SU339041A1 - - Google Patents
Info
- Publication number
- SU339041A1 SU339041A1 SU1358679A SU1358679A SU339041A1 SU 339041 A1 SU339041 A1 SU 339041A1 SU 1358679 A SU1358679 A SU 1358679A SU 1358679 A SU1358679 A SU 1358679A SU 339041 A1 SU339041 A1 SU 339041A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acids
- mixture
- methanol
- heated
- water
- Prior art date
Links
- 239000000284 extract Substances 0.000 claims description 23
- 239000002253 acid Substances 0.000 claims description 22
- 150000002632 lipids Chemical class 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 150000007513 acids Chemical class 0.000 claims description 18
- 238000009835 boiling Methods 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 7
- 150000001735 carboxylic acids Chemical class 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 5
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000002028 Biomass Substances 0.000 claims description 3
- 230000002378 acidificating effect Effects 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000002955 isolation Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 239000011261 inert gas Substances 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 51
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 37
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 27
- 239000000203 mixture Substances 0.000 description 19
- 239000000194 fatty acid Substances 0.000 description 17
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 16
- 235000014113 dietary fatty acids Nutrition 0.000 description 16
- 229930195729 fatty acid Natural products 0.000 description 16
- 150000004665 fatty acids Chemical class 0.000 description 16
- 238000004821 distillation Methods 0.000 description 14
- 239000007789 gas Chemical class 0.000 description 14
- 238000010992 reflux Methods 0.000 description 14
- 238000006386 neutralization reaction Methods 0.000 description 11
- 238000000605 extraction Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 244000005700 microbiome Species 0.000 description 5
- 239000012299 nitrogen atmosphere Substances 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 239000010410 layer Substances 0.000 description 4
- 239000002609 medium Substances 0.000 description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 210000005253 yeast cell Anatomy 0.000 description 4
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 235000019387 fatty acid methyl ester Nutrition 0.000 description 3
- 235000015097 nutrients Nutrition 0.000 description 3
- 239000012044 organic layer Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000004165 Methyl ester of fatty acids Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 241000222120 Candida <Saccharomycetales> Species 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 244000285963 Kluyveromyces fragilis Species 0.000 description 1
- 235000014663 Kluyveromyces fragilis Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- GHVZOJONCUEWAV-UHFFFAOYSA-N [K].CCO Chemical compound [K].CCO GHVZOJONCUEWAV-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- WGXZDYPGLJYBJW-UHFFFAOYSA-N chloroform;propan-2-ol Chemical compound CC(C)O.ClC(Cl)Cl WGXZDYPGLJYBJW-UHFFFAOYSA-N 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- DJFTXJLLHZRHKO-UHFFFAOYSA-N dipotassium oxygen(2-) hydrate Chemical compound O.[O--].[K+].[K+] DJFTXJLLHZRHKO-UHFFFAOYSA-N 0.000 description 1
- 239000012259 ether extract Substances 0.000 description 1
- MDKXBBPLEGPIRI-UHFFFAOYSA-N ethoxyethane;methanol Chemical compound OC.CCOCC MDKXBBPLEGPIRI-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU339041A1 true SU339041A1 (enrdf_load_html_response) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2058298C1 (ru) | Способ получения сложных эфиров жирных кислот | |
| US20080015367A1 (en) | Process for isolating phytosterols and tocopherols from deodorizer distillate | |
| CA2822314C (en) | Concentrate of omega 3 | |
| JP2019137687A (ja) | 魚油のコレステロール | |
| JP2010516627A (ja) | 飽和及び不飽和脂肪酸の分離方法 | |
| KR20080036107A (ko) | 카르복실레이트 알킬 에스테르의 제조 방법 | |
| JP2016222926A (ja) | 残留植物油ストリームからの植物性ステロールの再生 | |
| GB2152043A (en) | Method of preparing fatty acid composition containing high concentration of eicosapentaenoic acid | |
| Abdullah et al. | Algae oil extraction from freshwater microalgae Chlorella vulgaris | |
| US5371245A (en) | Recovery of tocopherols from plant and animal oils | |
| SU339041A1 (enrdf_load_html_response) | ||
| CN108026502B (zh) | 用于浓缩包含产油酵母的粘质生物质的细胞悬液的方法 | |
| CA1264477A (en) | Plant growth promotor from rice bran fatty acid distillation residue and a process for the isolation thereof and the preparation of a composition containing the same | |
| US2729655A (en) | Production of sterols | |
| RU2439093C1 (ru) | Способ химической переработки березовой коры с выделением таких продуктов как бетулин и суберин | |
| US3342876A (en) | Process for the isolation of alphaglyceryl ethers from marine oils | |
| RU2385900C1 (ru) | Способ получения жидкого биотоплива | |
| EP1226156B1 (en) | Process for producing phytosterols by saponification in an alcohol/water solvent | |
| JPS60155143A (ja) | 天然ロウからの脂肪族高級アルコ−ルの分離法 | |
| WO1994021766A1 (en) | Process for separating docosahexaenoic acid or ester thereof from marine microalgae | |
| NO132937B (enrdf_load_html_response) | ||
| US7087402B2 (en) | Selective transesterification of stanols in mixtures comprising sterols and stanols | |
| JP3807688B2 (ja) | 乾燥レシチンの製造方法 | |
| US2809205A (en) | Production of ustilic acids | |
| RU2464035C1 (ru) | Способ получения борнеола из отходов экстрактивных веществ древесной зелени пихты |