TW201103720A - Positionable gas injection nozzle assembly for an underwater pelletizing system - Google Patents

Positionable gas injection nozzle assembly for an underwater pelletizing system Download PDF

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Publication number
TW201103720A
TW201103720A TW099118710A TW99118710A TW201103720A TW 201103720 A TW201103720 A TW 201103720A TW 099118710 A TW099118710 A TW 099118710A TW 99118710 A TW99118710 A TW 99118710A TW 201103720 A TW201103720 A TW 201103720A
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TW
Taiwan
Prior art keywords
nozzle
nozzle tube
tube
particles
housing
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TW099118710A
Other languages
Chinese (zh)
Inventor
Robert G Mann
Charles W Simmons
Robert A Ryan
Original Assignee
Gala Inc
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Priority claimed from US12/457,442 external-priority patent/US8007701B2/en
Application filed by Gala Inc filed Critical Gala Inc
Publication of TW201103720A publication Critical patent/TW201103720A/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/02Making granules by dividing preformed material
    • B29B9/06Making granules by dividing preformed material in the form of filamentary material, e.g. combined with extrusion
    • B29B9/065Making granules by dividing preformed material in the form of filamentary material, e.g. combined with extrusion under-water, e.g. underwater pelletizers

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

A positionable gas nozzle assembly having a nozzle tube for injecting and directing pressurized air or other inert gas into a pellet slurry so as to increase the velocity of the slurry from a pelletizer to and through a dryer. The variably positionable nozzle tube can be inserted, retracted and/or intermediately positioned either manually or using an automated control system. The automated control system preferably includes a pneumatic cylinder movably engaged with a carriage that is fixedly coupled to the nozzle tube. The pneumatic cylinder contains a piston that is magnetically coupled with the carriage such that movement of the piston in response to the injection of pressurized air into the cylinder also moves the carriage and the nozzle tube to obtain the variable positions.

Description

201103720 六、發明說明· 本發明是2008年6月16曰共同申請之美國申請案第 12/213,204號之部份連續申請案,且在此請求其優先權。 【發明所屬技術領域;J 發明背景 1. 發明領域 本發明係大致有關於水下造粒系統,且特別係有關於 一與這系統一起使用之氣體注射噴嘴。 I:先前技術3 2. 相關技術之說明 發明所屬技術領域中具有通常知識者已發現產生部份 或完全結晶之顆粒是有利的且有時是必要的。為了協助實 現該結晶,在美國專利第7,157,032號;美國專利申★青案公 開第2〇05/0110182及2〇07/0132134;世界專利申請案公開第 W02005/051623號及WO2006/127698號中,本發明之受讓 人已揭露利用一喷嘴’且加壓空氣或其他氣體可通過該喷 嘴被注射入顆粒漿液中,以協助減少在上游造粒製程及了 游與後續製程間在輸送液體中之顆粒的停留時間,所有上 述專利及專利申請案均為本發明之受讓人擁有且在此如同 其全部完全揭露般加入作為參考。 類似地,W02007/027877揭露利用一嘴嘴,且加壓空氣 或其他氣體可通過該喷嘴被注射入顆粒漿液中,以促進在 該顆粒漿液中由顆粒抽吸液體。藉減少在上游造粒製程及 下游與後續製程間在輸送液體中之顆粒的停留時間,降低 201103720 該等顆粒之水分含量。減少之停留時間亦會產生更多所形 成顆粒之内㈣保持,且因此減少可供該等顆粒吸入之水 分。這巾㈣亦為本發之㈣人擁有,且亦全部在此加入 作為參考。 在某二條件τ ’顆粒會在造粒製程中凝結或形成集 塊。,形成顆粒集塊可有許多,其中黏性顆粒是一般的 且4見的心些集塊形成時,它們具有被捕捉在所謂“暫 jT點(hang up p〇lnts) +的傾向在此使用之用語“暫停 1在i個製財顆粒或顆粒之集塊會被暫停且滞 留.· 工成—阻礙堆積物的位置。舉例而言顆粒之集 鬼曰在w延時形成’過多炼融材料流過模孔發生在模 板上因此產生—不需要之大顆粒。大顆粒不是唯-的問 題’具有所㈤尺寸之顆粒亦會產生—問題。與喷嘴接觸之 黏I1 生顆粒或仍疋軟的顆粒會被“壓碎,,且由於它們的黏性 及匕們移動之速度而黏在噴嘴上。最後越來越多的顆粒與 黏在喷嘴上之顆粒接觸且顆粒開始互相黏著,產生一顆粒 塊’亦被稱為-集塊。最後該顆粒塊變大到足財斷輸送 液體及顆粒流動通㈣輸送管,這巾斷會迫使造粒製程停 止。 —個此種暫停點已被發現存在使用前述專利與申請案 二述之插入加壓氣體之裝置與方法的造粒管線中,即, 體插A喷嘴位在棚粒輸送管内之點。依據這些先前 &amp;例肖於注射該空氣之嘴嘴係如第i圖所示且大致以符 碗2〇〇夺- . &amp;不°先羽·技術之固定噴嘴管210最好是藉焊接在接 201103720 合部214連接於肘管202中,這固定喷嘴總成200無法移除以 便啟動。由於它無法可操縱地定位以容許該顆粒漿液圍繞 該固定喷嘴管210之周邊自由流動,所以它可因顆粒集塊作 用更作為阻塞之一可能來源。類似地,該固寒位置限制被 注射之空氣或其他氣體可透過閥調節被控制的程度。 因此,存在一可被調整以使由水下造粒系統產生之顆 粒的結晶及/或乾燥最佳化之可定位喷嘴的需要。 【發明内容】 發明概要 有鑒於前述者,本發明之一目的是提供一可定位喷 嘴,加壓氣體通過該可定位噴嘴被導入一水下造粒機之輸 送裝置,以增加一由一造粒製程被輸送至且通過一乾燥製 程之顆粒漿液的速度,同時透過該喷嘴之位置之改變,控 制該漿液流動之動態。 本發明之另一目的是提供一具有一喷嘴管及軸環之可 定位喷嘴,該可定位喷嘴在一殼體内滑動,該殼體連接於 一密封過渡轴環且固定於一肘管,該肘管在輸送通路内且 在該造粒裝置及該乾燥裝置之間。 本發明之另一目的是依據前述目的提供一可定位喷 嘴,其可在至少完全插入或前向位置與一完全抽出位置之 間調整,且定位該喷嘴以達成此調整係手動地或藉一單獨 或組合地使用機械、氣動、液壓、電氣、電子或其他方法 之自動控制系統來實現,以可適用於一特殊應用。 本發明之再一目的是依據前述目的提供一可定位喷 201103720 嘴,其可使用在前一目的中提出之任一方法手動地或自動 地調整,以將加壓氣體注射於一或多個中間或部份插入位 置。 本發明之又一目的是依據前述目的提供一可定位喷 嘴,其呈角度地定位在它連接之該肘管的内腔内,使得角 度範圍係由相對該下游總成之中心線之大約〇°至藉接觸該 喷嘴管之外側與該下游總成之内側表面所界定之最大角 度。 本發明之另一目的是提供一可定位噴嘴,其被圍繞該 下游設備之中心線同心地居中。 本發明之再一目的是提供一可定位噴嘴,加壓氣體通 過該可定位喷嘴被導入,此增加一由一造粒裝置被輸送至 且通過一乾燥裝置之顆粒漿液的速度,使得該等顆粒之内 熱被保持,以促進該等顆粒之乾燥,使得離開該乾燥裝置 之顆粒的水分含量小於大約1. 0重量%,且以小於0. 5重量% 更佳,並且以小於0. 25重量%最佳。 本發明之又一目的是提供一可定位喷嘴,加壓氣體通 過該可定位喷嘴被導入以增加一由一造粒裝置被輸送至且 通過一乾燥裝置之顆粒漿液的速度,使得該等顆粒之内熱 被保持,以同時促進該等顆粒之乾燥與結晶兩者。 本發明之另一目的是依據前述目的提供一可定位喷 嘴,加壓氣體通過該可定位喷嘴被導入,此增加一由一造 粒裝置被輸送至且通過一乾燥裝置之顆粒漿液的速度,使 得離開該乾燥裝置之顆粒結晶至少2 0重量%,且以至少3 0重 201103720 量%更佳,並且以至少40重量%最佳。 本發明之再一目的是提供一可定位喷嘴,其可至少部 份地抽出以在啟動該造粒製程時防止暫停,且可向前移動 以加快該顆粒漿液流入及通過該輸送管並在該等顆粒移動 通過該輸送管時促進抽吸該輸送液體遠離該等顆粒。 本發明之又一目的是提供一可定位喷嘴,其具有多數 橫截面形狀、内表面變化或内部結構之任一者,以對該顆 粒漿液之流動產生特定之所需效果。 依據這些及其他目的,本發明係有關於一種與一水下 造粒機裝置一起使用之注射設備,該水下造粒機裝置擠壓 且切割多數聚合物條成為多數顆粒,且該等顆粒成為一水 與顆粒漿液被輸送通過輸送管路至一離心乾燥機。該注射 設備包括一可調整注射位置之可定位喷嘴總成,以將一顆 粒加速物導入該水與顆粒漿液,增加該顆粒漿液到達及通 過該乾燥機之速度,使得更多顆粒之内熱被保持。該喷嘴 總成可在一完全插入位置及一完全抽出位置之間調整,在 該完全插入位置中,該總成之一噴嘴管向前地定位在該輸 送管路内,在該完全抽出位置中,該喷嘴管由該輸送管路 抽出以提供該漿液通過該管路之一完全不受阻礙的流動。 較佳地,該可定位喷嘴總成構形成使得該喷嘴管可手動地 或利用一自動控制系統不僅定位在該等完全插入及完全抽 出位置處,並且亦定在該完全向前插入位置及該完全抽出 位置之間的各種中間位置處。 隨後將明白之這些優點與其他目的及好處係在以下更 201103720 完整說明與請求之構造及操作的細節中,且參照形成其一 部份之添附圖式,其中全部類似之符號表示類似部件。 圖式簡單說明 第1圖是一先前技術之固定喷嘴配置之一切除及橫截 面圖。 第2圖是一依據本發明之水下造粒系統之示意圖,該水 下造粒系統包括一水下造粒機及輸送管路,且一可定位喷 嘴連接於一離心乾燥機。 第2a圖是顯示第2圖之可定位噴嘴的一放大圖。 第3圖是第2a圖之可定位喷嘴及輸送管路之一部份之 切除及橫截面圖,且該喷嘴管在一抽出位置。 第4圖是第2a圖之可定位喷嘴及輸送管路之一部份之 切除及橫截面圖,且該喷嘴管在一向前插入位置。 第5圖是第2a圖之可定位噴嘴及輸送管路之一部份之 示意俯視圖,且該喷嘴管在該向前插入位置。 第6a圖是使用一自動控制系統之第2a圖之可定位喷嘴 及輸送管路之一部份之切除及橫截面圖,且所示之喷嘴管 在一抽出位置。 第6b圖是沿著第6a圖之線6b-6b所戴取之喷嘴管殼體 的視圖。 第6c圖是第6a圖之自動控制系統實施例之切除及橫截 面圖,且所示之喷嘴管在一向前插入位置。 第6d圖是沿著第6d圖之線6d-6d所戴取之喷嘴管殼體 的視圖。 8 201103720 第7圖是一用於第如如圖之 無桿壓缸的部份切除圖。 卫制系統中之礤耦合 第8圖是一顯示用於第6 電路的圖。 圖之自動控制系統之控制 第切明之含有 刚孔口的圖。 罝翼片之哨·嘴管之 弟9b圖是本發明之含有堂 前孔口的圖。 &quot;直定向輪廓翼片之嘴嘴管之 第9c圖是本發明之 第9d圖是本發明 的圖 之前孔口 第9e圖是本發明之_ 第_是本發明之―具$縣端之喷嘴管 的圖 的圖。 漸縮圓錐形軌之噴嘴管 t實方也方式】 發明之詳細說明 雖然詳細地說明本發明之較佳實施例,但是在此應了 解的是可有其他實施例。因此,本發明之料不應受限於 在以下說明中揭露或在圖式中顯示之結構的細節、元件的 配置。本發明可為其他實施例且可以各種方式實施。又, 在所述較佳實施例中,為了清楚起見,將依靠特定用語。 在此應了解的是各特定用語包括以一類似方式操作以達成 一類似目的之所有技術等效物。只要可能,圖式之類似元 件係以相同符號表示。 201103720 本發明之可定位喷嘴總成協助促進各種聚合材料之結 晶且亦促進這些及其他材料之乾燥,同時消除已在先前設 計中遭遇之一集塊之可能暫停點。利用注射入該顆粒輸送 管路之加壓空氣或其他氣體,該顆粒漿液之速度增加。結 果是,由於速度增加及抽吸輸送液體遠離這些顆粒之表 面,該等顆粒受該輸送液體支配之時間減少。由於速度增 加,該等顆粒在該輸送液體中之停留時間較少,容許該等 顆粒保持比它們受該輸送液體支配一較長時間更多的内 熱。事實上,增加保持之内熱有助於該等顆粒之結晶。這 效果藉抽吸該輸送液體遠離該等顆粒之表面而更加強,使 得對該輸送液體之熱損失減少。 為了達到該等顆粒之最大通過量,本發明容許該喷嘴 之外形尺寸及位置可以調整。這對於漿液由該造粒機輸送 至該乾燥機之速度是重要的,這會再衝擊該系統藉抽吸分 離該等顆粒與該輸送液體及增加被該等顆粒保持之内熱之 量的效率。改變該喷嘴之外形尺寸及位置亦可用來改變該 漿液通過輸送管路之流動模式,產生或多或少之渴流,以 達成與被加工之材料相關之特定需求。 以下請參閱第2圖,大致以符號100表示之本發明之可 定位喷嘴組裝成大致以符號15表示之輸送管路,該輸送管 路15連接造粒裝置10與乾燥裝置20及任何後續之後處理。 一熔化及混合裝置(圖未示)連接於造粒機10,該造粒機10 連接於注入管12。輸送液體透過注入管12導入造粒機10之 切割室,且它在該切割室與該等顆粒混合以形成該顆粒漿 10 201103720 液。該顆粒漿液經由排出管14排出進入且通過觀察孔16, 並接著通過在輸送管路15中之可定位喷嘴總成100。一顆粒 加速物被注射且引導進入該輸送管路通過該可定位喷嘴總 成100以減少該等顆粒受該輸送液體支配之時間。由於其惰 性本質及立即可用性,該顆粒加速物最好是空氣。但是, 亦可使用如氮或類似氣體等具有惰性性質之其他氣體。該 被加速顆粒及輸送液體通過輸送管路18進入且通過乾燥機 總成20,該等顆粒在該乾燥機總成20中脫水及乾燥。該被 加速顆粒及輸送液體之細節說明如下。 該熔化及混合裝置(圖未示)可以是任何習知裝置或其 組合且可包括,但不限於,之熔化容器、單螺旋擠壓機、 雙螺旋擠壓機、靜態混合器、連續混合器、密閉式混煉機 等。 造粒機10可以是一水環造粒機、一水下造粒機等,且 最好是發明所屬技術領域中具有通常知識者已知之一嵌裝 有一擠壓模頭之水下造粒機。輸送液體可以是任何液體且 最好是水,除了水外以,依據本發明可用於造粒其他液體 包括乙醇、水-乙醇混合物、礦物油、蔬菜油、乙二醇混合 物等。或者,水或其他輸送液體可包含多數添加劑,包括, 但不限於,調流劑、塗料、消泡劑、共溶劑等。如在此所 使用,當連同該輸送液體參照“液體”或“水”時,這些 參照所指的是適用於作為一輸送液體之任何液體,具有或 沒有添加劑,且不僅是水。 本發明之被造粒及輸送的材料可以是聚合物、蠟及以 201103720 往被造粒加工之其他可擠壓材料。舉例而言,該等材料可 包括聚烯垣、聚醚、聚硫趟、聚醯胺、聚醯胺酿亞胺、聚 颯、聚碳酸酯、聚胺基甲酸酯、氟聚合物、乙烯聚合物、 可生物分解之聚合物、及其共聚合物。通常在進一步加工 之鈾被結晶之材料特別適用於依據本發明加工,且較佳 地,該等材料可以被乾燥至一小於丨重量%之水分含量且被 結晶至一至少20%之程度。更佳地,該等材料可以被乾燥至 小於0. 50重量%之水分含量且被結晶至一至少3⑽之程 度最佳地,該等材料可以被乾燥至一小於〇. 25重量%之水 刀含里且被結晶至一至少40%之程度。 替代地或任擇地,本發明之欲被造粒之材料可包含發 月所屬技術領域中具有通常知識者已知之任何習知填料及 填料及/或其他添加敎組合。該等填财包括纖維素粉末 及/或纖維、包括粉末及纖維之生物材料等。 、第2圖中之乾燥機可以是一脫水裝置、過濾裝置、 #動脫水裝置、流體化床、滾筒乾燥機、離心機、乾燥機、 :,燥機之至少-者’且最好是-自行清潔離心乾燥 。但是,用以分離該液體與在該液體及顆粒漿液中之顆 粒的任何分離裝置均可在本發明中制。後處理可包括但 不限於發明所屬技術似巾具有通f知識者已知之冷卻、 加強結晶、加熱、再乾燥、精壓加工、 固態 聚合、包裝等。 本七明之可定位噴嘴總成1〇〇之一實施例詳細地顯示 在第2a圖之放大圖中。如虛線所示,該總成包括-閥104、 12 201103720 一管路106、一單向閥108、及一喷嘴管110,該噴嘴管11〇 部份地插入肘管102且看不到。該喷嘴管11〇在插入點112處 插入肘管102且延伸入肘管102之内腔中到達肘管1〇2之接 合部114及流出管116 ’未顯示之進入氣體管線連接於一最 好是一球閥的閥104。 通過觀察孔16(見第2圖)之顆粒漿液通過流入管118且 進入並通過肘管102,在此它在通入流出管116及通過閥12〇 之前,與最好是空氣之加壓氣體交互作用。流入管118、肘 管102及流出管116可以是一已藉彎曲修改過以形成該肘管 且容許喷嘴管110插入之單件式管。但是,較佳地,該流入 管118、肘管102及流出管116是例如藉螺合或焊接連接在一 起之分開元件。流入管118及流出管116可具有與1〇2相同之 直徑,或它們可以具有與肘管102不同之直徑,在此情形 中,它們最好是漸縮至肘管1〇2之直徑。依據一較佳實施 例,流入管118及肘管102具有相同直徑且流出管116之直徑 由與肘管10 2之接合部114呈錐形地減少至與管延伸部1 &amp; 之連接處,該管延伸部122延伸至且連接於閥12〇。閥12〇最 好藉螺合或藉焊接連接於輸送管路18。 或者,流出管116及管延伸部122可藉一快拆連接器125 可分離地連接,如第2a圖所示。該快拆連接器125可以是任 何適合之營快拆總成,這種連接器有助於輕易通達該肘管 及噴嘴總成以便依需要檢查 '清潔、維護、及修理。 流入f 118、肘管1〇2 '流出管116及嘴嘴管11〇最好是 由包括工具鋼、飢鋼、碳鋼、硬化鋼、不鏽鋼、錄鋼等之 13 201103720 金屬構成’但亦可由耐磨工業級塑膠製成。這此元件以由 不鏽鋼製成更佳且由低碳不鏽鋼製成最佳。 單向閥108最好放置在一收納槽(圖未示)及該財管 之間且防止水及顆粒逆流進入該收納槽。單向閥1 〇 8容許加 壓空氣或其他氣體流經過它’但當空氣或其他氣體未通過 它時’來自該輸送液體之壓力將使單向閥1〇8關閉,因此防 止輸送液體及顆粒逆流。或者,最好是—具有一致動器之 電動機械閥的一自動閥可取代單向閥1 〇8。 閥104容許操作者控制該加壓空氣或其他氣體之流 量。較佳地,一球閥之閥104例如藉螺拴連接、焊接或螺接 連接於噴嘴管110。閥104最好依序連接於管路1〇6、單向閥 ⑽及喷嘴管11G。任擇地或替代地,—電動機械閥可取代 閥104與單向閥ι〇8兩者。 閥120更可調整該加壓空氣或其他氣體之逮度。閥1〇4 可關閉以容許習知造粒加工且不需加壓氣體注射。闊刚及 閥120是任擇的且任—者均可單獨使用而不需另_者。較佳 地’閥1〇4係用來調整加壓氣體且更佳地,間⑽與間12〇係 以合作組合之方式用於最大地控制及調整該加壓空氣或其 他氣體。 該可定位噴嘴總成較佳地定位如第2圖所示且詳細顯 不在第以、3、4及5财。請參見第2圖,以一輸送管㈣ 作為實施例之—輸送導管最好是筆直的且空氣或其他氣體 被注射入肘㈣2。仏、3及4圖最好錢送管㈣之軸成 一直線以使該注射對該顆粒驗的效果達到最大且均一地 14 201103720 抽吸該顆«液。肘㈣2或如—“γ”構形之等效結構的 位置取好是在該顆粒漿液離開造粒機丨〇後在該第一肘管 中。但是’該肘管102可位在-更遠離圖未示之造粒 機10且 在乾燥機20之前的選擇性肘管中。或者,多數喷嘴管可被 插入至少-肘管,以合作地促進輸送至及通過至少一輸送 管路18。 第3圖顯示在相對肘管1G2之-完全抽出位置之可定位 喷嘴總成100的-部份。如圖所示,該喷嘴管11〇之後端被 軸%122包圍,當該喷嘴管在圓柱形殼體128内滑動時,該 軸環122引導該後端。該噴嘴管11〇及軸環122可以是一單體 • 構造,但最好該喷嘴管110及轴環122是例如藉焊接連接在 一起之分開元件。該噴嘴管110及軸環122最好焊接在該軸 環之各端,在焊接件124與焊接件126處。 δ玄噴嘴管11〇及轴環122可變地定位且可自由地滑動通 過該殼體128 ’該殼體128之前端130螺接於一密封過渡轴環 132 ’該密封過渡軸環132在接合部112連接於肘管1〇2。該 喷嘴管110之前端被滑動地支持在該軸環132之中央孔133 内’在該殼體128内且於環繞該喷嘴管11〇沿圓周定位的是 一拉伸彈簧134。至少一導銷136連接於該軸環122,該導銷 136對齊且可定位在殼體128中之至少一溝槽138内,如第5 圖所詳示。對較大輸送管路及喷嘴總成而言,具有分別可 定位地對齊在殼體128中之兩溝槽138以提供較大之調整能 力的至少兩導銷136是較佳的。溝槽138係沿著殼體128之長 度呈直線長形且形成如第3圖所示之至少一角凹部14〇,或 15 201103720 如弟5圖所示之多數凹部“ο、mi。 