TR201706114A2 - ANERIPERSPIRANT FORMULATION IN AEROSOL STRUCTURE - Google Patents
ANERIPERSPIRANT FORMULATION IN AEROSOL STRUCTURE Download PDFInfo
- Publication number
- TR201706114A2 TR201706114A2 TR2017/06114A TR201706114A TR201706114A2 TR 201706114 A2 TR201706114 A2 TR 201706114A2 TR 2017/06114 A TR2017/06114 A TR 2017/06114A TR 201706114 A TR201706114 A TR 201706114A TR 201706114 A2 TR201706114 A2 TR 201706114A2
- Authority
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- Turkey
- Prior art keywords
- antiperspirant
- aluminum
- aerosol
- formulation
- volatile
- Prior art date
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- 239000000443 aerosol Substances 0.000 title claims abstract description 22
- 239000000203 mixture Substances 0.000 title claims abstract description 22
- 238000009472 formulation Methods 0.000 title claims abstract description 15
- 230000001166 anti-perspirative effect Effects 0.000 claims abstract description 37
- 239000003213 antiperspirant Substances 0.000 claims abstract description 37
- 150000002148 esters Chemical class 0.000 claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 230000002087 whitening effect Effects 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 10
- XTJFFFGAUHQWII-UHFFFAOYSA-N Dibutyl adipate Chemical compound CCCCOC(=O)CCCCC(=O)OCCCC XTJFFFGAUHQWII-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940100539 dibutyl adipate Drugs 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 7
- 239000003974 emollient agent Substances 0.000 claims abstract description 6
- 230000002401 inhibitory effect Effects 0.000 claims abstract description 6
- 230000008569 process Effects 0.000 claims abstract description 6
- 230000035900 sweating Effects 0.000 claims abstract description 6
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 5
- 239000000375 suspending agent Substances 0.000 claims abstract description 5
- 239000004753 textile Substances 0.000 claims abstract description 5
- 208000035985 Body Odor Diseases 0.000 claims abstract description 3
- 239000004927 clay Substances 0.000 claims description 7
- LVYZJEPLMYTTGH-UHFFFAOYSA-H dialuminum chloride pentahydroxide dihydrate Chemical compound [Cl-].[Al+3].[OH-].[OH-].[Al+3].[OH-].[OH-].[OH-].O.O LVYZJEPLMYTTGH-UHFFFAOYSA-H 0.000 claims description 6
- 229920001296 polysiloxane Polymers 0.000 claims description 6
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 5
- YCLAMANSVUJYPT-UHFFFAOYSA-L aluminum chloride hydroxide hydrate Chemical compound O.[OH-].[Al+3].[Cl-] YCLAMANSVUJYPT-UHFFFAOYSA-L 0.000 claims description 5
- 229940053431 aluminum sesquichlorohydrate Drugs 0.000 claims description 5
- 229940008099 dimethicone Drugs 0.000 claims description 5
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 5
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 5
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims description 5
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 5
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 claims description 4
- DLAHAXOYRFRPFQ-UHFFFAOYSA-N dodecyl benzoate Chemical compound CCCCCCCCCCCCOC(=O)C1=CC=CC=C1 DLAHAXOYRFRPFQ-UHFFFAOYSA-N 0.000 claims description 4
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 claims description 4
- 229910000271 hectorite Inorganic materials 0.000 claims description 4
- 239000002304 perfume Substances 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 description 8
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 6
- 229910052782 aluminium Inorganic materials 0.000 description 6
- 229920001223 polyethylene glycol Polymers 0.000 description 6
- HAMGNFFXQJOFRZ-UHFFFAOYSA-L aluminum;zirconium(4+);chloride;hydroxide;hydrate Chemical compound O.[OH-].[Al+3].[Cl-].[Zr+4] HAMGNFFXQJOFRZ-UHFFFAOYSA-L 0.000 description 5
