SU1578093A1 - Vitreous slip for ceramic capacitors - Google Patents
Vitreous slip for ceramic capacitors Download PDFInfo
- Publication number
- SU1578093A1 SU1578093A1 SU874318508A SU4318508A SU1578093A1 SU 1578093 A1 SU1578093 A1 SU 1578093A1 SU 874318508 A SU874318508 A SU 874318508A SU 4318508 A SU4318508 A SU 4318508A SU 1578093 A1 SU1578093 A1 SU 1578093A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- slip
- frit
- gluing
- methylcellulose
- ceramic capacitors
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Capacitors (AREA)
- Glass Compositions (AREA)
Abstract
Изобретение относитс к процессам склейки керамических изделий, в частности к составам глазурных шликеров. Целью изобретени вл етс исключение растекаемости и повышение за счет этого выхода годных блоков. Шликер включает фритту состава, мас.%: BI 2O 3 65-71The invention relates to the processes of gluing ceramic products, in particular to the compositions of glaze slips. The aim of the invention is to eliminate spreadability and increase due to this release of usable blocks. The slip includes a Frit composition, wt.%: BI 2O 3 65-71
ZNO 4,5-15ZNO 4.5-15
B 2O 3 4,5-8B 2O 3 4.5-8
CUO 0,5-1,5CUO 0.5-1.5
SIO 2 4-19SIO 2 4-19
CAO 1,5-5,5. Дл достижени цели шликер содержит следующие компоненты, мас.%: указанна фрита 70-80CAO 1.5-5.5. To achieve the goal, the slip contains the following components, wt%: indicated frit 70-80
метилцеллюлоза 0,2-1,2methylcellulose 0.2-1.2
вода 19,8-28,8. Шликер обеспечивает прочность клеевого узла 50-55 кг/мм 2 при температуре 600-700°С и времени склейки 5-15 мин. Потери на склейке составл ют 3-7%. 2 табл.water 19.8-28.8. The slip provides the glue unit strength of 50-55 kg / mm 2 at a temperature of 600-700 ° C and a gluing time of 5-15 minutes. Gluing loss is 3-7%. 2 tab.
Description
Изобретение относитс к процессам склейки керамических изделий, в частности к составам глазурных шликеров, предназначенных дл получени стекловидных клеевых узлов, и может быть использовано, в конденсаторостроении дл автоматизированной склейки конденсаторных пакетов в блок.The invention relates to processes for gluing ceramic products, in particular, to glaze slurry compositions intended for producing glassy glue assemblies, and can be used in capacitor manufacturing for the automatic gluing of capacitor packages into a block.
Целью изобретени вл етс исключение растекаемости и повышение за счет этого выхода годных блоков.The aim of the invention is to eliminate spreadability and increase due to this release of usable blocks.
Глазурный шликер получают следующим образом.Glaze slip is obtained as follows.
Предварительно известным образом приготавливают стекл нную фритту заданного состава. Дл этого компоненты фритты, вз тые в за вл емом соотношении , смешивают друг с другом, а полученную смесь подвергают варке при 950°С и последующему измельчению способом мокрого помола на шаровых мельницих в течение 24-48 ч до удельной поверхности 2000-3000 см2/г. В полученную таким образом смесь добавл ют требуемое количество водного раствора метилцеллюлозы и тшательно перемешивают на валковой мельнице в течение 2-3 ч до образовани однородной суспензии. Готовый глазурный шликер примен ют дл склейки пакетов керамических конденсаторов в единый : блок в автоматизированном режиме при температурах оплавлени 600-700°С в течение 5-15 мин. Затем полученные i конденсаторные блоки по прин тому в конденсаторостроении процессу подг вергают лужению по контактным поверхност м (торцам).A glass frit of a given composition is prepared in a previously known manner. For this, the components of the frit, taken in the stated ratio, are mixed with each other, and the resulting mixture is subjected to boiling at 950 ° C and subsequent grinding by wet grinding in ball mills for 24-48 hours to a specific surface of 2000-3000 cm2 / year The required amount of an aqueous solution of methylcellulose is added to the mixture thus obtained and mixed thoroughly in a roller mill for 2 to 3 hours until a homogeneous suspension is formed. The finished glaze slip is used for gluing together packages of ceramic capacitors into a single unit: an automated unit at a reflux temperature of 600-700 ° C for 5-15 minutes. Then, the obtained i capacitor units, received by the process in condenser construction, are tinned on the contact surfaces (ends).