請再參閱第3圖’最好是一螺旋彈f之拉伸彈菁134放 置在轴環122之前面上且在密封過渡軸環132之後面上。在 第3圖中,該拉伸彈簧134於該喷嘴管總成之抽出位置時拉 長。第4圖顯示該拉伸彈簧134在該可定位喷嘴總成ι〇〇之最 前方位置中被壓縮’其中該喷嘴管UQ完全被插入該肘管 102之内腔中。如圖所示,當完全被插入時,該軸 收納在該殼體128中’且導銷136被鎖定在角凹部14〇中,如 第更清楚地顯示。另-方面,當該噴嘴管僅部份地被插 入時’該導銷136將被鎖定在角凹部141中。 噴嘴管11〇最好被密封地定位在密封過渡軸環132中, 請參見第3與4圖。密封係藉包括〇環、“四邊形,,環、機械密 ^等發明所屬技術領域中具有通常知識者已知之任何機械 裝置,且不限於此。較佳地,密封係使用被扣持在密封過 渡輛環132之一圓周溝槽M4中的至少一 〇環142。◦環142密 封地嵌套環繞噴嘴管110之直徑,使得喷嘴管11〇可以被密 封地且可滑動地定位通過該至少一0環142。較佳地,至少 兩0環142分別被密封地定位在兩圓周溝槽144中。最佳地, 多數〇環14 2被密封地定位在同樣多數之圓周溝槽丨4 4中。 第5圖顯示可定位喷嘴總成100之一部份,其中如同等 如上地在第2a圖中顯示與說明者,該噴嘴管11〇被完全插入 肘官102之内腔中’大致與接合部114齊平。軸環丨22已被插 入殼體128中且導銷136已移動通過溝槽138而可被牢固地 定位在角凹部140中。 16 201103720 喷嘴管110可以被大致定位在由密封過渡軸環丨32内腔 内之肘管102的外部外側到至少該接合部114或者超出該接 合部114的整個範圍内。較佳地,該完全抽出位置係大致與 肘管102之外部齊平且該完全插入位置係大致在該接合部 114 處。 該喷嘴管11 〇在該可定位喷嘴總成1 〇〇内之移動可以藉 包括手動或最好利用一或多個自動控制系統等任何適當方 法來完成,該自動控制系統單獨或以各種組合地包括氣 動、電氣、電子、液壓裝置及方法,且可選擇性地包括可 程式邏輯控制,PLC。亦可在相同喷嘴總成内組合手動及自 動控制能力。由於被該角凹部140位置決定,故手動控制必 須特定安排該定位。但是,如果移動是自動的,則有多數 位置可供使用。例如,使用在第5圖中之導銷136及相關溝 槽138及角凹部14G與141,將不被預期必須使用—自動控制 系統來控制。 具有一用以定位該喷嘴之自動控制系統之本發明之可 疋位喷嘴的一較佳實施例顯示在第6a_6d圖中,在這實施例 中,該喷嘴使用一被使用者控制之氣壓缸氣動地移動至所 需位置。該氣壓缸最好是-大致以符號154表示之磁輕合無 桿壓缸,其磁性地結合-載架16G,該載架⑽藉一托架或 銷162固定連接於該喷嘴管11〇及軸環122。如圖所示,在第 6a與6c圖中,銷162最好連接在該載架16〇與軸環122之間, 且再焊接在喷嘴f 11Q上。但是,關162可以直接連接於 噴嘴管110。該銷162可藉發明所屬技術領域中具有通常知 17 201103720 識者已知之任何適當連接方法連接於該載架160及軸環 122/喷嘴管110,但是最好以螺栓連接至該載架160及軸環 122。該銷162藉一在殼體129中之槽孔139,通過包圍該噴 嘴管110及軸環122之殼體129,如第6b與6d圖所示。 可使用在本發明之一磁耦合無桿壓缸係在Series CY1B下由美國之SmC公司製造。如第7圖所示,該無桿壓 缸154包括一其中具有一活塞172之缸管170,該活塞172設 有一第一磁鐵174。一第二磁鐵175被支持在該載架160之— 本體176中且在該缸管170外側。 一用以使用該氣壓缸移動該喷嘴管110之控制電路係 顯示於第8圖中且大致以符號190表示。相對於喷嘴末端 155,該氣壓缸154在其遠端157處具有一第一空氣入口 156 且在其近端159處具有一第二空氣入口 158。為了移動該喷 嘴管110至第6c與6d圖所示之完全插入向前位置,致動—如 按鈕180之内推機構,這將改變空氣操作之阻擋閥181之位 置’以將加壓空氣注射入該第一空氣入口 156。該空氣在兮 近知)159之第二空氣入口 158處亦被注射入一單向閱184,vsr 開啟έ亥單向閥184且釋放已在壓缸154近端或前端中之加^ 空氣,藉此使該活塞172及與其磁性地結合之載架16〇可向 前移動,且銷162在該槽孔139中移動至第6d圖中所示之位 置。 相反地,為了使該喷嘴管110由該插入位置移動至第仏 與6b圖所示之一柚出位置,致動一如按鈕182之外推機構, 這改變一空氣操作之阻擋閥181之位置,以將加壓空氣主射 18 201103720 入該第二空氣入口 158。該空氣亦在遠端157之第一空氣入 口 156處被注射入一單向閥185,這開啟單向閥丨84且釋放已 在壓缸154遠端或後端中之加壓空氣,藉此使該活塞172及 與其磁性地結合之載架160可向前移動,且銷162在該槽孔 139中移動至第牝圖中所示之位置。在定位情況之間,在該 氣壓缸154處之單向閥184及單向閥185,由於被該控制電路 190控制,藉不容許空氣由空氣入口 156或空氣入口 158釋 出,將該噴嘴管固持定位》單向閥184及185亦提供速度控 制,以調節多快可使該喷嘴管移動。 用以使该活塞及載架160移動之加壓空氣可由如發明 所屬技術領域中具有通常知識者已知之空氣槽壓縮機等各 種空氣來源供應。利料氣動實施例,在該完全插入(第&amp; 與6d圖)與完全抽出(第仏與此圖)位置之間之喷嘴管之任 意數目的t間位置可錢過㈣被注射人料空氣入口 156、158中之加壓空氣量來實現。或者,類似之喷嘴管的 移動與控制可透過使用—線性氣壓紅,—液壓缸及動力單 兀、或與-滾珠螺桿或愛克姆螺桿(a_ %爾卜起之一飼 服馬達或步進馬達,而不是透過如發明所屬技術領域中 具有通常知識者已知之該磁轉合無桿壓缸154。但是,該磁 耦合無桿壓缸對於本發明而言是較佳的。 依據本發明,如有需要,用以移動該喷嘴之較佳自動 控制系統可與該噴嘴管之手動移動結合在一起。 較佳地’在该造粒機1〇 “啟動,,時,喷嘴管11〇可被放 置在一抽出位置’以避免其存在成為-在該輸送管路15中 19 201103720 之障礙。由於促使噴嘴管110抽出是有利的,故不需要之集 塊可在該造粒製私之開始狀態時輕易地形成且容許該顆粒 漿液使用輸送管路U之全内徑。 可定位噴嘴總成10 0係設計成容許操作者將加壓空氣 或其他氣體注射入輸送管路18 ,同時具有相對於該輸送管 路18及肘管1〇2調整該噴嘴管11〇之位置的選擇。噴嘴管11〇 可以抽出及插入且仍產生所需抽吸之程度係依靠,但不限 於:流量、顆粒對輸送液體比例、輸送液體溫度、肘管1〇2 相對該輸送管路18之直徑、在該肘管1〇2與該乾燥機2〇之間 的距離'及被造粒之材料種類來決定。 在此應了解的是,如第2a、3與4圖所示,喷嘴管之 外徑將小於例如,在接合部114之肘管1〇2之内徑。在這方 面,在内腔中之空間應大到足以容許使用具有用於該特殊 造粒系統之最大尺寸之顆粒所測量之至少兩顆粒的組合最 大尺寸,可通過在該噴嘴管11〇之外部與在接合部ιΐ4處之 肘管102内部之間。換言之,在該喷嘴管之外徑與該財管内 腔之内徑之間的間㈣域A到足以料各具有該造粒機之 最大尺寸之至少兩顆粒,可通並排通過其中且不會阻塞或 堵塞在該間隙區域中。舉例而言,不受限於此,本發明之 =實施例係至肘管之-G. 75英忖公稱噴嘴管11〇與一2 英时公稱喷錢八管1_組合,-2英私稱肘;I; 1G2,及 一由肘官102至乾燥機2〇之1.5英吋輸送管路18。另一實施 例係一0.75英时公稱喷嘴管11Q與-3·ο英时公稱肘管1〇2 之組合’且又—實關係5射公稱噴嘴管UG與一2. 〇 20 201103720 英吋公稱肘管之組合。 該噴嘴管110相對於第2a圖中之肘管102之接合部114 的方位可以環繞接合部114之中心線同心地居中,或在該中 心上方、在該中心線下方反射至該中心線之右或左,或在 任何角度沿圓周地環繞該中心線,其令形成在該喷嘴管110 之中心線與肘管1〇2之中心線之間的角度樹脂可由〇。至一 最大偏轉角。最大偏轉角係定義為喷嘴管110之外部接觸肘 管102之接合部114及/或該可定位喷嘴總成1〇〇延伸入肘管 102之接合部114下游之任何裝置的偏轉角度。較佳地,噴 嘴管110環繞肘管102之接合部Π4之中心線同心地定位且 共線。在此應了解的是肘管1 〇2之接合部114之中心線與接 合部114下游之輸送管路18之中心線共線。 喷嘴管110之前孔口 146可以呈包括圓形、正方形、矩 形' 橢圓形、多邊形等任何形狀且最好是圓形。該前孔口 146之直徑可大於、小於、或等於該喷嘴管11〇之直徑且最 好是等於。當前孔口 146之直徑不等於喷嘴管no之直徑 時,只有噴嘴管11〇之未與該最靠近〇環142接觸之部份的直 徑分別逐漸地增加或減少;請參見第3與4圖。但是,該遠 孔口 146之直徑無法大於該密封過渡軸環132之内徑。—噴 I s 11〇之末女而之漸縮錐形150顯示在第9e圖中,類似地, 該前孔口 146可以是如第9e圖所示之半圓形或如在第_ 中般呈螺旋形至C形。 喷嘴官110之⑽可設有包括但不限於職形 '順形、 _形内表面之至少—者及其許多組合之許多不 21 201103720 同變化。第9f圖顯示一圓錐錐形喷嘴管110,其中該錐形朝 該前孔口 146減少。 喷嘴管110之内侧亦可或者替代地含有一或多個翼片 152,如第9a與9b圖所示。該等翼片可以是筆直的或相對該 喷嘴管110之圓周緣傾斜90°,如第9a圖所示,或傾斜一較 小角度。類似地,該等翼片可以相對該喷嘴管110之圓周緣 彎曲或順形,如第9b圖所示。該等翼片可具有由小於至等 於喷嘴管110之長度之範圍的長度,且它們的高度無法超過 喷嘴管110之半徑。較佳地,該等翼片152小於該喷嘴管110 之長度且高度小於喷嘴管110之半徑。當包含多數翼片時, 它們亦可以互相呈任何角度地放置且構造可相同或不同。 該等翼片之目的是協助在該輸送管路18内產生更多渦流。 詳而言之,該被抽吸之顆粒漿液的流動可由層流變化至渦 流。未欲受限於任何理論,空氣或其他氣體注射入該顆粒 漿液將由該等顆粒抽吸該輸送液體,使得該輸送液體以一 層流方式沿著該輸送管路18輸送,同時蒸氣霧與顆粒在一 更渦旋之流動中沿著輸送管路18之長度傳播通過輸送管路 18之中心。在某些例子中,可能需要更渴旋之流動,此時 可有利地添加多數翼片。 依據本發明,加壓空氣或其他氣體可連續地或間歇地 流經喷嘴管110,最好是連續地流經喷嘴管110。如前所述, 這加壓氣體可被用來以一高速輸送該等顆粒。這高速氣流 可以使用加壓氣體達成,該壓縮氣體使用一用以調整通過 該輸送管路18之壓力到至少8巴(bar)之標準閥104,產生每 22 201103720 小時至少1 〇〇立方公尺之示範性流量。該管路18是標準管 徑,最好是1.5英吋管徑。對發明所屬技術領域中具有通常 知識者而言,流量及管徑將會依據處理量、包含填料之材 料組成、輸送液體溫度、所需結晶度、所需水分含量、及 該等顆粒及微粒之尺寸改變。該高速氣體有效地接觸該顆 粒水漿液,藉抽吸產生水蒸氣,且在整個漿液管線分散該 等顆粒以將這些顆粒以高速傳送至該乾燥機20,最好是以 由該造粒機10至該乾燥機20之出口小於1秒之速度傳送。該 高速抽吸在一空氣/氣體混合物中產生一可接近該氣態混 合物之體積之98-99%之顆粒的混合物。透過調整該喷嘴管 插入深度及在該喷嘴内添加表面變化性,在該輸送管路内 之漿液的流動特性可以改變。 現請參閱第2圖,形成在流入管118之垂直軸與輸送管 路18之縱軸之間的角度可以藉該造粒機10相對於至該乾燥 機20之入口 22之高度的變化,依需要由0°變化至等於或大 於90°,如第2圖所示。這高度差可歸因於該乾燥機20相對 於該造粒機10之實體定位或可以是該乾燥機與造粒機之尺 寸差所造成之結果,較佳之角度範圍是由大約30°至60°,且 更佳之角度是大約45°。進入該乾燥機入口 22之加大肘管24 有助於被高速抽吸之顆粒/水漿液由該輸送管路18轉移至 該乾燥機20之入口 22中且減少顆粒集塊於該乾燥機20中之 可能性。 喷嘴管110之外側表面及流入管118、肘管102、流出管 116與輸送管路18之内腔可藉表面處理來塗覆以減少研 23 201103720 磨、磨蝕、腐蝕、磨耗及不必要黏著與狹窄。該等表面處 理可以是滲氮、碳氮共滲及燒結之至少其中一者。類似地, 前述表面可以單獨地或組合地進行高速空氣與燃料改良熱 處理、電解電鍍、無電電鍍、火焰喷塗、熱喷塗、電漿處 理、無電鎳分散處理、及電解電漿溫度。這些處理使該表 面金屬化,較佳地,將金屬氮化物固定地連接至該表面, 更佳地,將金屬碳化物與金屬碳氮化物固定地連接至該表 面,進一步更佳地,將似鑽石碳固定地連接至該表面,又 更佳地,將在一耐磨金屬基質中之似鑽石碳連接至該表 面,且最佳地,將在一金屬碳化物基質之似鑽石碳連接至 該表面。其他陶瓷材料亦可使用且藉參考包含於此且不欲 受限。在沒有對該被塗覆表面必須密封地通過之部作的直 徑進行適當修改之情形下,該塗層厚度不應超過大約0. 002 英吋。 雖然本發明已藉其較佳形態說明過了,但是發明所屬 技術領域中具有通常知識者將可了解,在不偏離本發明及 在以下申請專利範圍中揭露之本發明等效物的精神與範疇 情形下,可於其中進行許多修改、添加、及刪改。 【圖式簡單說明】 第1圖是一先前技術之固定喷嘴配置之一切除及橫截 面圖。 第2圖是一依據本發明之水下造粒系統之示意圖,該水 下造粒系統包括一水下造粒機及輸送管路,且一可定位喷 嘴連接於一離心乾燥機。 24 201103720 第2a圖是顯示第2圖之可定位喷嘴的一放大圖。 第3圖是第2a圖之可定位喷嘴及輸送管路之一部份之 切除及橫截面圖,且該喷嘴管在一抽出位置。 第4圖是第2a圖之可定位噴嘴及輸送管路之一部份之 切除及橫截面圖,且該喷嘴管在一向前插入位置。 第5圖是第2a圖之可定位喷嘴及輸送管路之一部份之 示意俯視圖,且該喷嘴管在該向前插入位置。 第6a圖是使用一自動控制系統之第2a圖之可定位喷嘴 及輸送管路之一部份之切除及橫截面圖,且所示之喷嘴管 在一抽出位置。 第6b圖是沿著第6a圖之線6b-6b所截取之喷嘴管殼體 的視圖。 第6c圖是第6a圖之自動控制系統實施例之切除及橫截 面圖,且所示之喷嘴管在一向前插入位置。 第6d圖是沿著第6d圖之線6d-6d所截取之喷嘴管殼體 的視圖。 第7圖是一用於第6a-6d圖之自動控制系統中之磁耦合 無桿壓缸的部份切除圖。 第8圖是一顯示用於第6a-6d圖之自動控制系統之控制 電路的圖。 第9a圖是本發明之含有垂直定向筆直翼片之喷嘴管之 前孔口的圖。 第9b圖是本發明之含有垂直定向輪廓翼片之喷嘴管之 前孔口的圖。 25 201103720 第9c圖是本發明之一喷嘴管之半圓形前孔口的圖。 第9d圖是本發明之一喷嘴管之一螺旋形至C形之前孔 口的圖。 第9e圖是本發明之一具有錐形末端之喷嘴管的圖。 第9f圖是本發明之一具有一漸縮圓錐形錐孔之噴嘴管 的圖。 【主要元件符號說明】 10...造粒裝置;造粒機 112*··插入點 12…注入管 114…接合部 14…排出管 116…流出管 15...輸送管路 118…流入管 16…觀察孔 120…閥 18…輸送管路 122…管延伸部;抽環 20...乾燥裝置;乾燥機總成; 124,126···焊接件 乾燥機 125…快拆連接器 22…入口 128…殼體 24…加大肘管 129…殼體 100···可定位喷嘴;可定位喷嘴 130…前端 總成 132…密封過渡軸環 102…肘管 133···中央孔 104…閥 134…拉伸彈簧 106…管路 136…導銷 108···單向閥 138…溝槽 110···喷嘴管 139…槽孔 26 201103720 140,141…凹部 170···缸管 142... Ο環 172…活塞 144...圓周溝槽 174…第一磁鐵 146...前孔口 175…第二磁鐵 150...漸縮錐形 176…本體 152…翼片 180···按鈕 154...壓缸 181…空氣操作之阻擋閥 155···喷嘴末端 182···按紐 156··.第一空氣入口 184,185..·單向閥 157…遠端 190…控制電路 158···第二空氣入口 200...固定喷嘴總成 159…近端 202...肘管 160…載架 210...固定喷嘴管 162…銷 214...接合部 27The invention is a continuation-in-part of U.S. Application Serial No. 12/213,204, filed on Jun. [Technical Field of the Invention; J Background of the Invention 1.  FIELD OF THE INVENTION The present invention relates generally to underwater pelletizing systems, and in particular to a gas injection nozzle for use with such systems. I: Prior Art 3 2.  Description of the Related Art Those having ordinary skill in the art have discovered that it is advantageous and sometimes necessary to produce partially or fully crystallized particles. In order to assist in the realization of the crystallization, in U.S. Patent No. 7,157,032, U.S. Patent Application Serial No. 2,05/0110,182, and U.S. Patent Application Publication No. WO2005/051623, and WO2006/127698, The assignee of the present invention has disclosed the use of a nozzle' and pressurized air or other gas can be injected into the slurry slurry through the nozzle to assist in reducing the transport of liquid between the upstream granulation process and between the swim and subsequent processes. </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> </ RTI> <RTIgt; Similarly, WO2007/027877 discloses the use of a mouthpiece through which pressurized air or other gas can be injected into the slurry of particles to promote the suction of liquid by the particles in the slurry of particles. By reducing the residence time of the particles in the transport liquid between the upstream granulation process and the downstream and subsequent processes, the moisture content of the particles is reduced by 201103720. The reduced residence time will also result in more (4) retention within the formed particles, and thus reduce the amount of water available for inhalation of the particles. This towel (4) is also owned by the (4) person of this issue and is also hereby incorporated by reference. At some two conditions, the τ granules will condense or form agglomerates during the granulation process. There are many possible formations of particle agglomerates, in which the viscous particles are general and the cores are formed when they are formed, and they have a tendency to be captured at the so-called "hang up p〇lnts" + The phrase "pause 1 will be suspended and stagnant in the block of i-making granules or particles. · Workmanship—blocks the location of the deposit. For example, the collection of particles sneaky in the w-delay formation of 'excessive smelting material flowing through the die hole on the template thus producing - unwanted large particles. Large particles are not the only problem. Particles with a size of (five) also produce problems. Adhesive I1 particles that are in contact with the nozzle or particles that are still soft will be "crushed, and stick to the nozzle due to their viscosity and the speed at which they move. Finally, more and more particles stick to the nozzle. The particles on the particles contact and the particles begin to stick to each other, producing a particle block 'also known as a block. Finally, the particle block becomes large enough to transport the liquid and the particles flow through the (four) delivery tube, which will force the granulation. The process is stopped. - Such a pause point has been found in the granulation line using the apparatus and method for inserting pressurized gas as described in the aforementioned patent and application, that is, the point where the body insert A nozzle is located in the granule conveying pipe According to these previous &amp; examples, the nozzle for injecting the air is as shown in Figure i and is roughly robbed by the bowl 2 .  