SU1437413A1 - Composition for applying phosphate-lubricant coatings - Google Patents
Composition for applying phosphate-lubricant coatings Download PDFInfo
- Publication number
- SU1437413A1 SU1437413A1 SU874173370A SU4173370A SU1437413A1 SU 1437413 A1 SU1437413 A1 SU 1437413A1 SU 874173370 A SU874173370 A SU 874173370A SU 4173370 A SU4173370 A SU 4173370A SU 1437413 A1 SU1437413 A1 SU 1437413A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosphate
- fatty acids
- acid
- synthetic fatty
- primary
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/02—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using non-aqueous solutions
- C23C22/03—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using non-aqueous solutions containing phosphorus compounds
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
Abstract
Изобретение относитс к подготовке поверхности металлов дл холодной обработки давлением и может быть использовано в металлургической и машиностроительной пpo iЫIuлeннocтlI. Цель изобретени - повышение массы фосфатного покрыти ,антифрикционных и противозадирных свойств. Состав содержит ,мае, %: полифосфорна кислота 3-10, фосфат железа (TII) 0,1- 1,0; первичные етфные спирты 10-18; синтетические жирные кислоты 16-25,; вода 0,5-10,0; моноэтанолаьшды синтетических жирных кислот 3-15, кар- боксиметилделлюлоза 0,001-0,010; ni- неральное масло - остальное. Повышение массы фосфатного покрыти , антифрикционных и противозадирных свойств достигаетс путем дополнительного введени моноэтаноламидов синтетических жирных кисотот и карбоксиметил- целлюлозы. 1 табл. со (ЛThe invention relates to the preparation of the surface of metals for cold forming and can be used in the metallurgical and engineering industry iYi alentostI. The purpose of the invention is to increase the mass of phosphate coating, anti-friction and extreme pressure properties. The composition contains, in May,%: polyphosphoric acid 3-10, iron phosphate (TII) 0.1-1.0; primary etfny alcohols 10-18; synthetic fatty acids 16-25; water 0.5-10.0; monoethanol with synthetic fatty acids 3-15, carboxymethylcellulose 0.001-0.010; ni- neral oil - the rest. An increase in the mass of the phosphate coating, antifriction and extreme pressure properties is achieved by additionally introducing synthetic fatty acid monoethanolamides and carboxymethylcellulose. 1 tab. with (L
Description
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И обретепие отмогитсг; : rn i.u стоп- ке поверхности ic i-a:i;;rii-: ; . х;)Л о,гм; 1Й обработки даи.С й i -,, ii{:iy;:y rir TJ. IL(: пользовано в ieraллypi-ичf ::; r : ir iijHHocTponTej-ibHCH ггромьшигг .And gaining money; : rn i.u the stack of the surface ic i-a: i ;; rii-:; . x;) Oh, um; 1Y processing dai.S th i - ,, ii {: iy;: y rir TJ. IL (: used in ierallpi-ichf ::; r: ir iijHHocTponTej-ibHCH gromomshigg.
M :U:if Tt TPf HH - 1( ссы фосфатного rrri obiTtw, пити-ррртк гтоии - :; и противоза ;крньгх спойсть , M: U: if Tt TPf HH - 1 (sss phosphate rrri obiTtw, pit-rrttk gtoii -:; and counter-exposure; protection,
Изобретение иллюстриру /с : ела/;;; примераг-П Invention illustrative / s: ate / ;;; example-P
Лп полз чеии состава -Ьйсф - за (III) раствор ли в пол-гфосфоркой кислоте при 120-l50 C в т ;т: ение 2/- 40 при г;с-;аз.л ;ли первичньш жирные спирть;; ; скесь ъ-л-- лерживали при этой темпер /гут е Т5 - --- чение 1j5--2 ч, Затем доб;-;-.л .п -; оС тальные компоненть.Lp crawl of the composition of the Bisf - for (III) solution was dissolved in half-phosphoric acid at 120-150 C in t; t: 2 / - 40 at g; s-; az.l; whether primary fatty alcohol ;; ; skid l –– were kept at this temperature / g e e T5 - --- 1 h 5–2 h, then ext; -; - l. n -; Other components.
