SU1360130A1 - Method of producing 2-trit-butyl-peroxio-cycloalkanes - Google Patents

Method of producing 2-trit-butyl-peroxio-cycloalkanes

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Publication number
SU1360130A1
SU1360130A1 SU3762096/04K SU3762096K SU1360130A1 SU 1360130 A1 SU1360130 A1 SU 1360130A1 SU 3762096/04 K SU3762096/04 K SU 3762096/04K SU 3762096 K SU3762096 K SU 3762096K SU 1360130 A1 SU1360130 A1 SU 1360130A1
Authority
SU
USSR - Soviet Union
Prior art keywords
tert
butyl hydroperoxide
producing
oxacycloalkane
butyl
Prior art date
Application number
SU3762096/04K
Other languages
Russian (ru)
Inventor
А.М. Курдюков
Г.Н. Солодунова
М.Б. Изотова
Original Assignee
Волгоградский Политехнический Институт
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Волгоградский Политехнический Институт filed Critical Волгоградский Политехнический Институт
Application granted granted Critical
Publication of SU1360130A1 publication Critical patent/SU1360130A1/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1. Способ получения 2-трет-бутилпероксиоксациклоалканов общей формулыгде n=1, 2,взаимодействием соответствующего оксациклоалкана с гидроперекисью трет-бутила в присутствии неорганического хлорсодержащего соединения, отличающийся тем, что, с целью уменьшения потерь гидроперекиси трет-бутила и упрощения процесса, в качестве хлорсодержащего соединения используют хлористый сульфурил, который добавляют к смеси оксациклоалкана и гидроперекиси трет-бутила при 0-10C, после чего реакционную массу выдерживают при 18-22C в течение 0,7-1 ч, процесс ведут при молярном соотношении хлористого сульфурила, гидроперекиси трет-бутила и оксациклоалкана 1:(1,4-4):(3-12).2. Способ по п. 1, отличающийся тем, что процесс ведут в среде хлороформа.1. A method of producing 2-tert-butylperoxyoxacycloalkanes of the general formula where n = 1, 2, by reacting the corresponding oxacycloalkane with tert-butyl hydroperoxide in the presence of an inorganic chlorine-containing compound, in order to reduce the loss of tert-butyl hydroperoxide and simplify the process, chlorine-containing compounds are used sulfuryl chloride, which is added to a mixture of oxacycloalkane and tert-butyl hydroperoxide at 0-10C, after which the reaction mass is maintained at 18-22C for 0.7-1 h, the process is conducted at a molar ratio of chloride sulphuryl, tert-butyl hydroperoxide and oxacycloalkane 1: (1.4-4) :( 3-12) .2. The method according to p. 1, characterized in that the process is conducted in an environment of chloroform.

SU3762096/04K 1984-07-09 1984-07-09 Method of producing 2-trit-butyl-peroxio-cycloalkanes SU1360130A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU3762096/04A SU1360131A1 (en) 1984-07-09 1984-07-09 METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES

Publications (1)

Publication Number Publication Date
SU1360130A1 true SU1360130A1 (en) 2002-08-27

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ID=60533717

Family Applications (2)

Application Number Title Priority Date Filing Date
SU3762096/04A SU1360131A1 (en) 1984-07-09 1984-07-09 METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES
SU3762096/04K SU1360130A1 (en) 1984-07-09 1984-07-09 Method of producing 2-trit-butyl-peroxio-cycloalkanes

Family Applications Before (1)

Application Number Title Priority Date Filing Date
SU3762096/04A SU1360131A1 (en) 1984-07-09 1984-07-09 METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES

Country Status (1)

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SU (2) SU1360131A1 (en)

Also Published As

Publication number Publication date
SU1360131A1 (en) 2002-08-27

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