The fixed nozzle tube 210 of the first feather/technical technique is preferably connected to the elbow 202 by welding at the 201103720 joint 214. The fixed nozzle assembly 200 cannot be removed for activation. Since it is not steerably positioned to allow the particle slurry to flow freely around the periphery of the fixed nozzle tube 210, it may be a source of blockage due to particle agglomeration. Similarly, the cold-holding position limits the degree to which the injected air or other gas can be adjusted through the valve. Accordingly, there is a need for a positionable nozzle that can be adjusted to optimize crystallization and/or drying of the particles produced by the underwater pelletizing system. SUMMARY OF THE INVENTION In view of the foregoing, it is an object of the present invention to provide a positionable nozzle through which pressurized gas is introduced into a conveying device of an underwater granulator to increase one by one granulation. The process is transported to and through the speed of the particle slurry of a drying process while varying the position of the nozzle to control the dynamics of the slurry flow. Another object of the present invention is to provide a positionable nozzle having a nozzle tube and a collar, the positionable nozzle sliding in a casing, the casing being coupled to a sealed transition collar and fixed to an elbow, The elbow is in the delivery path and between the granulation device and the drying device. Another object of the present invention is to provide a positionable nozzle that can be adjusted between at least a fully inserted or forward position and a fully withdrawn position in accordance with the foregoing objectives, and that the nozzle is positioned to achieve this adjustment either manually or by a separate It can be implemented in combination with an automatic control system of mechanical, pneumatic, hydraulic, electrical, electronic or other means to suit a particular application. It is a further object of the present invention to provide a positionable spray 201103720 nozzle that can be manually or automatically adjusted using any of the methods set forth in the previous object to inject pressurized gas into one or more intermediates in accordance with the foregoing objectives. Or part of the insertion position. It is a further object of the present invention to provide a positionable nozzle that is angularly positioned within the lumen of the elbow to which it is attached, in accordance with the foregoing objectives, such that the angular extent is approximately 〇° from the centerline of the downstream assembly. The maximum angle defined by contacting the outer side of the nozzle tube with the inner side surface of the downstream assembly. Another object of the present invention is to provide a positionable nozzle that is concentrically centered about the centerline of the downstream device. It is a further object of the present invention to provide a positionable nozzle through which pressurized gas is introduced, which increases the velocity of a slurry of particles that is delivered to and through a drying device by a granulation device such that the particles The heat therein is maintained to promote drying of the particles such that the moisture content of the particles leaving the drying apparatus is less than about 1.  0% by weight, and less than 0.  5 wt% is more preferred, and is less than 0.  25 wt% is the best. It is a further object of the present invention to provide a positionable nozzle through which pressurized gas is introduced to increase the velocity of a slurry of particles transported by a granulation device through a drying device such that the particles Internal heat is maintained to simultaneously promote both drying and crystallization of the particles. Another object of the present invention is to provide a positionable nozzle through which the pressurized gas is introduced in accordance with the foregoing objects, which increases the speed of a slurry of particles which is delivered to and through a drying device by a granulation device. The particles leaving the drying apparatus crystallize at least 20% by weight, and more preferably at least 30% by weight of 201103720%, and most preferably at least 40% by weight. It is a further object of the present invention to provide a positionable nozzle that can be at least partially extracted to prevent a pause when the granulation process is initiated, and that can be moved forward to accelerate the flow of the particulate slurry through and through the delivery tube The movement of the transporting liquid away from the particles is facilitated as the particles move through the delivery tube. It is a further object of the present invention to provide a positionable nozzle having any of a plurality of cross-sectional shapes, internal surface variations or internal structures to produce a particular desired effect on the flow of the slurry. In accordance with these and other objects, the present invention is directed to an injection device for use with an underwater pelletizer apparatus that extrudes and cuts a plurality of polymer strands into a plurality of particles, and the particles become A water and particle slurry is conveyed through the transfer line to a centrifugal dryer. The injection device includes a positionable nozzle assembly that adjusts an injection position to introduce a particle accelerator into the water and particle slurry, increasing the speed at which the particle slurry reaches and passes through the dryer, such that more particles are thermally maintain. The nozzle assembly is adjustable between a fully inserted position in which one of the nozzle tubes is positioned forwardly within the delivery line and a fully withdrawn position in which the fully extracted position is The nozzle tube is withdrawn from the delivery line to provide a completely unimpeded flow of the slurry through one of the lines. Preferably, the positionable nozzle assembly is configured such that the nozzle tube can be positioned not only at the fully inserted and fully withdrawn positions, but also at the fully forward insertion position and by an automatic control system. Fully extracted at various intermediate positions between the positions. BRIEF DESCRIPTION OF THE DRAWINGS The advantages and other objects and advantages of the present invention will be apparent from the following description of the appended claims. BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a cutaway and cross-sectional view of one prior art fixed nozzle configuration. Figure 2 is a schematic illustration of an underwater pelletizing system including an underwater pelletizer and a transfer line, and a positionable nozzle coupled to a centrifugal dryer. Figure 2a is an enlarged view showing the positionable nozzle of Figure 2. Figure 3 is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a, and the nozzle tube is in an extracted position. Figure 4 is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a with the nozzle tube in a forwardly inserted position. Figure 5 is a schematic top plan view of a portion of the positionable nozzle and delivery line of Figure 2a with the nozzle tube in the forward insertion position. Figure 6a is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a using an automatic control system, and the nozzle tube shown is in an extracted position. Figure 6b is a view of the nozzle tube housing taken along line 6b-6b of Figure 6a. Figure 6c is a cutaway and cross-sectional view of the embodiment of the automatic control system of Figure 6a with the nozzle tube shown in a forward insertion position. Figure 6d is a view of the nozzle tube housing taken along line 6d-6d of Figure 6d. 8 201103720 Figure 7 is a partial cutaway view of a rodless cylinder as shown in the figure.礤 Coupling in the Guard System Figure 8 is a diagram showing the circuit for the sixth. Control of the automatic control system of the figure. Figure 9b of the whistle and mouth tube of the flap is a diagram of the front opening of the present invention. &lt;Fig. 9c of the nozzle tube of the straight oriented profile flap is a 9th view of the present invention. Fig. 9e is a view of the present invention. The first embodiment of the present invention is the present invention. A diagram of the diagram of the nozzle tube. DETAILED DESCRIPTION OF THE INVENTION While the preferred embodiment of the invention has been described in detail, it is understood that other embodiments are possible. Therefore, the material of the present invention should not be limited by the details of the structure disclosed in the following description or the structure shown in the drawings. The invention is capable of other embodiments and of various embodiments. Again, in the preferred embodiment, specific terms will be relied upon for clarity. It should be understood that the specific terms include all technical equivalents that operate in a similar manner to achieve a similar purpose. Whenever possible, similar elements of the drawings are denoted by the same symbols. 