SU137915A1 - The method of producing mercaptol - Google Patents

The method of producing mercaptol

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Publication number
SU137915A1
SU137915A1 SU671173A SU671173A SU137915A1 SU 137915 A1 SU137915 A1 SU 137915A1 SU 671173 A SU671173 A SU 671173A SU 671173 A SU671173 A SU 671173A SU 137915 A1 SU137915 A1 SU 137915A1
Authority
SU
USSR - Soviet Union
Prior art keywords
producing
mercaptol
mercaptols
mercaptans
known methods
Prior art date
Application number
SU671173A
Other languages
Russian (ru)
Inventor
А.В. Богданова
А.Н. Долгих
Г.И. Плотникова
М.Ф. Шостаковский
Original Assignee
А.В. Богданова
А.Н. Долгих
Г.И. Плотникова
М.Ф. Шостаковский
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by А.В. Богданова, А.Н. Долгих, Г.И. Плотникова, М.Ф. Шостаковский filed Critical А.В. Богданова
Priority to SU671173A priority Critical patent/SU137915A1/en
Application granted granted Critical
Publication of SU137915A1 publication Critical patent/SU137915A1/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Description

Способ  вл етс  более простым по. сравнению с известными способами получени  меркаптолов, так как известные способы осуществл ютс  в токе сухого НС илИ не дают хороших выходов.The method is more simple. compared with the known methods for producing mercaptols, since the known methods are carried out in a stream of dry HCI or do not give good yields.

Пример. Смесь из 5 г диэтилкетал  ацетона и 5 г этилмеркаптана нагревают в запа нной ампуле в течение 6 час при 120-130°. Разгонкой в вакууме выдел ют 5,1 г диэтилмеркаптола ацетал , который после повторной перегонки имеет следующие константы:Example. A mixture of 5 g diethyl ketal acetone and 5 g ethyl mercaptan is heated in a sealed ampoule for 6 hours at 120–130 °. 5.1 g of diethyl mercaptol acetal is isolated by distillation in vacuum, which, after repeated distillation, has the following constants:

т. кип. 77,5 -78°(16 мм, л| 1,4950; rf 0,9460. Найдено в %: С 51,21 и 51,17; Н- 9,72 и 9,84; S 38,80 и 38,73; C/HieSa вычислено %: С 51,17; Н 9,82; 5 39,03.m.p. 77.5 -78 ° (16 mm, l | 1.4950; rf 0.9460. Found in%: C 51.21 and 51.17; H- 9.72 and 9.84; S 38.80 and 38 , 73; C / HieSa calculated%: C 51.17; H 9.82; 5 39.03.

Способ получени  меркаптолов из меркаптанов, отличающийс  тем, что, с целью упрощени  процесса, меркаптаны подвергают взаимодействию с кетал ми.A method for producing mercaptols from mercaptans, characterized in that, in order to simplify the process, mercaptans are reacted with ketals.

Предмет изобретени Subject invention

SU671173A 1960-06-23 1960-06-23 The method of producing mercaptol SU137915A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU671173A SU137915A1 (en) 1960-06-23 1960-06-23 The method of producing mercaptol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU671173A SU137915A1 (en) 1960-06-23 1960-06-23 The method of producing mercaptol

Publications (1)

Publication Number Publication Date
SU137915A1 true SU137915A1 (en) 1960-11-30

Family

ID=48294097

Family Applications (1)

Application Number Title Priority Date Filing Date
SU671173A SU137915A1 (en) 1960-06-23 1960-06-23 The method of producing mercaptol

Country Status (1)

Country Link
SU (1) SU137915A1 (en)

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