В данном случае стеклофритта вл етс основой шликера, обеспечивающей оплавление и склейку при 600-700°С, а метилцеллюлоза стабилизирует снижение растекаемости при оплавлении и повышает пригодность глазурногоIn this case, glass frit is the basis of the slip, which provides melting and gluing at 600-700 ° C, and methylcellulose stabilizes the decrease in flowability during melting and increases the suitability of glaze
(Л(L
сwith
ел 1ate 1
0000
о соabout with
0000
шликера в случае автоматизированного процесса склейки.slip in the case of an automated gluing process.
Готов т составы шликеров, обладающие оптимальными свойствами, которые приведены в табл.1.Preparing slurry compositions with optimal properties, which are listed in Table 1.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU874318508A SU1578093A1 (en) | 1987-08-26 | 1987-08-26 | Vitreous slip for ceramic capacitors |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU874318508A SU1578093A1 (en) | 1987-08-26 | 1987-08-26 | Vitreous slip for ceramic capacitors |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1578093A1 true SU1578093A1 (en) | 1990-07-15 |
Family
ID=21332523
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU874318508A SU1578093A1 (en) | 1987-08-26 | 1987-08-26 | Vitreous slip for ceramic capacitors |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU1578093A1 (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996022255A1 (en) * | 1995-01-16 | 1996-07-25 | Cookson Group Plc | Sealing glass paste |
| WO1997036836A1 (en) * | 1996-04-02 | 1997-10-09 | Techneglas, Inc. | Sealing glass modifier for use with voc-free or low-voc vehicle |
| EP0883580A4 (en) * | 1996-02-27 | 1999-03-31 | Corning Inc | Sealing glass suspension |
| WO2011002485A1 (en) * | 2009-06-30 | 2011-01-06 | Guardian Industries Corp. | Non-toxic water-based frit paste, and assembly incorporating the same |
| US8733128B2 (en) | 2011-02-22 | 2014-05-27 | Guardian Industries Corp. | Materials and/or method of making vacuum insulating glass units including the same |
| US8802203B2 (en) | 2011-02-22 | 2014-08-12 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
| US9290408B2 (en) | 2011-02-22 | 2016-03-22 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
| US9309146B2 (en) | 2011-02-22 | 2016-04-12 | Guardian Industries Corp. | Vanadium-based frit materials, binders, and/or solvents and methods of making the same |
| US9359247B2 (en) | 2011-02-22 | 2016-06-07 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US9458052B2 (en) | 2011-02-22 | 2016-10-04 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US9593527B2 (en) | 2014-02-04 | 2017-03-14 | Guardian Industries Corp. | Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same |
| US9822580B2 (en) | 2011-02-22 | 2017-11-21 | Guardian Glass, LLC | Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same |
| US9988302B2 (en) | 2014-02-04 | 2018-06-05 | Guardian Glass, LLC | Frits for use in vacuum insulating glass (VIG) units, and/or associated methods |
-
1987
- 1987-08-26 SU SU874318508A patent/SU1578093A1/en active
Non-Patent Citations (1)
| Title |
|---|
| Авторское свидетельство СССР № 1252310, кл. С 03 С 8/16, 1984. Авторское свидетельство СССР № 1488269, кл. .С 03 С 8/16, 1988. * |
Cited By (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996022255A1 (en) * | 1995-01-16 | 1996-07-25 | Cookson Group Plc | Sealing glass paste |
| EP0883580A4 (en) * | 1996-02-27 | 1999-03-31 | Corning Inc | Sealing glass suspension |
| WO1997036836A1 (en) * | 1996-04-02 | 1997-10-09 | Techneglas, Inc. | Sealing glass modifier for use with voc-free or low-voc vehicle |
| US9428416B2 (en) | 2009-06-30 | 2016-08-30 | Guardian Industries Corp. | Non-toxic water-based frit slurry paste, and assembly incorporating the same |