201103720 The positionable nozzle assembly of the present invention assists in promoting crystallization of various polymeric materials and also facilitates drying of these and other materials while eliminating possible pauses in one of the blocks that have been encountered in previous designs. The speed of the particle slurry is increased by pressurized air or other gas injected into the particle delivery line. As a result, as the speed increases and the suction delivery liquid is away from the surface of the particles, the time at which the particles are dominated by the delivery liquid is reduced. Due to the increased speed, the particles have a lower residence time in the delivery liquid, allowing the particles to retain more internal heat for a longer period of time than they are subjected to the delivery liquid. In fact, increasing the heat within the retention contributes to the crystallization of the particles. This effect is enhanced by drawing the transport liquid away from the surface of the particles such that the heat loss to the transport liquid is reduced. In order to achieve the maximum throughput of the particles, the present invention allows the size and position of the nozzle to be adjusted. This is important for the speed at which the slurry is conveyed by the granulator to the dryer, which in turn impacts the system by pumping the efficiency of separating the particles from the transport liquid and increasing the amount of heat retained by the particles. Changing the shape and location of the nozzle can also be used to alter the flow pattern of the slurry through the transfer line, creating a more or less thirsty flow to achieve the specific needs associated with the material being processed. Referring now to Figure 2, the positionable nozzle of the present invention, generally indicated at 100, is assembled into a delivery line generally designated by the numeral 15, which is coupled to the granulation unit 10 and the drying unit 20 and any subsequent processing. . A melting and mixing device (not shown) is coupled to the granulator 10, which is coupled to the injection tube 12. The transport liquid is introduced into the cutting chamber of the granulator 10 through the injection tube 12, and it is mixed with the particles in the cutting chamber to form the slurry 10 201103720. The particle slurry is discharged into and through the sight glass 16 via the discharge tube 14 and then passed through the nozzle assembly 100 in the delivery line 15. A particulate accelerating material is injected and directed into the delivery line through the positionable nozzle assembly 100 to reduce the time during which the particles are dominated by the delivery liquid. Due to its inert nature and immediate availability, the particulate accelerating material is preferably air. However, other gases having inert properties such as nitrogen or the like may also be used. The accelerated particles and transport liquid enter through the transfer line 18 and pass through the dryer assembly 20, which is dewatered and dried in the dryer assembly 20. The details of the accelerated particles and the transported liquid are explained below. The melting and mixing device (not shown) may be any conventional device or combination thereof and may include, but is not limited to, a melting vessel, a single screw extruder, a twin screw extruder, a static mixer, a continuous mixer. , Closed mixer, etc. The granulator 10 may be a water ring granulator, an underwater granulator, etc., and is preferably an underwater granulator in which one of the ordinary knowledge is known in the art to which an extrusion die is embedded. . The transport liquid can be any liquid and preferably water, in addition to water, which can be used to granulate other liquids, including ethanol, water-ethanol mixtures, mineral oils, vegetable oils, glycol mixtures, and the like, in accordance with the present invention. Alternatively, water or other transport liquids may contain a plurality of additives including, but not limited to, flow agents, coatings, defoamers, cosolvents, and the like. As used herein, when referring to "liquid" or "water" in connection with the transport liquid, these references refer to any liquid suitable for use as a transport liquid, with or without additives, and not only water. The granulated and transported material of the present invention may be a polymer, a wax, and other extrudable materials which are granulated at 201103720. For example, such materials may include polyalkylenes, polyethers, polysulfoniums, polyamines, polyamidomines, polyfluorenes, polycarbonates, polyurethanes, fluoropolymers, ethylene. Polymers, biodegradable polymers, and copolymers thereof. The materials from which the further processed uranium is crystallized are particularly suitable for processing in accordance with the present invention, and preferably, the materials can be dried to a moisture content of less than 丨% by weight and crystallized to a level of at least 20%. More preferably, the materials can be dried to less than zero.  50% by weight of the moisture content and crystallized to a degree of at least 3 (10), the materials can be dried to a less than 〇.  A 25 wt% water knife is contained and crystallized to a level of at least 40%. Alternatively or optionally, the material to be granulated of the present invention may comprise any of the conventional fillers and fillers and/or other added bismuth combinations known to those of ordinary skill in the art. Such fillings include cellulose powders and/or fibers, biological materials including powders and fibers, and the like. The dryer in FIG. 2 may be a dewatering device, a filtering device, a #dynamic dewatering device, a fluidized bed, a tumble dryer, a centrifuge, a dryer, a dryer, at least one of - and preferably - Clean and dry by yourself. However, any separation means for separating the liquid from the particles in the liquid and particle slurry can be made in the present invention. Post-treatment may include, but is not limited to, cooling, crystallization, heating, re-drying, coining, solid state polymerization, packaging, etc., as known to those skilled in the art. An embodiment of the positionable nozzle assembly of the present invention is shown in detail in an enlarged view of Fig. 2a. As indicated by the dashed lines, the assembly includes a valve 104, 12 201103720, a line 106, a check valve 108, and a nozzle tube 110 that is partially inserted into the elbow 102 and is invisible. The nozzle tube 11 is inserted into the elbow 102 at the insertion point 112 and extends into the inner cavity of the elbow 102 to reach the joint portion 114 of the elbow 1〇2 and the outflow tube 116. The inlet gas line not shown is connected to the best. It is a valve 104 of a ball valve. The slurry of particles passing through the viewing aperture 16 (see Fig. 2) passes through the inflow tube 118 and enters and passes through the elbow 102 where it is before the passage of the outflow tube 116 and through the valve 12, with a pressurized gas, preferably air. Interaction. The inflow tube 118, the elbow 102, and the outflow tube 116 can be a one-piece tube that has been modified by bending to form the elbow and allows the nozzle tube 110 to be inserted. Preferably, however, the inflow tube 118, the elbow 102, and the outflow tube 116 are separate elements that are joined together by, for example, screwing or welding. The inflow tube 118 and the outflow tube 116 may have the same diameter as 1〇2, or they may have a different diameter than the elbow 102, in which case they preferably taper to the diameter of the elbow 1〇2. According to a preferred embodiment, the inflow tube 118 and the elbow 102 have the same diameter and the diameter of the outflow tube 116 is tapered by the junction 114 with the elbow 10 2 to the junction with the tube extension 1 &amp; The tube extension 122 extends to and is coupled to the valve 12A. The valve 12 is preferably connected to the delivery line 18 by screwing or by welding. Alternatively, the outflow tube 116 and the tube extension 122 can be detachably connected by a quick release connector 125, as shown in Figure 2a. The quick release connector 125 can be any suitable quick release assembly that facilitates easy access to the elbow and nozzle assembly for inspection, cleaning, maintenance, and repair as needed. Inflow f 118, elbow 1〇2 'outflow pipe 116 and nozzle pipe 11〇 are preferably made of 13 201103720 metal including tool steel, star steel, carbon steel, hardened steel, stainless steel, steel, etc. Made of wear-resistant industrial grade plastic. This component is preferably made of stainless steel and is preferably made of low carbon stainless steel. The check valve 108 is preferably placed between a receiving slot (not shown) and the manifold to prevent water and particles from flowing back into the receiving slot. The check valve 1 〇 8 allows pressurized air or other gas to flow through it 'but when air or other gas does not pass through it' the pressure from the transport liquid will cause the check valve 1 〇 8 to close, thus preventing the transport of liquids and particles countercurrent. Alternatively, it is preferable that an automatic valve having an electromechanical valve of an actuator can replace the one-way valve 1 〇 8. Valve 104 allows the operator to control the flow of pressurized air or other gases. Preferably, the valve 104 of a ball valve is connected to the nozzle tube 110, for example, by screwing, welding or screwing. The valve 104 is preferably connected to the line 1〇6, the check valve (10) and the nozzle tube 11G in sequence. Optionally or alternatively, an electromechanical valve can replace both valve 104 and check valve ι8. The valve 120 can more adjust the catch of the pressurized air or other gases. Valve 1〇4 can be closed to allow for conventional granulation processing without the need for pressurized gas injection. The wide and valve 120 are optional and can be used separately without the need for another. Preferably, the valve 1〇4 is used to adjust the pressurized gas and, more preferably, the intermediate (10) and the intermediate 12 are used in combination to maximize control and adjustment of the pressurized air or other gases. The positionable nozzle assembly is preferably positioned as shown in Fig. 2 and is not shown in detail in Figures 3, 4 and 5. Referring to Figure 2, a delivery tube (4) is used as an embodiment - the delivery catheter is preferably straight and air or other gas is injected into the elbow (4) 2. In the 仏, 3 and 4 diagrams, the axis of the best delivery tube (4) is in a straight line so that the effect of the injection on the granule is maximized and uniform. 