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 description 4
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 4
- 235000019645 odor Nutrition 0.000 description 4
- 239000002781 deodorant agent Substances 0.000 description 3
- 239000003380 propellant Substances 0.000 description 3
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- ZGUQGPFMMTZGBQ-UHFFFAOYSA-N [Al].[Al].[Zr] Chemical compound [Al].[Al].[Zr] ZGUQGPFMMTZGBQ-UHFFFAOYSA-N 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- YXZZLAMCXFHTTE-UHFFFAOYSA-N aluminum;propane-1,2-diol;trihypochlorite;hydrate Chemical compound O.[Al+3].Cl[O-].Cl[O-].Cl[O-].CC(O)CO YXZZLAMCXFHTTE-UHFFFAOYSA-N 0.000 description 2
- 230000036773 apocrine secretion Effects 0.000 description 2
- 150000005690 diesters Chemical group 0.000 description 2
- 210000000804 eccrine gland Anatomy 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 210000000106 sweat gland Anatomy 0.000 description 2
- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 description 1
- ABEXEQSGABRUHS-UHFFFAOYSA-N 16-methylheptadecyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCCCC(C)C ABEXEQSGABRUHS-UHFFFAOYSA-N 0.000 description 1
- RWKSBJVOQGKDFZ-UHFFFAOYSA-N 16-methylheptadecyl 2-hydroxypropanoate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)C(C)O RWKSBJVOQGKDFZ-UHFFFAOYSA-N 0.000 description 1
- SAMYFBLRCRWESN-UHFFFAOYSA-N 16-methylheptadecyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCCCCCCCCCCCCCCCC(C)C SAMYFBLRCRWESN-UHFFFAOYSA-N 0.000 description 1
- FKOKUHFZNIUSLW-UHFFFAOYSA-N 2-Hydroxypropyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(C)O FKOKUHFZNIUSLW-UHFFFAOYSA-N 0.000 description 1
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 description 1
- LNRUVXAPKCPQGX-UHFFFAOYSA-N 2-octyldodecyl benzoate Chemical compound CCCCCCCCCCC(CCCCCCCC)COC(=O)C1=CC=CC=C1 LNRUVXAPKCPQGX-UHFFFAOYSA-N 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical group CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 1
- 101000583175 Homo sapiens Prolactin-inducible protein Proteins 0.000 description 1
- 229920002884 Laureth 4 Polymers 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 239000004264 Petrolatum Substances 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 102100030350 Prolactin-inducible protein Human genes 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- ILXDAXZQNSOSAE-UHFFFAOYSA-N [AlH3].[Cl] Chemical compound [AlH3].[Cl] ILXDAXZQNSOSAE-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- -1 aluminum zirconium chlorohydrate Chemical compound 0.000 description 1
- 229940048496 aluminum zirconium pentachlorohydrex gly Drugs 0.000 description 1
- WYANSMZYIOPJFV-UHFFFAOYSA-L aluminum;2-aminoacetic acid;zirconium(4+);chloride;hydroxide;hydrate Chemical compound O.[OH-].[Al+3].[Cl-].[Zr+4].NCC(O)=O WYANSMZYIOPJFV-UHFFFAOYSA-L 0.000 description 1
- SJXYSRSHDPPYIU-UHFFFAOYSA-L aluminum;propane-1,2-diol;chloride;hydroxide;hydrate Chemical compound O.[OH-].[Al+3].[Cl-].CC(O)CO SJXYSRSHDPPYIU-UHFFFAOYSA-L 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 description 1
- 150000001558 benzoic acid derivatives Chemical class 0.000 description 1
- QNRYOQRUGRVBRL-UHFFFAOYSA-N benzyl dodecanoate Chemical compound CCCCCCCCCCCC(=O)OCC1=CC=CC=C1 QNRYOQRUGRVBRL-UHFFFAOYSA-N 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- XILPPDQAWPSZIL-UHFFFAOYSA-H dialuminum;dichloride;tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Al+3].[Al+3].[Cl-].[Cl-] XILPPDQAWPSZIL-UHFFFAOYSA-H 0.000 description 1
- KNXDJTLIRRQLBE-UHFFFAOYSA-H dialuminum;propane-1,2-diol;chloride;pentahydroxide;hydrate Chemical compound O.[OH-].[OH-].[OH-].[OH-].[OH-].[Al+3].[Al+3].[Cl-].CC(O)CO KNXDJTLIRRQLBE-UHFFFAOYSA-H 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000005183 environmental health Effects 0.000 description 1