| WO2011002485A1 (en) * | 2009-06-30 | 2011-01-06 | Guardian Industries Corp. | Non-toxic water-based frit paste, and assembly incorporating the same |
| EP2448876A1 (en) * | 2009-06-30 | 2012-05-09 | Guardian Industries Corp. | Non-toxic water-based frit paste, and assembly incorporating the same |
| CN102510842A (en) * | 2009-06-30 | 2012-06-20 | 格尔德殿工业公司 | Non-toxic water-based frit paste, and assembly incorporating the same |
| US8668798B2 (en) | 2009-06-30 | 2014-03-11 | Guardian Industries Corp. | Non-toxic water-based frit slurry paste, and assembly incorporating the same |
| CN106242284A (en) * | 2009-06-30 | 2016-12-21 | 格尔德殿工业公司 | Non-toxic water Frit paste and comprise its assembly |
| CN102510842B (en) * | 2009-06-30 | 2016-08-31 | 格尔德殿工业公司 | Non-toxic water Frit paste and comprise its assembly |
| US9458052B2 (en) | 2011-02-22 | 2016-10-04 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US11028009B2 (en) | 2011-02-22 | 2021-06-08 | Guardian Glass, LLC | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US9309146B2 (en) | 2011-02-22 | 2016-04-12 | Guardian Industries Corp. | Vanadium-based frit materials, binders, and/or solvents and methods of making the same |
| US9290408B2 (en) | 2011-02-22 | 2016-03-22 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
| US8802203B2 (en) | 2011-02-22 | 2014-08-12 | Guardian Industries Corp. | Vanadium-based frit materials, and/or methods of making the same |
| US8733128B2 (en) | 2011-02-22 | 2014-05-27 | Guardian Industries Corp. | Materials and/or method of making vacuum insulating glass units including the same |
| US9359247B2 (en) | 2011-02-22 | 2016-06-07 | Guardian Industries Corp. | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US9776910B2 (en) | 2011-02-22 | 2017-10-03 | Guardian Glass, LLC | Vanadium-based frit materials, and/or methods of making the same |
| US9822580B2 (en) | 2011-02-22 | 2017-11-21 | Guardian Glass, LLC | Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same |
| US10752535B2 (en) | 2011-02-22 | 2020-08-25 | Guardian Glass, LLC | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US10087676B2 (en) | 2011-02-22 | 2018-10-02 | Guardian Glass, LLC | Vanadium-based frit materials, and/or methods of making the same |
| US10107028B2 (en) | 2011-02-22 | 2018-10-23 | Guardian Glass, LLC | Method of making vacuum insulated glass (VIG) window unit |
| US10125045B2 (en) | 2011-02-22 | 2018-11-13 | Guardian Glass, LLC | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US10196299B2 (en) | 2011-02-22 | 2019-02-05 | Guardian Glass, LLC | Vanadium-based frit materials, and/or methods of making the same |
| US10329187B2 (en) | 2011-02-22 | 2019-06-25 | Guardian Glass, LLC | Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same |
| US11014847B2 (en) | 2011-02-22 | 2021-05-25 | Guardian Glass, LLC | Vanadium-based frit materials, and/or methods of making the same |
| US10858880B2 (en) | 2011-02-22 | 2020-12-08 | Guardian Glass, LLC | Vanadium-based frit materials, binders, and/or solvents and/or methods of making the same |
| US9593527B2 (en) | 2014-02-04 | 2017-03-14 | Guardian Industries Corp. | Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same |
| US10465433B2 (en) | 2014-02-04 | 2019-11-05 | Guardian Glass, Llc. | Vacuum insulating glass (VIG) unit with lead-free dual-frit seals and/or methods of making the same |
| US10421684B2 (en) | 2014-02-04 | 2019-09-24 | Guardian Glass, LLC | Frits for use in vacuum insulating glass (VIG) units, and/or associated methods |
| US9988302B2 (en) | 2014-02-04 | 2018-06-05 | Guardian Glass, LLC | Frits for use in vacuum insulating glass (VIG) units, and/or associated methods |
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