14 201103720 Aspirate the liquid. The position of the equivalent structure of the elbow (4) 2 or the "gamma" configuration is preferably in the first elbow after the particle slurry leaves the granulator. However, the elbow 102 can be located in a selective elbow that is further away from the granulator 10, not shown, and before the dryer 20. Alternatively, a plurality of nozzle tubes can be inserted into at least the elbow to cooperatively facilitate delivery to and through at least one delivery line 18. Figure 3 shows the portion of the positionable nozzle assembly 100 in the fully extracted position relative to the elbow 1G2. As shown, the rear end of the nozzle tube 11 is surrounded by a shaft % 122 which guides the rear end as the nozzle tube slides within the cylindrical housing 128. The nozzle tube 11 and the collar 122 may be of a single body configuration, but preferably the nozzle tube 110 and the collar 122 are separate elements joined together by welding, for example. Preferably, the nozzle tube 110 and the collar 122 are welded to each end of the collar at the weldment 124 and the weld 126. The δ 喷嘴 nozzle tube 11 〇 and the collar 122 are variably positioned and freely slidable through the housing 128 ' the front end 130 of the housing 128 is threaded to a sealed transition collar 132 'the sealing transition collar 132 is engaged The portion 112 is connected to the elbow 1〇2. The front end of the nozzle tube 110 is slidably supported within the central bore 133 of the collar 132. A tension spring 134 is positioned within the housing 128 and circumferentially surrounding the nozzle tube 11 . At least one guide pin 136 is coupled to the collar 122, the guide pin 136 being aligned and positionable within at least one of the grooves 138 in the housing 128, as detailed in FIG. For larger delivery lines and nozzle assemblies, it is preferred to have at least two guide pins 136 that are respectively positionally aligned with the two grooves 138 in the housing 128 to provide greater adjustment. The groove 138 is linearly elongated along the length of the housing 128 and forms at least one of the recesses 14 如 as shown in Fig. 3, or 15 201103720. Most recesses as shown in Fig. 5, ο, mi. Please refer again Figure 3 'preferably a stretched elastomer 134 of a helical spring f placed on the front face of the collar 122 and on the rear face of the sealed transition collar 132. In Fig. 3, the tension spring 134 is at the nozzle The drawing position of the tube assembly is elongated. Figure 4 shows that the tension spring 134 is compressed in the foremost position of the positionable nozzle assembly ι 'where the nozzle tube UQ is completely inserted into the elbow 102 In the inner chamber, as shown, when fully inserted, the shaft is received in the housing 128 and the guide pin 136 is locked in the corner recess 14 , as shown more clearly. The guide pin 136 will be locked in the corner recess 141 when the nozzle tube is only partially inserted. The nozzle tube 11 is preferably sealingly positioned in the seal transition collar 132, see Figures 3 and 4. The sealing system has the usual knowledge in the technical field of the invention including the ankle ring, the "quadrilateral, the ring, the mechanical seal" Any of the known mechanical device, and is not limited thereto. Preferably, the seal uses at least one ankle ring 142 that is retained in a circumferential groove M4 of the sealed transition ring 132. The annulus 142 is tightly nested around the diameter of the nozzle tube 110 such that the nozzle tube 11 can be sealingly and slidably positioned through the at least one 0-ring 142. Preferably, at least two zero rings 142 are each sealingly positioned in the two circumferential grooves 144. Most preferably, the majority of the annulus 14 2 is sealingly positioned in the same plurality of circumferential grooves 丨 4 4 . Figure 5 shows a portion of the positionable nozzle assembly 100, wherein, as shown and described above in Figure 2a, the nozzle tube 11 is fully inserted into the lumen of the elbow 102 'substantially with the joint 114 flush. The collar 22 has been inserted into the housing 128 and the guide pin 136 has been moved through the groove 138 to be securely positioned in the corner recess 140. 16 201103720 The nozzle tube 110 can be positioned generally within the entire outer circumference of the elbow 102 in the interior of the sealed transition collar 丨 32 to at least the joint 114 or beyond the extent of the joint 114. Preferably, the fully withdrawn position is substantially flush with the exterior of the elbow 102 and the fully inserted position is generally at the joint 114. Movement of the nozzle tube 11 within the positionable nozzle assembly 1 can be accomplished by any suitable method, including manual or preferably using one or more automatic control systems, either alone or in various combinations. It includes pneumatic, electrical, electronic, hydraulic devices and methods, and optionally includes programmable logic control, PLC. Manual and automatic control capabilities can also be combined in the same nozzle assembly. Since it is determined by the position of the corner recess 140, the manual control must specifically arrange the positioning. However, if the move is automatic, there are a number of locations available. For example, the guide pins 136 and associated grooves 138 and corner recesses 14G and 141 used in Figure 5 will not be expected to be controlled using an automatic control system. A preferred embodiment of the collapsible nozzle of the present invention having an automatic control system for positioning the nozzle is shown in Figures 6a-6d. In this embodiment, the nozzle uses a user controlled pneumatic cylinder pneumatic Move to the desired location. Preferably, the pneumatic cylinder is a magnetically coupled rodless cylinder, generally indicated at 154, magnetically coupled to the carrier 16G, the carrier (10) being fixedly coupled to the nozzle tube 11 by a bracket or pin 162. Collar 122. As shown, in Figures 6a and 6c, the pin 162 is preferably coupled between the carrier 16 and the collar 122 and re-welded to the nozzle f 11Q. However, the shutoff 162 can be directly connected to the nozzle tube 110. The pin 162 can be coupled to the carrier 160 and the collar 122/nozzle tube 110 by any suitable connection method known to those skilled in the art, but is preferably bolted to the carrier 160 and the shaft. Ring 122. The pin 162 is passed through a slot 139 in the housing 129 through a housing 129 that surrounds the nozzle tube 110 and the collar 122, as shown in Figures 6b and 6d. A magnetically coupled rodless cylinder system that can be used in the present invention is manufactured by SmC Corporation of the United States under Series CY1B. As shown in Fig. 7, the rodless cylinder 154 includes a cylinder tube 170 having a piston 172 therein, and the piston 172 is provided with a first magnet 174. A second magnet 175 is supported in the body 176 of the carrier 160 and outside of the cylinder tube 170. A control circuit for moving the nozzle tube 110 using the pneumatic cylinder is shown in Fig. 8 and is generally indicated by reference numeral 190. The pneumatic cylinder 154 has a first air inlet 156 at its distal end 157 and a second air inlet 158 at its proximal end 159 relative to the nozzle tip 155. In order to move the nozzle tube 110 to the fully inserted forward position shown in Figures 6c and 6d, actuation - such as the push mechanism of the button 180, which will change the position of the air operated blocking valve 181 'to inject pressurized air Into the first air inlet 156. The air is also injected into a one-way read 184 at a second air inlet 158 of the air 159. The vsr opens the one-way check valve 184 and releases the air that has been applied to the proximal or front end of the pressure cylinder 154. Thereby, the piston 172 and the carrier 16 磁性 magnetically coupled thereto can be moved forward, and the pin 162 is moved in the slot 139 to the position shown in Fig. 6d. Conversely, in order to move the nozzle tube 110 from the insertion position to the pomelo-out position shown in Figures 6 and 6b, actuating the push-out mechanism as the button 182 changes the position of the air-operated blocking valve 181. To introduce pressurized air main radiation 18 201103720 into the second air inlet 158. The air is also injected into a one-way valve 185 at the first air inlet 156 of the distal end 157, which opens the one-way valve 丨 84 and releases pressurized air that has been in the distal or rear end of the pressure cylinder 154, thereby The piston 172 and the carrier 160 magnetically coupled thereto are moved forward, and the pin 162 is moved in the slot 139 to the position shown in the figure. Between the positioning conditions, the one-way valve 184 and the one-way valve 185 at the pneumatic cylinder 154 are controlled by the control circuit 190, and the air is not allowed to be released by the air inlet 156 or the air inlet 158. The holding position" check valves 184 and 