TW200736298A - Process for increasing the molecular weight of a polyamide - Google Patents

Process for increasing the molecular weight of a polyamide

Info

Publication number
TW200736298A
TW200736298A TW096104450A TW96104450A TW200736298A TW 200736298 A TW200736298 A TW 200736298A TW 096104450 A TW096104450 A TW 096104450A TW 96104450 A TW96104450 A TW 96104450A TW 200736298 A TW200736298 A TW 200736298A
Authority
TW
Taiwan
Prior art keywords
polyamide
increasing
molecular weight
countercurrent
contacted
Prior art date
Application number
TW096104450A
Other languages
Chinese (zh)
Other versions
TWI409288B (en
Inventor
Cornelia Emilie Maria Bronsaer
Mathijs Hubert Gertrudes Maassen
Geenen Albert Arnold Van
Renier Henricus Maria Kierkels
Original Assignee
Dsm Ip Assets Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=36648817&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=TW200736298(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv
Publication of TW200736298A publication Critical patent/TW200736298A/en
Application granted granted Critical
Publication of TWI409288B publication Critical patent/TWI409288B/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams
    • C08G69/16—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/46—Post-polymerisation treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyamides (AREA)
  • Artificial Filaments (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

Process for increasing the molecular weight of a polyamide comprising a first step, wherein the polyamide is contacted in countercurrent with a first stream comprising 15 to 100 wr% H2O and 85 to 0 wt% N2 at a temperature between 90 and 180 DEG C and for a time between 5 and 10 hours and a second step, wherein the polyamide obtained in the first step is contacted in countercurrent with a second stream comprising 90 to 100 wt% N2 and 10 to 0wt% H2O at a temperature between 130 and 200 DEG C and for a time between 10 and 30 hours.
TW096104450A 2006-02-08 2007-02-07 Process for increasing the molecular weight of a polyamide TWI409288B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP06075258 2006-02-08

Publications (2)

Publication Number Publication Date
TW200736298A true TW200736298A (en) 2007-10-01
TWI409288B TWI409288B (en) 2013-09-21

Family

ID=36648817

Family Applications (1)

Application Number Title Priority Date Filing Date
TW096104450A TWI409288B (en) 2006-02-08 2007-02-07 Process for increasing the molecular weight of a polyamide

Country Status (11)

Country Link
US (1) US20090306331A1 (en)
EP (1) EP1981931B1 (en)
CN (1) CN101379116B (en)
AT (1) ATE449807T1 (en)
BR (1) BRPI0707534A2 (en)
DE (1) DE602007003444D1 (en)
EA (1) EA013823B1 (en)
ES (1) ES2335940T3 (en)
PL (1) PL1981931T3 (en)
TW (1) TWI409288B (en)
WO (1) WO2007090602A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2376845T3 (en) * 2008-06-20 2012-03-20 Basf Se Continuous procedure for multi-stage drying and subsequent condensation of polyamide granules
US20120065339A1 (en) * 2010-09-10 2012-03-15 Basf Se Process for producing polyamide that is stable during processing
EP2671902B1 (en) * 2012-06-05 2018-01-03 Polymetrix AG Polyamide conditioning
US20140350213A1 (en) * 2012-07-06 2014-11-27 Basf Se Purification of polyamide particles

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3015651A (en) * 1956-09-28 1962-01-02 Du Pont Increasing viscosity of polycaprolactam by removing extractables with solvents and further solid phase polymerizing the polymer
US3374207A (en) * 1964-11-12 1968-03-19 Inventa Ag Continuous process for the extraction of monomers and oligomers from highly polymerized caprolactam granules
US3386967A (en) * 1965-01-19 1968-06-04 Allied Chem Polycaproamide having excess number of carboxyl end groups over amino end groups
DE3710803A1 (en) * 1987-03-31 1988-10-20 Basf Ag METHOD FOR REMOVING CAPROLACTAM AND ITS OLIGOMERS FROM SUCH CONTAINING POLYAMIDE GRANULES
US4891420A (en) * 1988-06-30 1990-01-02 Basf Aktiengesellschaft Continuous process for the hydrolytic production of polycaprolactam by tempering unextracted granular polymer material with moist inert gas
DE3923061C1 (en) * 1989-07-13 1990-07-26 Basf Ag, 6700 Ludwigshafen, De
DE4421704A1 (en) * 1994-06-21 1996-01-04 Bayer Ag Process for the production of high molecular weight polyamide 6
DE19752183A1 (en) * 1997-11-25 1999-05-27 Basf Ag Continuous extraction of polyamide particle
DE10047657B4 (en) * 2000-09-26 2005-02-10 Basf Ag Process for the preparation of polycaprolactam, a polycaprolactam and its use
EP1331236A1 (en) * 2002-01-25 2003-07-30 Dsm N.V. Solid-state post-condensation process for increasing the molecular weight of a polyamide

Also Published As

Publication number Publication date
DE602007003444D1 (en) 2010-01-07
CN101379116A (en) 2009-03-04
EA200801808A1 (en) 2008-12-30
TWI409288B (en) 2013-09-21
ATE449807T1 (en) 2009-12-15
EA013823B1 (en) 2010-08-30
EP1981931A1 (en) 2008-10-22
PL1981931T3 (en) 2010-04-30
BRPI0707534A2 (en) 2011-05-03
EP1981931B1 (en) 2009-11-25
CN101379116B (en) 2011-05-25
ES2335940T3 (en) 2010-04-06
WO2007090602A1 (en) 2007-08-16
US20090306331A1 (en) 2009-12-10

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Legal Events

Date Code Title Description
MM4A Annulment or lapse of patent due to non-payment of fees