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229940060384 isostearyl isostearate Drugs 0.000 description 1
- 229940113915 isostearyl palmitate Drugs 0.000 description 1
- 229940061515 laureth-4 Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 150000005217 methyl ethers Chemical class 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical class CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229940066842 petrolatum Drugs 0.000 description 1
- 235000019271 petrolatum Nutrition 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229940057874 phenyl trimethicone Drugs 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
Abstract
Bu buluş, taşıyıcı ajan, emoliyan ve beyazlık azaltıcı ester ve askıda tutucu ajanın art arda eklenerek karıştırılması, karıştırma işlemi sürerken antiperspirant aktifinin eklenmesi, ardından esansın ilave edilmesi ve son olarak karışımın homojenize edilmesi işlemlerini kapsayan; terleme ve terleme sonucunda oluşan istenmeyen vücut kokularını inhibe ederken; dibutil adipat içeren bileşimi aracılığı ile kullanım sırasında tekstil üzerinde oluşabilecek beyaz iz oluşumunu engelleyen aerosol yapıda tasarlanmış bir antiperspirant formülasyonu ile ilgilidir.The present invention encompasses the process of mixing the carrier agent, emollient and whitening ester and suspending agent with successive addition, adding the antiperspirant active while stirring, followed by adding the essence and finally homogenizing the mixture; while inhibiting perspiration and undesired body odors as a result of sweating; The present invention relates to an antiperspirant formulation designed in an aerosol structure which prevents the formation of white marks on the textile during use by means of its composition comprising dibutyl adipate.
Description
TARIFNAME AEROSOL YAPIDA BIR ANTIPERSPIRANT FORMÜLASYONU Teknik Alan Bu bulus aerosol yapida olan ve yüksek miktarda antiperspirant aktifi içeren, kullanim sirasinda ve sonrasinda tekstil üzerinde olusacak beyazligi en aza indirecek yeni bir formülasyon ile ilgilidir. Önceki Teknik Bugüne kadar tüketiciye sunulan deodorantlar temel olarak terlemeyi önleyici ya da terleme sonucu olusan istenmeyen kötü kokuyu inhibe edici olmak üzere iki farkli ihtiyaca cevap verecek yapidadir. Bazi ürünler bu iki temel fonksiyonu yapisinda bulundururken bazi ürünlerde bu fonsiyonlardan sadece birinin saglanmasi amaçlanmistir. Kötü kokuyu inhibe edici formüller antibakteriyel aktifler ya da parfüm hammaddeleri ile bu özelligi saglarken, terlemeyi önleyici fonksiyonun temel dayanagi genellikle alüminyum/klor/hidrat yapisinda olan antiperspirant aktifleridir. En yaygin olarak kullanilan türevleri ise alüminyum klorohidrat, alüminyum sesquiklorohidrat ve alüminyum zirkonium klorohidrat GLY hammaddeleridir. DESCRIPTION AN ANTIPERSPIRANT FORMULATION IN AN AEROSOL STRUCTURE Technical Area This invention is in aerosol form and contains a high amount of antiperspirant active, Minimize the whiteness that will occur on the textile during and after use. It is about a new formulation that will download. Prior Art So far, deodorants offered to the consumer are basically antiperspirant or antiperspirant. It also has two functions, inhibiting the undesirable bad odor caused by sweating. It is structured to meet different needs. Some products have these two basic functions. In some products, only one of these functions is intended to be provided. odor inhibiting formulas antibacterial While providing this feature with actives or perfume raw materials, antiperspirant The mainstay of the function is usually aluminum/chlorine/hydrate structure. antiperspirant actives. The most widely used derivatives are aluminum. chlorohydrate, aluminum sesquichlorohydrate, and aluminum zirconium chlorohydrate GLY raw materials.
