SU362786A1 - METHOD OF OBTAINING MAGNESIUM PHOSPHATE - Google Patents

METHOD OF OBTAINING MAGNESIUM PHOSPHATE

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Publication number
SU362786A1
SU362786A1 SU1483540A SU1483540A SU362786A1 SU 362786 A1 SU362786 A1 SU 362786A1 SU 1483540 A SU1483540 A SU 1483540A SU 1483540 A SU1483540 A SU 1483540A SU 362786 A1 SU362786 A1 SU 362786A1
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SU
USSR - Soviet Union
Prior art keywords
magnesium phosphate
obtaining magnesium
phosphoric acid
mgo
temperature
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Application number
SU1483540A
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Russian (ru)
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Publication date
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Priority to SU1483540A priority Critical patent/SU362786A1/en
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Publication of SU362786A1 publication Critical patent/SU362786A1/en

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Изобретение относитс  к области получени  соединений фосфора, в частности к способу нолучепи  фосфата магни , который может найти применение в качестве св зующего.The invention relates to the field of the preparation of phosphorus compounds, in particular, to the method of the preparation of magnesium phosphate, which can be used as a binder.

Известен способ нолучепи  фосфатов магни  путем нейтрализации фосфорной кислоты окисью или гидроокисью магнн  нри температуре 25-80°С при различных соотношени х PaOs и MgO.A known method for the accumulation of magnesium phosphates by neutralizing phosphoric acid with magnium oxide or hydroxide is at a temperature of 25-80 ° C at different ratios of PaOs and MgO.

С целью нолучени  в зкого нродукта нредложено нагревание раствора вести нри температуре около 200°С в течение 20-30 мин до получени  раствора в зкостью 35-40 пуаз.In order to obtain a viscous product, it is proposed to heat the solution at a temperature of about 200 ° C for 20-30 minutes until the solution has a viscosity of 35-40 poise.

Соотношение PsOs : MgO при нейтрализации термической фосфорной кислоты окисью или гидроокисью магни  поддерживают в пределах 5-10: 1 нри концентрацнн кислоты 80-90%.The ratio of PsOs: MgO at neutralization of thermal phosphoric acid with oxide or magnesium hydroxide is maintained within the range of 5-10: 1 at a concentration of acid of 80-90%.

Пример. В трехгорлую колбу емкостью 0,5 л засынают 5,85 г гидроокиси магнии и вливают затем 78,6 мл терм11,ческой фосфорной кислоты удельного веса 1,72; соотношение P.205:MgO G: 1. Содержимое колбы нагревают нри носто нном перемешивании прн темнературе 100-110°С в течение 30 мин. Затем новышают температуру до 200-230°С и выдерживают раствор в течеиие 30 мин до нолучепи  раствора в зкостью 35-40 пуаз. Получают смолоподобное полпмерное вещество .Example. In a three-necked flask with a capacity of 0.5 l, 5.85 g of magnesium hydroxide are injected into the flask and then 78.6 ml of thermal 11, chesic phosphoric acid with a specific gravity of 1.72; the ratio of P.205: MgO G: 1. The contents of the flask are heated by in situ stirring at a temperature of 100-110 ° C for 30 minutes. Then, the temperature is increased to 200–230 ° C and the solution is kept for 30 minutes until the solution reaches a viscosity of 35–40 poises. A gum-like half-dimensional substance is obtained.

Предмет изобретени Subject invention

1.Снособ нолучени  фосфата магни  нутем нейтралнзации фосфорной кислоты окисью или гидроокисью магнн  нрн нагреваннн, нри1. The phosphate obtaining method by the magnitude of the neutralization of phosphoric acid by the oxide or hydroxide magnn hnn is heated, nr

соотношении MgO нор дка 5-10 : 1, отличающийс  тем, что, с целью получени  в зкого нродукта, нагревание ведут нрп темнературе около 200°С в течение 20-30 мин.a MgO ratio of 5-10: 1, characterized in that, in order to obtain a viscous product, heating is carried out at about 200 ° C for 20-30 minutes.

2.Снособ но и. 1, отлимающийсл тем, что берут термнческую фосфорную кислоту2.Snosob but and. 1, is tricked by taking thermal phosphoric acid

реактпвиой квалификации с коицентрацией 80-90%.reactor qualification with a concentration of 80-90%.

SU1483540A 1970-10-12 1970-10-12 METHOD OF OBTAINING MAGNESIUM PHOSPHATE SU362786A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU1483540A SU362786A1 (en) 1970-10-12 1970-10-12 METHOD OF OBTAINING MAGNESIUM PHOSPHATE

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU1483540A SU362786A1 (en) 1970-10-12 1970-10-12 METHOD OF OBTAINING MAGNESIUM PHOSPHATE

Publications (1)

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SU362786A1 true SU362786A1 (en) 1972-12-30

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Country Link
SU (1) SU362786A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4650587A (en) * 1982-09-09 1987-03-17 Akzona Incorporated Ammonia scavenger

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4650587A (en) * 1982-09-09 1987-03-17 Akzona Incorporated Ammonia scavenger

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