TH23284Y - Preparation of a composite of Indian gooseberry extract with magnesium iron-layer double hydroxide using the solid-state method. - Google Patents

Abstract

OCR (Solid State Creation) is a method of synthesis using the solid-state method of mixing two or more precursor powders, such as Moringa oleifera extract and magnesium iron-layered double hydroxide. This can be effectively applied to produce antioxidant and antibacterial products. Herbal composite materials are prepared by mixing Moringa oleifera extract and synthesizing magnesium iron-layered double hydroxide using the solid-state method. This novel preparation method is chemical-free, environmentally friendly, applicable to other herbal extracts, and involves a simple and inexpensive synthesis process.

Claims (2)

OCR 1. The composite material of Indian gooseberry extract with magnesium iron-layer double hydroxide consists of: 1) Indian gooseberry extract and 2) magnesium iron-layer double hydroxide. The composite material was prepared using the solid-state method by mixing the Indian gooseberry extract and magnesium iron-layer double hydroxide in a ratio of 1:5 by weight. 2. The process for producing composite materials of Terminalia chebula extract with magnesium iron-layer double hydroxide, as per claim 1, using the solid-solid method, involves the following steps: 2.1 Extraction of the solution from Terminalia chebula: 2.1.1 Collect plant samples, specifically the leaves of Terminalia chebula. 2.1.2 Wash and clean the leaves, cut them into small pieces, and dry them at 60°C for 48 hours until the weight is constant. 2.1.3 Soak the dried Terminalia chebula samples in ethanol solvent and perform cold extraction at room temperature for 2 weeks. Then filter to obtain only the solution. 2.1.4 Evaporate the ethanol extract to dryness using a rotary distillation apparatus to obtain the crude ethanol extract of the plant. 2.1.5 Evaporate the water from the solution to remove excess solvent. 2.2 Synthesis of Magnesium Iron-Layer Double Hydroxide: 2.2.1 Weigh 24.0150 g of magnesium chloride hexahydrate and mix with 5.3336 g of aluminum chloride. Dissolve in 80 ml of deionized water. 2.2.2 Adjust the pH of the solution to 7 using concentrated ammonia solution while stirring with a magnetic rod. 2.2.3 Cover the container and incubate at 80°C for 24 hours. 2.2.4 Adjust the pH of the resulting precipitate to 7 and wash it 5 times with deionized water until no chloride ions remain. Test with silver nitrate solution and ethanol 3 times. Dry the precipitate at 60°C to obtain magnesium iron-layer double hydroxide. 2.3 Synthesis of Composite Material of Ma-Mao Extract with Magnesium Iron-Layer Double Hydroxide. 2.3.1 Mix the mulberry extract and magnesium-layer double hydroxide in a 1:by weight ratio. Apply acetone evenly to the mixture. 2.3.2 Grind the mixture thoroughly for 30 minutes to obtain a composite of mulberry extract and magnesium iron-layer double hydroxide.