Terleme; termal regülasyonu saglayarak, vücudun sicakliginin yaklasik olarak 37°Cade sabit tutulmasini saglarken, ter bezleri salgilarinin bakteriyle etkilesimi sonucunda kötü koku olusumuna sebebiyet vermektedir. Ter bezleri cilt yüzeyinin hemen altinda yer alir ve ekrin ve apokrin olmak üzere iki temel sinifa ayrilirlar. Sweating; by providing thermal regulation, the temperature of the body is approximately The interaction of sweat gland secretions with bacteria while maintaining a constant 37°C resulting in bad odour. sweat glands of the skin surface They are located just below and are divided into two basic classes, eccrine and apocrine.
Vücuda yayilan ve çok sayida bulunan ekrin bezleri, termal regülasyon için esas islevi yerine getiren, kokusuz, seyreltik, elektrolit bir çözelti salgilarlar. Kötü kokunun asil kaynagi ise organik materyaller bakimindan zengin olan, genel olarak koltukaltinda yogunlasan ve bu sebeple bakteriler için elverisli, sicak ve nemli bir ortam yaratan apokrin salgisidir. Ekrin bezleri de nemli ortam olusturup apokrin salgisinin dispersiyonuna katki saglayarak dolayli yoldan da olsa kötü 2154.11 koku olusumunu tetiklerler. Eccrine glands, which are numerous and spread throughout the body, are essential for thermal regulation. They secrete an odorless, dilute, electrolyte solution that performs its function. Bad The main source of the smell is the general, rich in organic materials. It is condensed in the armpit and therefore suitable for bacteria, warm and It is the apocrine secretion that creates a moist environment. Eccrine glands also create a moist environment. contributes to the dispersion of apocrine secretion, albeit indirectly. 2154.11 trigger odor formation.
Antiperspirantlar aerosol deodorant, roll on deodorant ve stick formunda tüketiciye sunulurlar. Roll on formlarinda genel olarak hidratli alüminyum klor yapisindaki antiperspirant aktifi esans ile birlikte kozmetik bir likit bir formül içerisinde emülsiye edilir. Stick formunda emülsiyon yerine, antiperspirant aktifin kati form içerisinde süspansiyon olusturmasi ile yapi olusturulur. Pazarin daha büyük kismini olusturan aerosol antiperspirant ürünlerde ise homojen likit yapida askida tutulan alüminyum içeren antiperspirant aktifinin itici LPG gaz karisimi ile püskürtülmesi ile ürünün kullanimi saglanir. Birbirinden farkli olan bu yapilarda genel amaç terlemeyi yeteri kadar baskilayacak antiperspirant aktifinin formülde bulundurulmasi, homojen bir yapinin olusturulmasi, kullanim sirasinda özellikle koyu renk ve siyah kiyafetlerde beyaz pudramsi sekilde olusabilen beyaz kalintinin en aza indirilmesi seklinde özetlenebilir. Antiperspirants are in aerosol deodorant, roll-on deodorant and stick form. are offered to the consumer. Generally, hydrated aluminum chlorine in roll-on forms It is a cosmetic liquid formula with antiperspirant active essence in its structure. is emulsified. Instead of emulsion in stick form, antiperspirant active Structure is formed by creating suspension in solid form. your market more In aerosol antiperspirant products that make up the majority of it, it is homogeneous liquid. with the propellant LPG gas mixture of the suspended aluminum-containing antiperspirant active. By spraying, the use of the product is ensured. In these structures, which are different from each other, general purpose, antiperspirant active that will suppress sweating sufficiently should be included in the formula. to be kept, to create a homogeneous structure, especially during use white powder that can occur as white powder on dark and black clothes can be summarized as minimizing the residue.
