SU513973A1 - The method of obtaining 1- (3 "-phenylpropene2" -yl) -2,5-dimethyl-4-phenyl-4-propionyloxypiperidine or its hydrochloride - Google Patents
The method of obtaining 1- (3 "-phenylpropene2" -yl) -2,5-dimethyl-4-phenyl-4-propionyloxypiperidine or its hydrochlorideInfo
- Publication number
- SU513973A1 SU513973A1 SU2018964A SU2018964A SU513973A1 SU 513973 A1 SU513973 A1 SU 513973A1 SU 2018964 A SU2018964 A SU 2018964A SU 2018964 A SU2018964 A SU 2018964A SU 513973 A1 SU513973 A1 SU 513973A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- hydrochloride
- dimethyl
- phenyl
- propionyloxypiperidine
- obtaining
- Prior art date
Links
Landscapes
- Hydrogenated Pyridines (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
катализатор отфильтровывают и промывают гор чим этанолом. Спиртовый раствор упаривают и кристаллизацией масл нистого остатка из петролейного эфира получают 1,00 г (66%) указаииого продукта с т. пл. 109-110°С, Rf 0,68 (эфир : петролейный эфир 1 : 2).the catalyst is filtered off and washed with hot ethanol. The alcoholic solution is evaporated and 1.00 g (66%) of the title product with m.p. 109-110 ° C, Rf 0.68 (ether: petroleum ether 1: 2).
Найдено, %: С 79,83; 79,88; Н 8,66: 8,35; N 3,70; 3,73.Found,%: C 79.83; 79.88; H 8.66: 8.35; N 3.70; 3.73.
C25H3lN02.C25H3lN02.
Вычислено, .%: С 79,60; Н 8,27; N 3,70.Calculated,%: C 79.60; H 8.27; N 3.70.
Гидрохлорид получают с 97%-ным выходом обработкой основани эфирным раствором хлористого водорода. Он выдел етс в виде мелких бесцветных кристаллов с т. пл. 192-193°С (из этилацетата).The hydrochloride is obtained in 97% yield by treating the base with an ethereal solution of hydrogen chloride. It is isolated in the form of small, colorless crystals with a m.p. 192-193 ° C (from ethyl acetate).
Найдено, %: С 72,35; 72,67; Н 7,70; 7,71; N 3,24; 3,04; С1 18,40; 8,48.Found,%: C 72.35; 72.67; H 7.70; 7.71; N 3.24; 3.04; C1 18.40; 8.48.
C2 H32C1N02C2 H32C1N02
Вычислено, Calculated
С 72,53; Н 7,79; N 3,38; С1 8,56.C, 72.53; H 7.79; N 3.38; C1 8.56.
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU2018964A SU513973A1 (en) | 1974-04-19 | 1974-04-19 | The method of obtaining 1- (3 "-phenylpropene2" -yl) -2,5-dimethyl-4-phenyl-4-propionyloxypiperidine or its hydrochloride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU2018964A SU513973A1 (en) | 1974-04-19 | 1974-04-19 | The method of obtaining 1- (3 "-phenylpropene2" -yl) -2,5-dimethyl-4-phenyl-4-propionyloxypiperidine or its hydrochloride |
Publications (1)
Publication Number | Publication Date |
---|---|
SU513973A1 true SU513973A1 (en) | 1976-05-15 |
Family
ID=20582907
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU2018964A SU513973A1 (en) | 1974-04-19 | 1974-04-19 | The method of obtaining 1- (3 "-phenylpropene2" -yl) -2,5-dimethyl-4-phenyl-4-propionyloxypiperidine or its hydrochloride |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU513973A1 (en) |
-
1974
- 1974-04-19 SU SU2018964A patent/SU513973A1/en active
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