TR200605914A2 - SINGLE STAGE CALCINATION-AUTOGENE GRINDING AND SEPARATION METHOD (KÖS) AND CANCINE TINCAL PRODUCTION - Google Patents
SINGLE STAGE CALCINATION-AUTOGENE GRINDING AND SEPARATION METHOD (KÖS) AND CANCINE TINCAL PRODUCTIONInfo
- Publication number
- TR200605914A2 TR200605914A2 TR2006/05914A TR200605914A TR200605914A2 TR 200605914 A2 TR200605914 A2 TR 200605914A2 TR 2006/05914 A TR2006/05914 A TR 2006/05914A TR 200605914 A TR200605914 A TR 200605914A TR 200605914 A2 TR200605914 A2 TR 200605914A2
- Authority
- TR
- Turkey
- Prior art keywords
- product
- calcined
- tincal
- tinkal
- micronized
- Prior art date
Links
Landscapes
- Manufacture And Refinement Of Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
Tüvenan tinkalden belirtilen standartlarda Mikronıze Kalsine Tınkal Üretiminin gerçekleştirilmesinde kullanılan "Tek Kademede Kalsınasyon-Otojen Öğütme ve Separasyon Yöntemi (KOŞ)" ile yüksek B2O3 içerikli bor ürünü üretilmekte, üretimde su tüketilmemekte, kuru atık çıkarılarak depolanabılmekte ve atık barajına ihtiyaç duyulmamaktadır. Bu nedenle bu yöntem işletme çevre sorunlarını en aza indiren yeni bir yöntemdir. Prosese optimum tüvenan cevher beslenmesiyle tek kademede %20-28 B2O3 tenörlü, 10 mol kristal suyuna sahip tüvenan tinkal cevherinden, B2O3'ce %90-95 verimle çözünmeyen madde oranı (safsızlık) ortalama %10-15 olan, -200 mikron ebatmda, 0,2-0,3 g/cm dökme yoğunluğunda, 1-2 mol kristal suyu içeriğine sahip, %0-0,4 kaba rutubete sahip (40 °C de 20 saat) %50-58 B2O3 tenörlü Na2B4O7.(1-2)H2O kimyasal formüllü yeni bir ürün olan "Mikronize Kalsine Tinkal" m üretilmesi sağlanmıştır. Mikronize kalsine tinkal düşük dökme yoğunluğuna ve düşük tane boyuna sahip olması nedeniyle nakliye ve proses kullanımlarında güçlüklere yol açacaktır. Bu sorunları ortadan kaldırmak için, mikronıze kalsine tınkalin 2 aşamasında ürünün kimyasal yapısını bozmadan "Kompaktlama Yöntemi" ile kompaktlaması yapılmak suretiyle dökme yoğunluğu ve tane boyu arttırılarak "Kompaktlanmış Kalsine Tinkal" ürünü elde edilmiştir. Fırın ağzından kuru olarak alınan kalsine kil (atık), ortalama %3-5 B2O3 tenörlü ve katı halde depolanabilecek olup, çevre kirliliğini sulu atığa göre minimum seviyede tutacaktır. Mikronize Kalsine Tinkal ürününün kimyasal yapısı (Na2B4O7 (1-2)H2O), tane boyunun inceliği, çözünmeyen madde miktarının azlığı, B2O3 miktarının yüksek olması gibi ürün özellikleri; çözünürlüğünün yüksek olmasına ve endüstride alternatif ürün olarak direkt kullanılmasıyla beraber rafine bor ürünlerin üretilmesi imkanlarını sağlamaktadır.Boron product with high B2O3 content is produced by "Single Stage Calcination-Autogenous Grinding and Separation Method (KOŞ)", which is used in the production of Micronized Calcined Tincal in the specified standards from Tüvenan tinkal. Therefore, this method is a new method that minimizes business environmental problems. The optimum tufting ore feed to the process is 20-28% B2O3 grade, 10 moles of crystal water from the tincal ore in a single stage. The insoluble matter ratio (impurity) is 10-15% with a yield of 90-95% by B2O3. Na2B4O7 with a bulk density of 2-0.3 g / cm, a content of 1-2 moles of crystalline water, a roughness of 0-0.4% (20 hours at 40 ° C) and a grade of 50-58% B2O3. ) A new product with the chemical formula H2O "Micronized Calcined Tinkal" was produced. Micronized calcined tincal has low bulk density and low grain size which will cause difficulties in transportation and process use. In order to eliminate these problems, "Compacted Calcined Tinkal" product was obtained by increasing the bulk density and grain size by compacting the product with the "Compacting Method" without disturbing the chemical structure of the product in the micronized calcined tinkaline 2 stage. Calcined clay (waste) taken dry from the furnace mouth can be stored in average 3-5% B2O3 grade and solid state and will keep the environmental pollution at minimum level compared to aqueous waste. Chemical structure of Micronized Calcined Tinkal product (Na2B4O7 (1-2) H2O), fineness of grain size, low amount of insoluble matter, high B2O3 content; It provides the possibility of producing refined boron products with its high solubility and direct use as an alternative product in the industry.