Literatürde antiperspirant aktifi olarak tanimlanmis olan hammaddeler; alüminyum klorid, alüminyum klorohidrat, alüminyum klorohidreks, alüminyum klorohidreks PG, alüminyum klorohidreks PEG, alüminyum diklorohidrat, alüminyum diklorohidreks PG, alüminyum diklorohidreks PEG, alüminyum sesquiklorohidrat, alüminyum sesquiklorohidreks PG, alüminyum sesquiklorohidreks PEG, alüminyum sülfat, alüminyum zirkonyum oktoklorohidrat, alüminyum zirkonyum oktoklorohidreks GLY, alüminyum zirkonyum pentaklorohidrat, alüminyum zirkonyum pentaklorohidreks GLY, alüminyum zirkonyum tetraklorohidrat, alüminyum zirkonyum triklorohidrat, alüminyum zirkonyum tetraklorohidrat GLY ve alüminyum zirkonyum triklorohidrat GLY seklinde siralanabilir. Raw materials defined as antiperspirant active in the literature; aluminum chloride, aluminum chlorohydrate, aluminum chlorohydrex, aluminum chlorohydrex PG, aluminum chlorohydrex PEG, aluminum dichlorohydrate, aluminum dichlorohydrex PG, aluminum dichlorohydrex PEG, aluminum sesquichlorohydrate, aluminum sesquichlorohydrex PG, aluminum sesquichlorohydrex PEG, aluminum sulfate, aluminum zirconium octochlorohydrate, aluminum zirconium octochlorohydrex GLY, aluminum zirconium pentachlorohydrate, aluminum zirconium pentachlorohydrex GLY, aluminum zirconium tetrachlorohydrate, aluminum zirconium trichlorohydrate, aluminum zirconium tetrachlorohydrate GLY and aluminum zirconium trichlorohydrate can be listed as GLY.
Bu formüllerin tümünde aplikasyonu kolaylastirmak ve ciltte yagli olmayan yumusak bir his birakmak amaci ile nemlendiriciler, uçucu silikonlar ve benzer yapida farkli hammaddeler kullanilir. Sonuçta elde edilen yapi dermatolojik 2154.11 olarak kullanicinin cildi ile uyumlu olmali, aerosol formlarda ise partikül boyutu / insan ve çevre sagligi açisindan özellikle irdelenmelidir. In all of these formulas, it is easy to apply and non-oily on the skin. moisturizers, volatile silicones and similar Different raw materials are used in the construction. The resulting structure is dermatological 2154.11 It should be compatible with the user's skin, and in aerosol forms, the particle size / It should be especially examined in terms of human and environmental health.
Antiperspirant ürünlerde temel kriterlerden biri olan mümkün olan en düsük düzeyde beyaz kalinti olusturma hedefi son yillarda gittikçe önem kazanmis ve bu durum tüketiciye sunulan ürünlerin çesitliliginin de daha çok bu yöne evrilmesi ile sonuçlanmistir. Bu amaçla farkli polimer yapida hidrokarbon bilesikleri, ester yapilari, düz ya da halka yapida silikon türevleri antiperspirant forrnüllere entegre edilmeye baslanmistir. One of the basic criteria in antiperspirant products, the lowest possible The goal of creating a high level of white residue has become increasingly important in recent years, and this The situation is due to the fact that the variety of products offered to the consumer evolves more in this direction. has been concluded. For this purpose, hydrocarbon compounds with different polymer structures, ester structures, flat or ring-shaped silicone derivatives integrated into antiperspirant formulas is pressed.