В качестве фосфата желзза (LII; использовали фосфатный пгл ь;. зл ю-дий с отходом производства т; метг ллур гт;- ческой поомьппгенкости и с:;дерзгаи1 й в своем составе Д8 i--iac,% гюсфата железа (HI), 22% фосфата ;-,;-;н; :а нAs a phosphate of iron (LII; used phosphate pgl;; evil sludge with production waste t; metgllu rt; - cheskoy poomppgenkosti and with:; bold; in its composition D8 i - iac,% of iron (HI) , 22% phosphate; -,; -; n;: a n
около 20% ОрТОфОСфорИО : КтГЛО ЫПерзичнь е )тл;пнь е рь-бкралг-: из р да стп-:;ртов, со;1,.--;; , 0--2о атомов уг.;еро.а „about 20% of Ortofosporio: KTGLO YPerzichn (e) tl; phni rb-braklg-: from r yes stp -:; mouths, with; 1, .-- ;; , 0--2o atoms of angles; ero.a „
Мкнеральное масло выбирали иэ р - да масел5 и iefoщиx кикема тческую кость 10-150 сСт npir К jcaqecT- ве син гети еекик й;иркнх K: ;CJ;O I- ис-- пользовали ( фракций С , ,,, или фракции С f, J и пъппс „The core oil was chosen as the p - yes of the oils5 and ie of the crusty bone of 10-150 cSt npir K jcaqecT - ve sin geti ekiks y; irks K:; CJ; O I- used (fractions C, ,,, or fractions C f, J and ppps „
Пластины р;з стали 08KI; обе ::жир :- - валн травлеш-1ем к i5% -HGt- расггпоре серной кислоты промыва.ги5 , обрабатывали в смазочном состаг;::; нри /О Массу фосфата o:roeдeл и весо ;л ; методом nocjie сн ти смаз:;14}1ого сло в среде Изонро:п-1лового c;: -i vra AHTSI- фрикц5-1онные свойства , сост.Илов оце:Н1-г-- вали но усилрт м волочени образцов проволоки из. с гали 45, cj njfi6c T aHH ii.; таким же обра.зом„ и ,, на разрывной ;aIпинe Р--0;; у ХХЛ 785-i 74), моделируБщгй основкь -- холодной деформациг ;цро;: о;::и, Иоло чение o6pf;:;iTi,ofi ;трово::оки /. етроь; 1,7 М1Ч проводил: {; спо.;1Ь;;:Сл:а кп а:ч- твердосплавных волок :;о марагр.. ; - 1,5-1,3-1 „1-0,98- 0„88. 1ротгапозйли1. свойства c;ocTai-;o:i ;)це -(1иии;и -la i iainHHe трешш 2070 СМ . vo числу оборотов o6pa; ua до резко о ,г1ИчеPlates p; h steel 08KI; Both: Fat: - - Valn travlesh-1em to i5% -HGt- wash sulfuric acid rinsea.gi, treated in a lubricant deposit; ::; NR / O Mass of phosphate o: rodedel and weight; l; using the nocjie method of removing the lubricant:; 14} of the 1st layer in the medium of Isonro: n-1 c ;: -i vra AHTSI- friccs 5-1-ion properties, condition. Filter: H1-g - but reinforced drawing wire samples from. Gali 45, cj njfi6c T aHH ii .; in the same way "and ,, on a discontinuous; aIpine P - 0 ;; in the HHL 785-i 74), the model basis is cold deformation; red ;: о; :: и, Иолоеение o6pf;:; iTi, ofi; trovo :: oki /. the wind; 1.7 M1CH spent: {; sp.; 1b ;;: Sl: a kp a: h - hard-alloyed fibers:; o maragr ..; - 1.5-1.3-1 "1-0.98-0" 88. 1HG properties c; ocTai-; o: i;) tse - (1iii; and -la i iainHHe thrash 2070 CM. vo revolutions o6pa; ua to sharply o, r1Iche
л:1 |мел-| п трени , ;1л исп, ; : ; iyi/iiiHppH f:Cj-a-ie оара:;;:,ь1 из ста/и; -и ,; -ia;ierpoi-; ц О М;- с: образлиощей ; О F-fM ,|нали п г ыигеука занной техпоПОГГИ . ;-;а v;;ii;a,: : ИХ ГфЯВОДИЛИ в l: 1 | chalk- | n friction,; 1l sp, :; iyi / iiiHppH f: Cj-a-ie oara: ;;:, 1 out of a hundred / s; s -ia; ierpoi-; C O M; - with: the image; About F-fM, | ; -; a v ;; ii; a ,:: THEIR CONFINED THEY