185 also provide speed control to adjust how fast the nozzle tube can be moved. The pressurized air used to move the piston and carrier 160 may be supplied by various air sources, such as air tank compressors known to those of ordinary skill in the art. In the pneumatic embodiment, any number of t-positions between the fully inserted (the &amp;&amp; 6d) and fully extracted (the second and the same) positions can be used to (4) injected air The amount of pressurized air in the inlets 156, 158 is achieved. Or, similar to the movement and control of the nozzle tube can be through the use of - linear pressure red, - hydraulic cylinder and power unit, or with - ball screw or Aikem screw (a_% erb one of the feeding motor or stepping The motor, rather than through the magnetically coupled rodless cylinder 154 as is known in the art to which the invention pertains. However, the magnetically coupled rodless cylinder is preferred for the present invention. If desired, a preferred automatic control system for moving the nozzle can be combined with manual movement of the nozzle tube. Preferably, when the granulator is "started", the nozzle tube 11 can be Placed in a withdrawal position 'to avoid its presence becomes a barrier in the delivery line 15 19 201103720. Since it is advantageous to cause the nozzle tube 110 to be withdrawn, the unwanted mass can be at the beginning of the granulation process. The particle slurry is easily formed and allowed to use the full inner diameter of the delivery line U. The positionable nozzle assembly 100 is designed to allow an operator to inject pressurized air or other gas into the delivery line 18 while having a relative The delivery line 18 and the elbow 1〇2 adjust the position of the nozzle tube 11. The nozzle tube 11〇 can be withdrawn and inserted and still produces the desired suction depending on, but not limited to: flow rate, particle pair delivery The liquid ratio, the temperature of the transport liquid, the diameter of the elbow 1 〇 2 relative to the transport line 18, the distance between the elbow 1 〇 2 and the dryer 2 ' and the type of material being granulated are determined. It should be understood that, as shown in Figures 2a, 3 and 4, the outer diameter of the nozzle tube will be less than, for example, the inner diameter of the elbow 1 〇 2 at the joint portion 114. In this regard, the space in the inner chamber It should be large enough to permit the use of the combined maximum size of at least two particles having particles of the largest size for the particular granulation system, through the elbow 102 at the outside of the nozzle tube 11 and at the joint ι4 Between the insides. In other words, between the outer diameter of the nozzle tube and the inner diameter of the inner lumen of the inner tube, the area A is sufficient to at least two particles each having the largest size of the granulator, and can pass through the side by side. And will not block or block in the gap area. For example In other words, the embodiment of the present invention is to the elbow-G.  The 75-inch nominal nozzle tube 11〇 and a 2 inch time nominal spray money eight tube 1_ combination, -2 inch private elbow; I; 1G2, and one from the elbow officer 102 to the dryer 2〇1. 5 inches of delivery line 18. Another embodiment is a 0. 75-hour nominal nozzle tube 11Q and -3 · ο 公 公 公 肘 肘 肘 肘 肘 肘 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 且 公 公 公 公  〇 20 201103720 The combination of the English and the elbows. The orientation of the nozzle tube 110 relative to the joint 114 of the elbow 102 in Figure 2a may be concentrically centered about the centerline of the joint 114 or above the center, below the centerline to the right of the centerline Or left, or circumferentially surrounding the centerline at any angle, such that the angle between the centerline of the nozzle tube 110 and the centerline of the elbow 1〇2 can be made of 〇. To a maximum deflection angle. The maximum deflection angle is defined as the deflection angle of the outer portion of the nozzle tube 110 that contacts the joint 114 of the elbow 102 and/or the position of the positionable nozzle assembly 1 that extends into the downstream of the joint 114 of the elbow 102. Preferably, the nozzle tube 110 is concentrically positioned and collinear about the centerline of the joint portion 4 of the elbow 102. It should be understood here that the centerline of the joint 114 of the elbow 1 〇 2 is collinear with the centerline of the transfer line 18 downstream of the joint 114. Prior to nozzle tube 110, orifice 146 may be of any shape including circular, square, rectangular 'elliptical, polygonal, etc. and preferably circular. The diameter of the front aperture 146 may be greater than, less than, or equal to the diameter of the nozzle tube 11 and preferably equal to. When the diameter of the current orifice 146 is not equal to the diameter of the nozzle tube no, only the diameter of the portion of the nozzle tube 11 that is not in contact with the nearest annulus 142 is gradually increased or decreased, respectively; see Figures 3 and 4. However, the diameter of the distal aperture 146 cannot be greater than the inner diameter of the sealed transition collar 132. - the final taper 150 of the spray I s 11 显示 is shown in Fig. 9e, and similarly, the front aperture 146 may be a semicircle as shown in Fig. 9e or as in the _ Spiral to C shape. The nozzle officer 110 may be provided with a number of variations including, but not limited to, a conformal shape, at least a sigmoid inner surface, and many combinations thereof. Figure 9f shows a conical tapered nozzle tube 110 in which the taper is reduced toward the front aperture 146. The inside of the nozzle tube 110 may also or alternatively contain one or more fins 152 as shown in Figures 9a and 9b. The fins may be straight or inclined at 90[deg.] with respect to the circumferential edge of the nozzle tube 110, as shown in Figure 9a, or inclined at a smaller angle. Similarly, the fins may be curved or conformed to the circumference of the nozzle tube 110 as shown in Figure 9b. The fins may have a length ranging from less than to the length of the nozzle tube 110, and their height cannot exceed the radius of the nozzle tube 110. Preferably, the fins 152 are smaller than the length of the nozzle tube 110 and the height is smaller than the radius of the nozzle tube 110. When a plurality of fins are included, they can also be placed at any angle to each other and the configurations can be the same or different. The purpose of the fins is to assist in creating more eddy currents within the delivery line 18. In detail, the flow of the pumped slurry of particles can be varied from laminar to eddy. Without wishing to be bound by any theory, the injection of air or other gas into the slurry of particles will draw the transported liquid from the particles such that the transported liquid is transported along the transfer line 18 in a laminar flow while the vapor mist and particles are A more vortex flow propagates through the center of the transfer line 18 along the length of the transfer line 18. In some instances, a more thirsty flow may be required, in which case most of the fins may be advantageously added. In accordance with the present invention, pressurized air or other gas may flow continuously or intermittently through the nozzle tube 110, preferably continuously through the nozzle tube 110. As previously mentioned, this pressurized gas can be used to deliver the particles at a high velocity. This high velocity gas stream can be achieved using a pressurized gas using a standard valve 104 for adjusting the pressure through the transfer line 18 to at least 8 bar, resulting in at least 1 〇〇 cubic meter per 22 201103720 hours. Exemplary traffic. The line 18 is a standard tube diameter, preferably 1. 5 inches in diameter. For those of ordinary skill in the art to which the invention pertains, the flow rate and diameter will depend on the amount of treatment, the composition of the material comprising the filler, the temperature of the liquid to be delivered, the desired degree of crystallinity, the desired moisture content, and the particles and particulates. The size changes. The high velocity gas is in effective contact with the particulate water slurry, the water vapor is produced by suction, and the particles are dispersed throughout the slurry line to deliver the particles to the dryer 20 at high speed, preferably by the pelletizer 10. The transfer to the outlet of the dryer 20 is less than 1 second. The high velocity pump produces a mixture of 98-99% of the particles in a volume of the gaseous mixture in an air/gas mixture. By adjusting the insertion depth of the nozzle tube and adding surface variability within the nozzle, the flow characteristics of the slurry in the delivery line can be varied. Referring now to Figure 2, the angle formed between the vertical axis of the inflow tube 118 and the longitudinal axis of the delivery line 18 can be varied by the height of the granulator 10 relative to the inlet 22 to the dryer 20. It needs to be changed from 0° to equal to or greater than 90°, as shown in Figure 2. This height difference can be attributed to the physical positioning of the dryer 20 relative to the granulator 10 or can be the result of a difference in size between the dryer and the granulator, preferably from about 30 to about 60. °, and a better angle is about 45°. The enlarged elbow 24 entering the dryer inlet 22 facilitates the transfer of the high velocity suctioned particulate/water slurry from the delivery line 18 into the inlet 22 of the dryer 20 and reduces the particulate buildup in the dryer 20 The possibility in the middle. The outer surface of the nozzle tube 110 and the inner tube of the inflow tube 118, the elbow 102, the outflow tube 116 and the delivery line 18 can be coated by surface treatment to reduce grinding, abrasion, corrosion, abrasion and unnecessary adhesion. narrow. The surface treatment may be at least one of nitriding, carbonitriding, and sintering. Similarly, the foregoing surfaces may be subjected to high speed air and fuel modified heat treatment, electrolytic plating, electroless plating, flame spraying, thermal spraying, plasma treatment, electroless nickel dispersion treatment, and electrolytic plasma temperature, either singly or in combination. These treatments metallize the surface, preferably, the metal nitride is fixedly attached to the surface, and more preferably, the metal carbide and the metal carbonitride are fixedly attached to the surface, and more preferably, it will Diamond carbon is fixedly attached to the surface, and more preferably, diamond-like carbon in a wear resistant metal matrix is attached to the surface, and optimally, diamond-like carbon in a metal carbide matrix is attached to the surface surface. Other ceramic materials may also be used and are hereby incorporated by reference. In the case where the diameter of the portion to be coated that must pass through the seal is not properly modified, the thickness of the coating should not exceed about 0.  