SU1363829A1 - Method of synthesis of d-(1-d-(1-h)-)-glucoseamine - Google Patents

Method of synthesis of d-(1-d-(1-h)-)-glucoseamine

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Publication number
SU1363829A1
SU1363829A1 SU3986820/04A SU3986820A SU1363829A1 SU 1363829 A1 SU1363829 A1 SU 1363829A1 SU 3986820/04 A SU3986820/04 A SU 3986820/04A SU 3986820 A SU3986820 A SU 3986820A SU 1363829 A1 SU1363829 A1 SU 1363829A1
Authority
SU
USSR - Soviet Union
Prior art keywords
product
glucoseamine
pdo
synthesis
carried out
Prior art date
Application number
SU3986820/04A
Other languages
Russian (ru)
Inventor
Г.П. Акулов
Ю.Л. Каминский
Е.В. Снеткова
Original Assignee
Г.П. Акулов
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Г.П. Акулов filed Critical Г.П. Акулов
Priority to SU3986820/04A priority Critical patent/SU1363829A1/en
Application granted granted Critical
Publication of SU1363829A1 publication Critical patent/SU1363829A1/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

FIELD: aminosugars. SUBSTANCE: synthesis is carried out by catalytic heterogeneous isotopic exchange between D-glucoseamine and gaseous tritium in phosphate buffer in the presence of catalyst - 5% PdO/PdO/AlOat pH value 5.8-6.0. Purification and desalting of the end product is carried out by thin layer chromatography method. Synthesized product has radiochemical purity 95% and molar activity 15-20 Cu/mmole that is 3-4 times more as compared with that of known preparation. EFFECT: increased molar radioactivity of product. 1 tbl
SU3986820/04A 1985-12-03 1985-12-03 Method of synthesis of d-(1-d-(1-h)-)-glucoseamine SU1363829A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU3986820/04A SU1363829A1 (en) 1985-12-03 1985-12-03 Method of synthesis of d-(1-d-(1-h)-)-glucoseamine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU3986820/04A SU1363829A1 (en) 1985-12-03 1985-12-03 Method of synthesis of d-(1-d-(1-h)-)-glucoseamine

Publications (1)

Publication Number Publication Date
SU1363829A1 true SU1363829A1 (en) 1994-08-15

Family

ID=60533714

Family Applications (1)

Application Number Title Priority Date Filing Date
SU3986820/04A SU1363829A1 (en) 1985-12-03 1985-12-03 Method of synthesis of d-(1-d-(1-h)-)-glucoseamine

Country Status (1)

Country Link
SU (1) SU1363829A1 (en)

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