SU362786A1 - METHOD OF OBTAINING MAGNESIUM PHOSPHATE - Google Patents
METHOD OF OBTAINING MAGNESIUM PHOSPHATEInfo
- Publication number
- SU362786A1 SU362786A1 SU1483540A SU1483540A SU362786A1 SU 362786 A1 SU362786 A1 SU 362786A1 SU 1483540 A SU1483540 A SU 1483540A SU 1483540 A SU1483540 A SU 1483540A SU 362786 A1 SU362786 A1 SU 362786A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- magnesium phosphate
- obtaining magnesium
- phosphoric acid
- mgo
- temperature
- Prior art date
Links
Description
1one
Изобретение относитс к области получени соединений фосфора, в частности к способу нолучепи фосфата магни , который может найти применение в качестве св зующего.The invention relates to the field of the preparation of phosphorus compounds, in particular, to the method of the preparation of magnesium phosphate, which can be used as a binder.
Известен способ нолучепи фосфатов магни путем нейтрализации фосфорной кислоты окисью или гидроокисью магнн нри температуре 25-80°С при различных соотношени х PaOs и MgO.A known method for the accumulation of magnesium phosphates by neutralizing phosphoric acid with magnium oxide or hydroxide is at a temperature of 25-80 ° C at different ratios of PaOs and MgO.
С целью нолучени в зкого нродукта нредложено нагревание раствора вести нри температуре около 200°С в течение 20-30 мин до получени раствора в зкостью 35-40 пуаз.In order to obtain a viscous product, it is proposed to heat the solution at a temperature of about 200 ° C for 20-30 minutes until the solution has a viscosity of 35-40 poise.
Соотношение PsOs : MgO при нейтрализации термической фосфорной кислоты окисью или гидроокисью магни поддерживают в пределах 5-10: 1 нри концентрацнн кислоты 80-90%.The ratio of PsOs: MgO at neutralization of thermal phosphoric acid with oxide or magnesium hydroxide is maintained within the range of 5-10: 1 at a concentration of acid of 80-90%.
Пример. В трехгорлую колбу емкостью 0,5 л засынают 5,85 г гидроокиси магнии и вливают затем 78,6 мл терм11,ческой фосфорной кислоты удельного веса 1,72; соотношение P.205:MgO G: 1. Содержимое колбы нагревают нри носто нном перемешивании прн темнературе 100-110°С в течение 30 мин. Затем новышают температуру до 200-230°С и выдерживают раствор в течеиие 30 мин до нолучепи раствора в зкостью 35-40 пуаз. Получают смолоподобное полпмерное вещество .Example. In a three-necked flask with a capacity of 0.5 l, 5.85 g of magnesium hydroxide are injected into the flask and then 78.6 ml of thermal 11, chesic phosphoric acid with a specific gravity of 1.72; the ratio of P.205: MgO G: 1. The contents of the flask are heated by in situ stirring at a temperature of 100-110 ° C for 30 minutes. Then, the temperature is increased to 200–230 ° C and the solution is kept for 30 minutes until the solution reaches a viscosity of 35–40 poises. A gum-like half-dimensional substance is obtained.
Предмет изобретени Subject invention
1.Снособ нолучени фосфата магни нутем нейтралнзации фосфорной кислоты окисью или гидроокисью магнн нрн нагреваннн, нри1. The phosphate obtaining method by the magnitude of the neutralization of phosphoric acid by the oxide or hydroxide magnn hnn is heated, nr
соотношении MgO нор дка 5-10 : 1, отличающийс тем, что, с целью получени в зкого нродукта, нагревание ведут нрп темнературе около 200°С в течение 20-30 мин.a MgO ratio of 5-10: 1, characterized in that, in order to obtain a viscous product, heating is carried out at about 200 ° C for 20-30 minutes.
2.Снособ но и. 1, отлимающийсл тем, что берут термнческую фосфорную кислоту2.Snosob but and. 1, is tricked by taking thermal phosphoric acid
реактпвиой квалификации с коицентрацией 80-90%.reactor qualification with a concentration of 80-90%.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1483540A SU362786A1 (en) | 1970-10-12 | 1970-10-12 | METHOD OF OBTAINING MAGNESIUM PHOSPHATE |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1483540A SU362786A1 (en) | 1970-10-12 | 1970-10-12 | METHOD OF OBTAINING MAGNESIUM PHOSPHATE |
Publications (1)
Publication Number | Publication Date |
---|---|
SU362786A1 true SU362786A1 (en) | 1972-12-30 |
Family
ID=20458458
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU1483540A SU362786A1 (en) | 1970-10-12 | 1970-10-12 | METHOD OF OBTAINING MAGNESIUM PHOSPHATE |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU362786A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4650587A (en) * | 1982-09-09 | 1987-03-17 | Akzona Incorporated | Ammonia scavenger |
-
1970
- 1970-10-12 SU SU1483540A patent/SU362786A1/en active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4650587A (en) * | 1982-09-09 | 1987-03-17 | Akzona Incorporated | Ammonia scavenger |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Fluck et al. | Principles of phosphorus chemistry. VIII. Reorganization of triply connected monophosphorus compounds | |
GB1347074A (en) | Solid phosphoric acid catalyst and method of manufacture and use thereof | |
SU362786A1 (en) | METHOD OF OBTAINING MAGNESIUM PHOSPHATE | |
US2962354A (en) | Method for producing condensed phosphatesalts | |
US2583549A (en) | Preparation of pentaerythrityl phosphates | |
US1696975A (en) | Process for preparing fertilizer | |
GB937041A (en) | Preparation of triarylphosphates | |
Edwards et al. | The Mechanism of Formation of Sodium Triphosphate from Orthophosphate Mixtures1 | |
US2809171A (en) | Monoisopropylaminoborane polymers | |
SU432097A1 (en) | Method of producing trimetaphosphate | |
GB1298159A (en) | Manufacture of phosphorus pentafluoride | |
GB451359A (en) | Process for the manufacture of valuable products from boron fluoride and oxy-acids of phosphorus | |
US1336974A (en) | Manufacture of a boron derivative of pyrophosphoric acid | |
US3262961A (en) | Process for soluble sodium tetraborate inhibitors | |
SU414188A1 (en) | ||
SU434093A1 (en) | METHOD OF OBTAINING POLYMETALLOPHOSPHATES | |
Frame Jr | High Temperature Aggregation Reactions of Some Phosphorus (v) Compounds | |
SU149568A1 (en) | The method of producing siloxy phosphonitrile chloride | |
SU464564A1 (en) | Refractory mass | |
US1983588A (en) | Manufacture of triaryl phosphates | |
東節男 et al. | Studies on the Water-Settable Cement | |
SU415860A1 (en) | ||
HIGASHI et al. | Studies on the Water-Settable Cement Part 11. Preparatory Experiments on Water-settable Phosphate Cement and Properties of Water-settable Primary Calcium Phosphate | |
JPS6013879A (en) | Heat storing composition | |
US870962A (en) | Manufacture of a new material suitable for use in dentistry. |