002 miles. Although the present invention has been described in its preferred embodiments, the spirit and scope of the equivalents of the present invention disclosed herein without departing from the scope of the invention In this case, many modifications, additions, and deletions can be made therein. BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a cutaway and cross-sectional view showing a prior art fixed nozzle configuration. Figure 2 is a schematic illustration of an underwater pelletizing system including an underwater pelletizer and a transfer line, and a positionable nozzle coupled to a centrifugal dryer. 24 201103720 Figure 2a is an enlarged view showing the positionable nozzle of Figure 2. Figure 3 is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a, and the nozzle tube is in an extracted position. Figure 4 is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a with the nozzle tube in a forwardly inserted position. Figure 5 is a schematic top plan view of a portion of the positionable nozzle and delivery line of Figure 2a with the nozzle tube in the forward insertion position. Figure 6a is a cutaway and cross-sectional view of a portion of the positionable nozzle and delivery line of Figure 2a using an automatic control system, and the nozzle tube shown is in an extracted position. Figure 6b is a view of the nozzle tube housing taken along line 6b-6b of Figure 6a. Figure 6c is a cutaway and cross-sectional view of the embodiment of the automatic control system of Figure 6a with the nozzle tube shown in a forward insertion position. Figure 6d is a view of the nozzle tube housing taken along line 6d-6d of Figure 6d. Figure 7 is a partial cutaway view of a magnetically coupled rodless cylinder for use in the automatic control system of Figures 6a-6d. Figure 8 is a diagram showing the control circuit for the automatic control system of Figures 6a-6d. Figure 9a is a view of the front orifice of the nozzle tube of the present invention containing vertically oriented straight fins. Figure 9b is a view of the front aperture of the nozzle tube of the present invention containing vertically oriented profile fins. 25 201103720 Figure 9c is a view of a semi-circular front aperture of a nozzle tube of the present invention. Figure 9d is a view of one of the nozzle tubes of the present invention from a spiral to a C-shaped orifice. Figure 9e is a view of one of the nozzle tubes of the present invention having a tapered end. Figure 9f is a view of a nozzle tube of the present invention having a tapered conical bore. [Main component symbol description] 10. . . Granulation device; granulator 112*·· insertion point 12...injection tube 114...joining portion 14...discharge tube 116...outflow tube 15. . . Conveying line 118... Inflow tube 16... Observation hole 120... Valve 18... Delivery line 122... Tube extension; Extraction ring 20. . . Drying device; dryer assembly; 124,126···welding dryer 125... quick release connector 22...inlet 128...housing 24...increase elbow 129...housing 100···positionable nozzle; positionable nozzle 130... front end assembly 132...sealing transition collar 102...elbow tube 133···central hole 104...valve 134...tension spring 106...line 136...guide pin 108···check valve 138...groove 110· · Nozzle tube 139 ... slot 26 201103720 140, 141... recess 170 · · · cylinder tube 142. . .  Ο ring 172... piston 144. . . Circumferential groove 174...first magnet 146. . . Front aperture 175...second magnet 150. . . Tapered cone 176... body 152... wing 180··· button 154. . . Pressure cylinder 181... Air operated barrier valve 155···Nozzle end 182··· button 156··. First air inlet 184, 185. . • Check valve 157... Distal 190... Control circuit 158···Second air inlet 200. . . Fixed nozzle assembly 159...proximal end 202. . . Elbow tube 160... carrier 210. . . Fixed nozzle tube 162...pin 214. . . Joint 27

Claims (1)

201103720 七、申請專利範圍: 1. 一種與一水下造粒機裝置一起使用之注射設備,該水下 造粒機裝置擠壓且切割多數聚合物條成為多數顆粒,該 裝置包括將液體導入該造粒機中之管路及一將一液體 與顆粒漿液輸送至該造粒機外且輸送至一用以乾燥該 等顆粒之離心乾燥機的輸送通路,該注射設備包含: 一可定位喷嘴總成,在一殼體内具有一可移動喷嘴 管,用以將一顆粒加速物導入該液體與顆粒漿液以增加 該顆粒漿液到達及通過該乾燥機之速度,使得更多該等 顆粒之内熱被保持,該喷嘴管可在一完全插入位置及一 完全抽出位置之間移動。 2. 如申請專利範圍第1項之注射設備,其中該水下造粒機 裝置之輸送通路包括一與該造粒機耦合之流出管,該漿 液通過該流出管到達一輸送管路,且該輸送管路被一成 角度肘管接合部接合,該可移動喷嘴管可延伸入該接合 部以在該喷嘴總成下游與該輸送管路之一軸成一直線。 3. 如申請專利範圍第2項之注射設備,其中該可定位喷嘴 總成更包含一固定於該成角度接合部之密封過渡軸 環、一連接於該密封過渡軸環之殼體、及一固定於該喷 嘴管且被收納在該殼體内之滑動軸環,該滑動軸環及該 噴嘴管可在該殼體内自由地移動。 4. 如申請專利範圍第3項之注射設備,其中該殼體包括一 拉伸彈簀,該拉伸彈簧沿圓周緣定位環繞該喷嘴管且安 置在該滑動軸環之一前面及該密封過渡軸環之一後面 28 201103720 上,當該可移動喷嘴管相對於該成角度接合部前進時, 該拉伸彈簧被壓縮。 ‘ 5. 如申請專利範圍第4項之注射設備,其中該喷嘴管可在 該完全插入與完全抽出位置之間手動地調整且該殼體 具有平行於該可移動噴嘴管延伸之至少一溝槽,該溝槽 具有至少一成角度凹部,該滑動轴環具有一與其連接之 導銷,該導銷可定位在該溝槽内且當被收納在成角度凹 部中時,以與一特殊插入位置相關之一設定程度之拉伸 彈簧壓力鎖定該喷嘴總成。 6. 如申請專利範圍第5項之注射設備,其中該顆粒加速物 是加壓氣體且該喷嘴總成更包括至少一構形成可控制 該加壓氣體之流動的閥。 7. 如申請專利範圍第1項之注射設備,其中該可定位喷嘴 總成包括一自動控制系統,以自動地實行該喷嘴管在該 完全插入與完全抽出位置之間的移動,且將該喷嘴管定 位在其間之任何位置。 8. 如申請專利範圍第7項之注射設備,其中該自動控制系 統包括一磁搞合無桿氣壓缸、一線性氣壓缸、一液壓缸 與動力單元、或與一滾珠螺桿或愛克姆螺桿(acme screw) —起之一祠服馬達或一步進馬達。 9. 如申請專利範圍第7項之注射設備,其中該自動控制系 統包括一氣壓缸,該氣壓缸安裝至該殼體且構形成可回 應加壓空氣注射入該壓缸,在該壓缸之第一與第二端之 間移動該喷嘴管。 29 201103720 10. 如申請專利範圍第9項之注射設備,其中該可定位喷嘴 總成更包括一固定於該喷嘴管且被收納在該殼體内之 滑動轴環、及一與該氣壓缸可移動地結合之載架,該氣 壓缸包含一活塞,該活塞與該載架磁性地結合,使得該 活塞藉該加壓空氣之注射的移動亦使該載架及該喷嘴 管移動。 11. 如申請專利範圍第10項之注射設備,其中該載架藉一銷 與該滑動軸環耦合,該銷通過在該殼體中之一槽孔。 12. —種用以加工聚合物及其他可擠壓材料成為多數顆粒 之裝置,包含: 一造粒機,用以在一液體中將多數擠壓條切割成多 數顆粒; 輸送管路,用以將一液體與顆粒漿液輸送至該造粒 機外且輸送至一分離設備,以分離顆粒與液體;及 一注射器,用以將一顆粒加速物導入在該輸送管路 内之該液體與顆粒漿液中,以增加該等顆粒通過該加工 裝置之速度,使得該等顆粒保持一高度之内熱,該注射 器包括一在一殼體内之可定位喷嘴管,該喷嘴管可插入 該輸送管路内且可在相對該管路之一完全插入位置與 一完全抽出位置之間移動。 13. 如申請專利範圍第12項之裝置,其中該喷嘴管是一可調 整喷嘴總成之一部份,該可調整喷嘴總成包括一固定於 該輸送管路之密封過渡軸環、一連接於該密封過渡軸環 之殼體、及一被收納在該殼體内之滑動軸環,該滑動軸 30 201103720 環及該噴嘴管可在該殼體内自由地移動。 14·如申請專利範圍第13項之裝置,其中該殼體包括一拉伸 彈黃’該拉伸彈簧沿圓周緣定位環繞該噴嘴管且安置在 。亥滑動轴環之—前面及該密封過渡轴環之一後面上,當 °亥喷嘴總成朝該完全插入位置前進時,該拉伸彈簧被壓 縮。 15·如申請專利範圍第14項之裝置,其中該喷嘴管可手動地 調整且該殼體具有平行於該喷嘴管延伸之至少一溝 槽’該溝槽具有至少__成角度凹部,該滑動軸環具有一 -…、連接之導銷,該導銷可定位在該溝槽内且當被收納 在成角度凹部切,以與—特殊插人位置相關之一設定 程度之拉伸彈簧壓力鎖定該噴嘴總成。 申二專如ID第12項之裝置,其中該可定位噴嘴總成 :括-自動控制系統,該自動控制系統構形成可自動地 ^丁該噴嘴管在該完全插人與完全抽出位置之間的移 動,且將該噴嘴管再定位在其間之任何位置。 17·Γ=範圍第16項之農置,其中該自動控制系統包 二_:無桿氣歷缸、1性氣壓缸、-液厂堅缸與動 :兀:、與1珠螺桿我愛克姆螺桿—起之一伺服 達或一步進馬達。 18:申請:!範圍第16項之裝置,其中該自動控制系統包 :構:該氣壓缸在其第一第二端處安裝至該殼體 第=應加壓空&amp;射入該壓紅,在該等第一與 第一壓缸缟之間移動該嘴嘴管。 31 201103720 19. 如申請專利範圍第18項之裝置,其中該可定位喷嘴總成 更包括一固定於該喷嘴管且被收纳在該殼體内之滑動 軸環、及一與該氣壓缸可移動地結合之載架,該氣壓缸 包含一活塞,該活塞與該載架磁性地結合,使得該活塞 藉該加壓空氣之注射的移動亦使該載架及該噴嘴管移 動。 20. 如申請專利範圍第19項之裝置,其中該載架藉一銷與該 滑動軸環耦合,該銷通過在該殼體中之一槽孔。 21. 如申請專利範圍第1項之注射設備,其中該喷嘴管之一 幾何構形是圓形、正方形、矩形、橢圓形、多邊形、半 圓形、螺旋形或C形。 22. 如申請專利範圍第21項之注射設備,其中該喷嘴管在一 流出端處呈錐形。 23. 如申請專利範圍第21項之注射設備,其中該喷嘴管具有 一内表面,該内表面呈螺旋形、順形、膛線形、錐形或 其某種組合。 24. —種用以加工可擠壓材料成為多數顆粒之方法,其包 含: 將一可擠壓材料擠壓成多數條; 在一液體中將該等擠壓條切割成多數顆粒; 輸送該等顆粒及該液體作為一通過一輸送導管之 液體與顆粒漿液; 調整一可定位加壓氣體噴嘴總成至在該輸送導管 内之一所需程度之插入; 32 201103720 使用該氣體噴嘴總成將一加壓氣體以一高速注射 入該輸送導管,以在該漿液移動通過該輸送導管時,促 使該液體與該等顆粒分離;及 分離該等顆粒與該液體。 2 5 ·如申請專利範圍第2 4項之方法,其中該氣體喷嘴總成包 括一嵌合在一滑動軸環内之氣體喷嘴,該滑動轴環上具 有一導銷,該調整之步驟係手動地實行且該注射之步驟 更包括將該氣體喷嘴滑入一安裝在該輸送管路上之殼 體,該殼體具有至少一溝槽及一成角度凹部,以在該喷 嘴在該所需程度之插入時收納該導銷於一固定位置。 26. 如申請專利範圍第24項之方法,其中該調整之步驟包括 在一自動控制系統之控制下,自動地移動該氣體喷嘴總 成之一氣體喷嘴至該所需程度之插入。 27. 如申請專利範圍第26項之方法,其中該自動地移動一氣 體噴嘴至該所需程度之插入的步驟係使用一磁耦合無 桿氣壓缸、一線性氣壓缸、一液壓缸與動力單元、或與 一滾珠螺桿或愛克姆螺桿一起之一伺服馬達或一步進 馬達來實行。 2 8.如申請專利範圍第2 4項之方法,其中該氣體噴嘴總成包 括一具有一氣壓缸之自動控制系統,該氣壓缸構形成可 自動地實行該喷嘴管在完全插入與完全抽出位置之間 的移動,該方法包括將加壓空氣注射入該壓缸之一端中 以將該喷嘴管移動至該完全插入位置之步驟,及將加壓 空氣注射入該壓缸之一相對端中以將該喷嘴管移動至 33 201103720 該完全抽出位置之步驟。 29. 如申請專利範圍第28項之方法,更包含將該喷嘴管固定 地耦合至一載架之步驟及將該載架磁性地耦合至一在 該壓缸内之活塞之步驟,使得該等注射加壓空氣之步驟 移動該活塞且,透過磁性耦合,亦移動該載架及喷嘴管。 30. 如申請專利範圍第24項之方法,其中該可擠壓材料是一 具有足以結晶之熱的可結晶聚合材料,且該注射步驟使 該聚合材料保持足以開始自結晶到至少20%之程度的 熱。 31. 如申請專利範圍第24項之方法,其中該注射步驟促進該 等顆粒與該液體之分離及/或在該分離該等顆粒與該液 體之步驟時之顆粒的乾燥。 34201103720 VII. Patent application scope: 1. An injection device for use with an underwater granulator device, which squeezes and cuts a plurality of polymer strips into a plurality of particles, the device comprising introducing liquid into the a conduit in the granulator and a delivery of a liquid and particulate slurry to the granulator and to a centrifugal dryer for drying the granules, the injection device comprising: a total positionable nozzle Forming a movable nozzle tube in a housing for introducing a particle accelerating material into the liquid and particle slurry to increase the speed at which the particle slurry reaches and passes through the dryer, so that more internal heat of the particles Being held, the nozzle tube is movable between a fully inserted position and a fully withdrawn position. 2. The injection device of claim 1, wherein the delivery path of the underwater granulator device comprises an outflow tube coupled to the granulator, the slurry passing through the outflow tube to a delivery line, and The delivery line is engaged by an angled elbow joint that extends into the joint to be in line with one of the delivery lines downstream of the nozzle assembly. 