Literatürde bu grup içerisinde siniflandirilan ve pratikte kullanimi olan hammaddeler; izostearil izostearat, gliseret-7-benzoat, Cl2-C15 alkil benzoat, oktildodekil benzoat, izostearil laktat, izostearil palmitat, benzil laurat, lauret 4, lauret 7, olet 2, PEG 4, PEG 12, izopropil miristat, izopropil palmitat, butil stearat, polietilen glikol metil eterleri, PPG 2 setearet 9, PPG 2 izodeket 12, PPG 5 butil eter, PPG 14 butil eter, PPG 15 butil eter, PPG 53 butil eter, oktildodekanol, polideken, mineral yaglar, vazelin, feniltrimetikon, dimetikon kopoliol ve bunlarin karisimlaridir. Örnek olarak USSl94249A patentinde aerosol olmayan bir formda %1-30 araliginda propilen glikol stearat ve etoksile stearil alkol emülsiye edicileri ile formüle edilmis, %2-20 araliginda uçucu olmayan dimetikon, %10-60 araliginda alüminyum tuzu ve %70,e kadar su içeren formülün beyazligi engelleyen bir yapi olusturdugu iddia edilmektedir. US5840289A numarali diger bir patentte ögütme islemi ile aktiflestirilmis, bosluklu yapida olmayan, 1,52 - 1,57 araliginda düzenli bir refraktif indeks degerine sahip alüminyum klorür ve 1.40 - 1,57 refraktif indeks degerine sahip olan benzoat esterleri, hidrojene polibütan, PPG-14 bütil eter, izopropil palmitat, fenil silikon ve izopropil miristat gibi beyazlik maskeleyici özellik gösteren hammadde grubundan bir ya da birkaç hammaddenin kullanildigi formülün beyazligi azaltici etkiye sahip oldugu iddia edilmektedir. 2154.11 oraninda etanolün kullanildigi, antiperspirant aktifi olarak %l-%15 araliginda alüminyum klorohidrat bulunduran ve ayni zamanda uçucu silikon ve organik yumusatici ajan içeren, beyaz izleri azaltici özellikte aerosol formda bir antiperspirant formülasyonundan bahsedilmistir. Classified in this group in the literature and used in practice. raw materials; isostearyl isostearate, glyceret-7-benzoate, Cl2-C15 alkyl benzoate, octyldodecyl benzoate, isostearyl lactate, isostearyl palmitate, benzyl laurate, laureth 4, lauret 7, olet 2, PEG 4, PEG 12, isopropyl myristate, isopropyl palmitate, butyl stearate, polyethylene glycol methyl ethers, PPG 2 cetearet 9, PPG 2 isodecet 12, PPG 5 butyl ether, PPG 14 butyl ether, PPG 15 butyl ether, PPG 53 butyl ether, octyldodecanol, polydecene, mineral oils, petrolatum, phenyltrimethicone, dimethicone copolyol and their are mixtures. For example, 1-30% in a non-aerosol form in the USS194249A patent. with propylene glycol stearate and ethoxylated stearyl alcohol emulsifiers in the range formulated, 2-20% non-volatile dimethicone, 10-60% A structure that prevents the whiteness of the formula containing aluminum salt and water up to 70%. allegedly created. Grinding in another patent numbered US5840289A activated by the process, non-gap, regular in the range of 1.52 - 1.57 aluminum chloride with a refractive index value of 1.40 - 1.57 benzoate esters with index value, hydrogenated polybutane, PPG-14 butyl whiteness such as ether, isopropyl palmitate, phenyl silicone and isopropyl myristate one or more raw materials from the raw material group showing masking properties. It is claimed that the formula in which it is used has a whitening-reducing effect. 2154.11 1%-15% of ethanol is used as an antiperspirant active. containing aluminum chlorohydrate and also volatile silicon and organic An aerosol form containing a softening agent, which reduces white marks. antiperspirant formulation is mentioned.
Yaptigimiz arastirmalar, beyazligi azaltici amaçla dibutil adipat kullanimi ile ilgili olarak literatür çalismalarinin henüz yapilmadigi yönündedir. Our researches have been related to the use of dibutyl adipate for whitening reduction. As a result, literature studies have not been done yet.
Bulusun Kisa Açiklamasi Bu bulusun öncelikli amaci aerosol antiperspirant ürünlerinde en temel sorunlardan biri olarak degerlendirilen kiyafetler üzerinde beyaz kalinti birakma etkisinin en aza indirilmesini saglayan formül içerigini tanimlamaktir. Brief Description of the Invention The primary purpose of this invention is to provide the most basic in aerosol antiperspirant products. leaving a white residue on clothes, which is considered as one of the problems The aim is to define the formula content that minimizes the effect.
