於70g蒸餾水中得到填料混合液,而用350目篩網進行過濾該基料混合液與該填料混合液,然後用剪切乳化機高速攪拌該基料混合液與該填料混合液10分鐘,而混合均勻為奈米散熱塗料。【00014】 基於如是之構成,本發明使用氟碳樹脂做為奈米散熱塗料之基料,而由於氟碳樹脂引入的氟元素電負性大,碳氟鍵能強,乃具有優越的耐候性、耐熱性、耐低溫性及耐化學藥品性,且具有獨特的自清潔性,進而產生抗污染環保的作用;另,選自奈米竹炭、奈米碳管、奈米氧化鋅、奈米氧化鍺或前述填料之組合做為奈米散熱塗料之填料,而因這些填料具有高度發達的孔隙結構致使表面積大,增加了擴散表面積,加速了散熱速率;其中,奈米竹炭具有很高的輻射能,熱焓低,同樣有利於改善材料的散熱效果;是以,具有抗污染性佳及高散熱性之功效。又,選自天拿水、醋酸乙酯、無水乙醇、蒸餾水或前述混合溶劑之組合做為混合溶劑,而因這些混合溶劑的溶解效果好,另具有利於填料均勻分散之功效。【00015】 綜上所述,本發明所揭示之技術手段,確具「新穎性」、「進步性」及「可供產業利用」等發明專利要件,祈請 鈞局惠賜專利,以勵發明,無任德感。【00016】 惟,上述所揭露之圖式、說明,僅為本發明之較佳實施例,大凡熟悉此項技藝人士,依本案精神範疇所作之修飾或等效變化,仍應包括在本案申請專利範圍內。[00010] First, as shown in FIG. 1 , the preparation method of the nano heat-dissipating paint of the present invention comprises the following steps: a. dissolving the fluorocarbon resin as a base material in a mixed solvent to obtain a base material mixture. a liquid, and the weight ratio of the base material to the mixed solvent is 0.9 to 1.4 times; b. a filler having a pore structure in a weight ratio of 0.2 to 0.33 times the base material is dissolved in a mixed solvent to obtain a filler mixture, and The weight ratio of the filler to the mixed solvent is 0.3 to 0.6 times; c. the mixture of the base obtained in the step a and the mixture obtained in the step b are filtered using a 350 mesh screen; and d. The filtered mixture of the base material and the filler is uniformly mixed by a shear emulsifier at a high speed. [00011] In the first embodiment of the nano heat-dissipating paint of the present invention, 120 g of fluorocarbon resin is dissolved in 120 g of ethyl acetate to obtain a base mixture, and 30 g of naphtha charcoal is dissolved in 80 g of absolute ethanol. The mixture of the filler is filtered, and the mixture of the base material and the filler is filtered by a 350 mesh sieve, and then the mixture of the base material and the filler is stirred at a high speed by a shear emulsifier for 10 minutes, and the mixture is uniformly mixed into a nanometer. Heat sink coating (see "Figure 2"). [00012] In addition, in the second embodiment of the nano heat-dissipating paint of the present invention, 120 g of fluorocarbon resin is dissolved in 100 g of water to obtain a base mixture, and 30 g of naphtha charcoal is dissolved in 60 g of ethyl acetate. The mixture of the filler is filtered, and the mixture of the base material and the filler is filtered by a 350 mesh sieve, and then the mixture of the base material and the filler is stirred at a high speed by a shear emulsifier for 10 minutes, and the mixture is uniformly mixed into a nanometer. Heat sink coating. In addition, in the third embodiment of the nano heat-dissipating paint of the present invention, 120 g of fluorocarbon resin is dissolved in 100 g of ethyl acetate to obtain a base mixture, and 30 g of naphtha charcoal is dissolved in 70 g of distilled water to obtain a filler mixture. Liquid, and the mixture of the base material and the filler is filtered by a 350 mesh sieve, and then the mixture of the base material and the filler is stirred at a high speed by a shear emulsifier for 10 minutes, and uniformly mixed into a nano heat-dissipating paint. . [00014] Based on the constitution, the present invention uses a fluorocarbon resin as a base material for a nano heat-dissipating paint, and the fluorine element introduced by the fluorocarbon resin has a large electronegativity and a strong carbon-fluorine bond, and has excellent weather resistance. , heat resistance, low temperature resistance and chemical resistance, and has a unique self-cleaning property, which in turn produces anti-pollution and environmental protection; in addition, it is selected from the group consisting of nano bamboo charcoal, carbon nanotubes, nano zinc oxide, and nano oxidation.锗 or a combination of the foregoing fillers is used as a filler for nano heat-dissipating coatings, and these fillers have a highly developed pore structure, resulting in a large surface area, increased diffusion surface area, and accelerated heat dissipation rate; among them, nano-charcoal has high radiant energy. The heat is low, which is also beneficial to improve the heat dissipation effect of the material; therefore, it has the effects of good anti-pollution and high heat dissipation. Further, a combination selected from the group consisting of dicamba, ethyl acetate, absolute ethanol, distilled water or the aforementioned mixed solvent is used as a mixed solvent, and since the mixed solvent has a good dissolving effect, it also has an effect of facilitating uniform dispersion of the filler. [00015] In summary, the technical means disclosed in the present invention have the invention patents such as "novelty", "progressiveness" and "available for industrial use", and pray for the patent to encourage the invention. There is no sense of morality. [00016] However, the drawings and descriptions disclosed above are only preferred embodiments of the present invention, and those skilled in the art who are familiar with the art, the modifications or equivalent changes made in the spirit of the present invention should still include the patent application in this case. Within the scope.
圖1係本發明之奈米散熱塗料製備方法之工序流程圖。圖2係本發明之奈米散熱塗料之電子顯微鏡圖。1 is a flow chart showing the steps of a method for preparing a nano heat-dissipating paint of the present invention. 2 is an electron micrograph of the nano heat-dissipating paint of the present invention.
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