3. The injection device of claim 2, wherein the positionable nozzle assembly further comprises a sealed transition collar fixed to the angled joint, a housing coupled to the sealed transition collar, and a housing A sliding collar fixed to the nozzle tube and housed in the housing, the sliding collar and the nozzle tube are freely movable within the housing. 4. The injection device of claim 3, wherein the housing comprises a tensile magazine positioned around the circumference of the nozzle tube and disposed in front of one of the sliding collars and the sealing transition One of the collars is behind 28 201103720, the tension spring is compressed as the movable nozzle tube advances relative to the angled joint. 5. The injection device of claim 4, wherein the nozzle tube is manually adjustable between the fully inserted and fully withdrawn positions and the housing has at least one groove extending parallel to the movable nozzle tube The groove has at least one angled recess having a guide pin coupled thereto, the guide pin being positionable within the groove and when received in the angled recess for a particular insertion position One of the associated degree of tension spring pressure locks the nozzle assembly. 6. The injection device of claim 5, wherein the particulate accelerating material is a pressurized gas and the nozzle assembly further comprises at least one valve configured to control the flow of the pressurized gas. 7. The injection device of claim 1, wherein the positionable nozzle assembly includes an automatic control system to automatically effect movement of the nozzle tube between the fully inserted and fully withdrawn positions, and the nozzle is The tube is positioned anywhere in between. 8. The injection device of claim 7, wherein the automatic control system comprises a magnetically engaged rodless pneumatic cylinder, a linear pneumatic cylinder, a hydraulic cylinder and a power unit, or a ball screw or an Aike screw (acme screw) — A motor or a stepper motor. 9. The injection device of claim 7, wherein the automatic control system comprises a pneumatic cylinder mounted to the housing and configured to be injected into the pressure cylinder in response to pressurized air, wherein the pressure cylinder is The nozzle tube is moved between the first and second ends. The apparatus of claim 9, wherein the positionable nozzle assembly further comprises a sliding collar fixed to the nozzle tube and housed in the housing, and a pneumatic cylinder The mobilely coupled carrier includes a piston that is magnetically coupled to the carrier such that movement of the piston by the injection of pressurized air also moves the carrier and the nozzle tube. 11. The injection device of claim 10, wherein the carrier is coupled to the sliding collar by a pin that passes through a slot in the housing. 12. A device for processing polymers and other extrudable materials into a plurality of particles, comprising: a granulator for cutting a plurality of extruded strips into a plurality of particles in a liquid; a transfer line for Delivering a liquid and particle slurry to the granulator and to a separation device for separating particles and liquid; and a syringe for introducing a particle accelerator into the liquid and particle slurry in the delivery line In order to increase the speed at which the particles pass through the processing device such that the particles maintain a high degree of internal heat, the syringe includes a positionable nozzle tube in a housing, the nozzle tube being insertable into the delivery line And it is movable between a fully inserted position relative to the one of the lines and a fully withdrawn position. 13. The device of claim 12, wherein the nozzle tube is a portion of an adjustable nozzle assembly, the adjustable nozzle assembly including a sealed transition collar, a connection secured to the delivery line The housing of the sealed transition collar and a sliding collar housed in the housing, the sliding shaft 30201103720 ring and the nozzle tube are freely movable within the housing. 14. The device of claim 13 wherein the housing comprises a tensile spring. The tension spring is positioned around the nozzle tube along a circumferential edge and disposed therein. On the rear side of the sliding collar of the sea and one of the sealing transition collars, the tension spring is compressed as the nozzle assembly advances toward the fully inserted position. 15. The device of claim 14, wherein the nozzle tube is manually adjustable and the housing has at least one groove extending parallel to the nozzle tube. The groove has at least an angled recess, the sliding The collar has a -..., connected guide pin that can be positioned within the groove and that is locked in an angled recess to accommodate a degree of tension spring compression associated with a particular insertion position The nozzle assembly. The second device is the device of ID No. 12, wherein the positionable nozzle assembly comprises: an automatic control system, the automatic control system is configured to automatically control the nozzle tube between the fully inserted and fully extracted positions Move and reposition the nozzle tube anywhere in between. 17·Γ=Scope No. 16 of the farm, in which the automatic control system package two _: no rod gas calendar cylinder, 1 pneumatic cylinder, - liquid factory hard cylinder and movement: 兀:, with 1 bead screw I love The screw is a servo-up or a stepper motor. 18: The device of claim 16, wherein the automatic control system package: the pneumatic cylinder is mounted to the housing at the first second end thereof; the pressure should be pressurized &amp; injection into the pressure red The nozzle tube is moved between the first and first cylinders. The apparatus of claim 18, wherein the positionable nozzle assembly further comprises a sliding collar fixed to the nozzle tube and housed in the housing, and a movable cylinder movable In combination with the carrier, the pneumatic cylinder includes a piston that is magnetically coupled to the carrier such that movement of the piston by the injection of pressurized air also moves the carrier and the nozzle tube. 20. The device of claim 19, wherein the carrier is coupled to the sliding collar by a pin that passes through a slot in the housing. 21. The injection device of claim 1, wherein one of the nozzle tubes is geometric in shape of a circle, a square, a rectangle, an ellipse, a polygon, a semicircle, a spiral or a C. 22. The injection device of claim 21, wherein the nozzle tube is tapered at an outflow end. 23. The injection device of claim 21, wherein the nozzle tube has an inner surface that is helical, conformal, meandered, tapered, or some combination thereof. 24. A method for processing an extrudable material into a plurality of particles, comprising: extruding an extrudable material into a plurality of strips; cutting the extruded strip into a plurality of particles in a liquid; conveying the same The particles and the liquid act as a liquid and particle slurry through a delivery conduit; an insertion of a positionable pressurized gas nozzle assembly to a desired extent within the delivery conduit; 32 201103720 using the gas nozzle assembly Pressurized gas is injected into the delivery conduit at a high velocity to cause separation of the liquid from the particles as the slurry moves through the delivery conduit; and to separate the particles from the liquid. The method of claim 24, wherein the gas nozzle assembly comprises a gas nozzle fitted in a sliding collar, the sliding collar having a guide pin, the step of adjusting is manual And the step of injecting further comprises sliding the gas nozzle into a housing mounted on the delivery line, the housing having at least one groove and an angled recess for the desired degree of the nozzle The guide pin is received at a fixed position when inserted. 26. The method of claim 24, wherein the step of adjusting comprises automatically moving a gas nozzle of the gas nozzle assembly to the desired degree of insertion under the control of an automatic control system. 27. The method of claim 26, wherein the step of automatically moving a gas nozzle to the desired degree of insertion uses a magnetically coupled rodless pneumatic cylinder, a linear pneumatic cylinder, a hydraulic cylinder, and a power unit Or a servo motor or a stepper motor together with a ball screw or an Aikem screw. 2. The method of claim 24, wherein the gas nozzle assembly comprises an automatic control system having a pneumatic cylinder configured to automatically perform the nozzle tube in a fully inserted and fully withdrawn position Between the movements, the method includes the steps of injecting pressurized air into one end of the cylinder to move the nozzle tube to the fully inserted position, and injecting pressurized air into the opposite end of the cylinder Move the nozzle tube to the step of 33 201103720, the fully extracted position. 29. The method of claim 28, further comprising the step of fixedly coupling the nozzle tube to a carrier and magnetically coupling the carrier to a piston within the cylinder, such that The step of injecting pressurized air moves the piston and, through magnetic coupling, also moves the carrier and the nozzle tube. 30. The method of claim 24, wherein the extrudable material is a crystallizable polymeric material having sufficient heat to crystallize, and the injecting step maintains the polymeric material sufficient to initiate self-crystallization to at least 20%. hot. 31. The method of claim 24, wherein the injecting step facilitates separation of the particles from the liquid and/or drying of the particles in the step of separating the particles from the liquid. 34
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