Bu bulusun diger amaci, diester yapida bir emoliyan hammaddenin kullanildigi aerosol yapida beyazlik azaltici özelllikte formül içerigi tanimlamaktir. The other purpose of this invention is to use an emollient raw material in diester structure. It is to define the content of the formula with whitening reducing feature in aerosol structure.
Bu bulusun diger amaci, adipik asit ve bütil alkol diesteri olan dibütil adipatin kullanildigi aerosol yapida beyazlik azaltici bir formül gelistirilmesidir. Another object of this invention is dibutyl adipate, a diester of adipic acid and butyl alcohol. It is the development of a whitening reducing formula in the aerosol structure in which it is used.
Bulusun Ayrintili Açiklamasi Bu bulus ile ilgili olarak, hedeflenen formülasyonun elde edilmesi amaciyla yürütülen üretim yöntemi detayini açiklayan akim semasi ekte Sekil llde yer almaktadir. Detailed Description of the Invention With regard to this invention, in order to achieve the targeted formulation, The flow chart describing the details of the production method carried out is given in the appendix. takes.
Terleme ve bunun sonucu olusan istenmeyen Vücut kokularini inhibe ederken; kullanim sirasinda tekstil üzerinde olusabilecek beyaz iz olusumunu engelleyen bulus konusu aerosol yapida bir antiperspirant formülasyonu, - askida tutucu kil yapida ajan, tasiyici ajan ve esterlerin karistirilmasi - karistirma islemi sürerken antiperspirant aktifinin eklenmesi 2154.11 - bunu takiben esansin eklenmesi - nihai karisimin homojenize edilmesi adimlariyla elde edilmekte ve; tasiyici ajan olarak uçucu ve uçucu olmayan silikon, askida tutucu ajan olarak hektorit kili, emoliyan ve beyazligi azaltici esterleri, antiperspirant aktifi olarak alüminyum tuzlarindan olusmaktadir. While inhibiting sweating and the resulting undesirable body odors; It prevents the formation of white marks that may occur on the textile during use. the subject of the invention is an antiperspirant formulation in aerosol form, - mixing of suspending clay structure agent, carrier agent and esters - adding antiperspirant active while mixing is in progress 2154.11 - followed by the addition of essential oil - obtained by homogenizing the final mixture, and; volatile and non-volatile silicone as carrier agent, suspending agent Hectorite clay, emollient and whitening reducing esters, as antiperspirant active consists of aluminum salts.
Bu amaçla ilk asamada askida tutucu kil yapida ajan, tasiyici ajan ve esterler 50- 500 rpm araliginda, tercihen 300 rpm hizinda birbiri üzerine eklenerek karistirilmaktadir. For this purpose, in the first stage, suspended clay structure agent, carrier agent and esters are used in 50- By adding them on top of each other at a speed of 500 rpm, preferably 300 rpm. are mixed.
Tasiyici ajan olarak uçucu ve uçucu olmayan silikonlar, siklo penta siloksan ve dimetikon tercih edilir. Askida tutucu ajan olarak hektorit kili, emoliyan ester olarak da izopropil palmitat ve C12-15 alkil benzoat kullanilir. Bulusun temel iddiasini olusturan beyazlik azaltici ester olarak da dibutil adipat tercih edilmektedir. Volatile and non-volatile silicones, cyclopenta siloxane and dimethicone is preferred. Hectorite clay as suspending agent, emollient ester Also, isopropyl palmitate and C12-15 alkyl benzoate are used. Invention is fundamental Dibutyl adipate is preferred as the whitening reducing ester that makes its claim. is being done.
Karistirma devam ederken alüminyum tuzu yapisindaki antiperspirant aktifi, tercihen alüminyum klorohidrat ve/veya alüminyum sesquiklorohidrat ilavesi yapilir. While mixing continues, antiperspirant active in aluminum salt structure, preferably addition of aluminum chlorohydrate and/or aluminum sesquichlorohydrate makes.