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TR2006/05914A TR200605914A2 (en) | 2006-10-20 | 2006-10-20 | SINGLE STAGE CALCINATION-AUTOGENE GRINDING AND SEPARATION METHOD (KÖS) AND CANCINE TINCAL PRODUCTION |
| UAA200904965A UA95988C2 (en) | 2006-10-20 | 2007-10-17 | Micronized calcined tincal product, process for its production by calcination, autogenic grinding and separation in single step (cags), compacted calcined tincal product and process for its production |
| PCT/IB2007/054225 WO2008047314A2 (en) | 2006-10-20 | 2007-10-17 | Calcined tincal production method by calcination autogenic grinding and seperation (casg) method in a single step |
| CN2007800389380A CN101605726B (en) | 2006-10-20 | 2007-10-17 | Calcined tincal production method by calcination autogenic grinding and seperation (casg) method in a single step |
| US12/446,090 US20110027158A1 (en) | 2006-10-20 | 2007-10-17 | Calcined Tincal Production Method by Calcination Autogenic Grinding and Separation (CASG) Method in a Single Step |
| RU2009114569/05A RU2443628C2 (en) | 2006-10-20 | 2007-10-17 | Method of producing calcined tincal by calcination using autogenic crushing and separation in one step |
| JP2009532943A JP5580593B2 (en) | 2006-10-20 | 2007-10-17 | Method for producing calcined borax by calcined self-pulverization and separation (CASG) method in a single step |
| EP07118803.1A EP1914200B1 (en) | 2006-10-20 | 2007-10-18 | Calcined tincal production method by calcination autogenic grinding and separation (CASG) method in a single step |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TR2006/05914A TR200605914A2 (en) | 2006-10-20 | 2006-10-20 | SINGLE STAGE CALCINATION-AUTOGENE GRINDING AND SEPARATION METHOD (KÖS) AND CANCINE TINCAL PRODUCTION |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TR200605914A2 true TR200605914A2 (en) | 2008-05-21 |
Family
ID=41470944
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TR2006/05914A TR200605914A2 (en) | 2006-10-20 | 2006-10-20 | SINGLE STAGE CALCINATION-AUTOGENE GRINDING AND SEPARATION METHOD (KÖS) AND CANCINE TINCAL PRODUCTION |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN101605726B (en) |
| TR (1) | TR200605914A2 (en) |
| UA (1) | UA95988C2 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101913618A (en) * | 2010-08-16 | 2010-12-15 | 禄丰天源工贸有限公司 | Sodium borate modifying method |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4031354A (en) * | 1974-05-15 | 1977-06-21 | Canada Packers Limited | Rotary heating apparatus for puffing borax |
| US4041132A (en) * | 1974-09-09 | 1977-08-09 | United States Borax & Chemical Corporation | Fluid bed dehydration of borax |
| US4412978A (en) * | 1982-03-15 | 1983-11-01 | Stokely-Van Camp, Inc. | Method and apparatus for manufacturing improved puffed borax |
-
2006
- 2006-10-20 TR TR2006/05914A patent/TR200605914A2/en unknown
-
2007
- 2007-10-17 CN CN2007800389380A patent/CN101605726B/en not_active Expired - Fee Related
- 2007-10-17 UA UAA200904965A patent/UA95988C2/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN101605726B (en) | 2012-05-09 |
| UA95988C2 (en) | 2011-09-26 |
| CN101605726A (en) | 2009-12-16 |
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