кгаагакт по :;бразую:цим с Е1еобработан- ;i;,iM оГфазцо - ,, Прижимаюиа агрузка ii. Образцы приводили во вращение ;7ричем иснЬгТуемый образен, имел частого npaiueHH .q 500 об/мин Коэффициент ироск ии зычани пары трени 15%. При исаьта ;;и х замер ли момент трени на налу и ч;исло о опотов до задира испы ч; -;ог--о образца В качестве критери :нрактеризую п:е: о п эотивозадирные стзс:йства смазоч:ных составов,, выбрано 4i:t.jio оборотов образца до резкого У 1е/п-1че1 и моке;п-а трени , т,е. доkaagakt on:; brazuyu: zim with E1eobrabotan-; i;, iM oGfaztso- ,, Prisyamuyaia load ii. Samples were put into rotation; 7, which is energy-efficient, had a frequency of npaiueHH 500 r / min. When Isat ;; and x, the moment of friction on the bench and the h; -; og - o sample As a criterion: practical i n: e: o n erotivozadirnye stzs: properties of lubricant compositions, 4i were selected: t.jio sample turns to sharp U 1e / n-1ч1 and moke; training, t, e. before
Результаты 1- спытаний приведены в таблице,The results of 1 tests are given in the table.
ехнико-зкономическим;- преимущест вам состава вл ютс повьт ение масс фосфатного покрыти , антифрикционных и ггротивозадирных свойств. - The advantages of the composition are the upwelling of the phosphate coating mass, anti-friction and anti-scuff properties.
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU874173370A SU1437413A1 (en) | 1987-01-04 | 1987-01-04 | Composition for applying phosphate-lubricant coatings |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU874173370A SU1437413A1 (en) | 1987-01-04 | 1987-01-04 | Composition for applying phosphate-lubricant coatings |
Publications (1)
Publication Number | Publication Date |
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SU1437413A1 true SU1437413A1 (en) | 1988-11-15 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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SU874173370A SU1437413A1 (en) | 1987-01-04 | 1987-01-04 | Composition for applying phosphate-lubricant coatings |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0813619A4 (en) * | 1995-02-24 | 1998-05-20 | Mdechem Inc | Method of preparing iron-phosphate conversion surfaces |
WO1999021946A1 (en) * | 1997-10-29 | 1999-05-06 | Metallgesellschaft Aktiengesellschaft | Regeneration of acid reaction lubricant residues |
-
1987
- 1987-01-04 SU SU874173370A patent/SU1437413A1/en active
Non-Patent Citations (1)
Title |
---|
Патент DE (f 1204913, кл. С 23 F 7-/08, 1965. Патент DE 2102295, кл. С 10 М 7/44, 1971. * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0813619A4 (en) * | 1995-02-24 | 1998-05-20 | Mdechem Inc | Method of preparing iron-phosphate conversion surfaces |
WO1999021946A1 (en) * | 1997-10-29 | 1999-05-06 | Metallgesellschaft Aktiengesellschaft | Regeneration of acid reaction lubricant residues |
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