Aerosol yapida bir antiperspirant formülasyonu, beyazlik azaltici ester olarak agirlikça % 10-15 oraninda dibutil adipat içermektedir. An aerosol antiperspirant formulation, as a whitening reducing ester It contains 10-15% dibutyl adipate by weight.
Antiperspirant aktifi ilavesinden sonra esans eklenerek karistirma islemi tamamlanir; karistirma prosesi toplamda 10-15 dk araliginda sürer, prosesin son adiminda yüksek devirde, tercihen 3500 rpm hizinda 2-5 dk homojenizasyon islemi gerçeklestirilir. After adding antiperspirant active, mixing process by adding essence is completed; The mixing process takes 10-15 minutes in total. Homogenization for 2-5 minutes at high speed, preferably at 3500 rpm operation is performed.
Bu yöntemde üretilen aerosol yapidaki formülün itici gazlar disindaki bilesen dagilimi; siklo penta siloksan, izopropil palmitate ve dibutil adipat için her biri 2154.11 biri % 1-20, tercihen %3-10; alüminyum klorohidrat ve/veya alüminyum Bahsi geçen formül itici gaz ilavesi ile basinçli kap formuna uygun olacak sekilde tasarlanmistir. Içerik, terleme ve bunun sonucu olusan istenmeyen vücut kokularini inhibe ederken; kullanim sirasinda tekstil üzerinde olusabilecek beyaz iz olusumunu yeni bir içerikle engelleme temel iddiasina sahiptir. The component of the aerosol structured formula produced in this method, excluding propellants, distribution; each for cyclo penta siloxane, isopropyl palmitate and dibutyl adipate 2154.11 one is 1-20%, preferably 3-10%; aluminum chlorohydrate and/or aluminum The aforementioned formula should be adjusted to be suitable for the pressure vessel form with the addition of propellant gas. is designed. Content, perspiration and the resulting unwanted body while inhibiting odors; whitening that may occur on the textile during use. It has the basic claim of preventing trace formation with a new content.
Askida tutucu kil yapida ajan, tasiyici ajan ve esterlerin karistirilmasi Karistirma islemi sürerken antiperspirant aktifinin eklenmesi Aktif maddeyi takiben takiben esansin eklenmesi Nihai karisimin homojenize edilmesi Suspending clay structure agent, carrier agent and esters mixing While the mixing process is in progress, the antiperspirant active adding Essence following the active substance adding Homogenize the final mixture to be made
Claims (7)
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TR2017/06114A TR201706114A2 (en) | 2017-04-25 | 2017-04-25 | ANERIPERSPIRANT FORMULATION IN AEROSOL STRUCTURE |
| PCT/TR2018/050175 WO2018236320A2 (en) | 2017-04-25 | 2018-04-19 | An antiperspirant formulation in aerosol form |
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| Application Number | Priority Date | Filing Date | Title |
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| TR2017/06114A TR201706114A2 (en) | 2017-04-25 | 2017-04-25 | ANERIPERSPIRANT FORMULATION IN AEROSOL STRUCTURE |
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| US5156834A (en) * | 1979-11-07 | 1992-10-20 | The Procter & Gamble Company | Antiperspirant compositions |
| US4900542A (en) * | 1985-03-20 | 1990-02-13 | Carter-Wallace Inc. | Manufacturing process for microcrystalline emulsions |
| US6534045B2 (en) * | 2000-12-21 | 2003-03-18 | Colgate Palmolive Company | High efficacy antiperspirant stick |
| CA2738683C (en) * | 2008-10-23 | 2013-11-26 | The Procter & Gamble Company | Anhydrous antiperspirant compositions |
| DE102012224157A1 (en) * | 2012-12-21 | 2014-06-26 | Henkel Ag & Co. Kgaa | Textile-friendly antiperspirant sprays with hydroxycarboxylic acids |
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