TH155134A - Process for purification of lutein from marigold flower by chromatography method. - Google Patents
Process for purification of lutein from marigold flower by chromatography method.Info
- Publication number
- TH155134A TH155134A TH1201000430A TH1201000430A TH155134A TH 155134 A TH155134 A TH 155134A TH 1201000430 A TH1201000430 A TH 1201000430A TH 1201000430 A TH1201000430 A TH 1201000430A TH 155134 A TH155134 A TH 155134A
- Authority
- TH
- Thailand
- Prior art keywords
- lutein
- purification
- chromatography method
- marigold flower
- adsorbent
- Prior art date
Links
- 235000005881 Calendula officinalis Nutrition 0.000 title claims abstract 5
- 229960005375 Lutein Drugs 0.000 title claims abstract 5
- KBPHJBAIARWVSC-NRHWGSPPSA-N Lutein Natural products O[C@H]1C=C(C)[C@H](/C=C/C(=C\C=C\C(=C/C=C/C=C(\C=C\C=C(/C=C/C=2C(C)(C)C[C@H](O)CC=2C)\C)/C)\C)/C)C(C)(C)C1 KBPHJBAIARWVSC-NRHWGSPPSA-N 0.000 title claims abstract 5
- 235000012311 Tagetes erecta Nutrition 0.000 title claims abstract 5
- 235000003595 Tagetes minuta Nutrition 0.000 title claims abstract 5
- 235000012680 lutein Nutrition 0.000 title claims abstract 5
- 239000001656 lutein Substances 0.000 title claims abstract 5
- 238000000034 method Methods 0.000 title claims abstract 4
- 238000000746 purification Methods 0.000 title claims abstract 4
- 238000004587 chromatography analysis Methods 0.000 title abstract 3
- KBPHJBAIARWVSC-RGZFRNHPSA-N (1R)-4-[(1E,3E,5E,7E,9E,11E,13E,15E,17E)-18-[(1R,4R)-4-hydroxy-2,6,6-trimethylcyclohex-2-en-1-yl]-3,7,12,16-tetramethyloctadeca-1,3,5,7,9,11,13,15,17-nonaenyl]-3,5,5-trimethylcyclohex-3-en-1-ol Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-RGZFRNHPSA-N 0.000 title 1
- 240000000785 Tagetes erecta Species 0.000 title 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N acetic acid ethyl ester Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract 9
- VLKZOEOYAKHREP-UHFFFAOYSA-N hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims abstract 6
- KBPHJBAIARWVSC-TWGKZGRNSA-N (3R,3'R,6'R)-β,ε-carotene-3,3'-diol Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=C[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-TWGKZGRNSA-N 0.000 claims abstract 4
- 241000736851 Tagetes Species 0.000 claims abstract 4
- 239000003463 adsorbent Substances 0.000 claims abstract 3
- 239000008079 hexane Substances 0.000 claims abstract 3
- 239000000741 silica gel Substances 0.000 claims abstract 3
- 229910002027 silica gel Inorganic materials 0.000 claims abstract 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract 3
- 238000003379 elimination reaction Methods 0.000 claims 1
- 239000011259 mixed solution Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 238000010828 elution Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
Abstract
DC60 (02/02/55) การประดิษฐ์นี้เกี่ยวข้องกับกรรมวิธีในการทำสารลูทีนจากดอกดาวเรืองให้บริสุทธิ์ด้วยวิธี โครมาโตกราฟีโดยใช้ซิลิกาเจลเป็นตัวดูดซับ และใช้สารชะเป็นสารละลายผสมของเฮกเซนกับเอธิล อะซิเตต โดยใช้อุณหภูมิในการทำให้บริสุทธิ์ระหว่าง 25-40 องศาเซลเซียส การประดิษฐ์นี้เกี่ยวข้องกับกรรมวิธีในการทำสารลูทีนจากดอกดาวเรืองให้บริสุทธิ์ด้วยวิธี โครมาโตกราฟีโดยใช้ซิลิกาเจลเป็นตัวดูดซับ และใช้สารชะเป็นสารละลายผสมของเฮกเซนกับเอธิล อะซิเตต โดยใช้อุณหภูมิในการทำให้บริสุทธิ์ระหว่าง 25-40 องศาเซลเซียส DC60 (02/02/55) This invention involves a process for purifying lutein from marigold flowers by means of Chromatography using silica gel as the adsorbent The elution was used as a mixture of hexane and ethyl acetate using a purification temperature between 25-40 ° C. This invention involved a process for purifying lutein from marigold flowers. In a way Chromatography using silica gel as the adsorbent The elution was used as a mixture of hexane and ethyl acetate using the purification temperature between 25-40 ° C.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TH155134A true TH155134A (en) | 2016-08-09 |
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