SU1360130A1 - Method of producing 2-trit-butyl-peroxio-cycloalkanes - Google Patents
Method of producing 2-trit-butyl-peroxio-cycloalkanesInfo
- Publication number
- SU1360130A1 SU1360130A1 SU3762096/04K SU3762096K SU1360130A1 SU 1360130 A1 SU1360130 A1 SU 1360130A1 SU 3762096/04 K SU3762096/04 K SU 3762096/04K SU 3762096 K SU3762096 K SU 3762096K SU 1360130 A1 SU1360130 A1 SU 1360130A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- tert
- butyl hydroperoxide
- producing
- oxacycloalkane
- butyl
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1. Способ получения 2-трет-бутилпероксиоксациклоалканов общей формулыгде n=1, 2,взаимодействием соответствующего оксациклоалкана с гидроперекисью трет-бутила в присутствии неорганического хлорсодержащего соединения, отличающийся тем, что, с целью уменьшения потерь гидроперекиси трет-бутила и упрощения процесса, в качестве хлорсодержащего соединения используют хлористый сульфурил, который добавляют к смеси оксациклоалкана и гидроперекиси трет-бутила при 0-10C, после чего реакционную массу выдерживают при 18-22C в течение 0,7-1 ч, процесс ведут при молярном соотношении хлористого сульфурила, гидроперекиси трет-бутила и оксациклоалкана 1:(1,4-4):(3-12).2. Способ по п. 1, отличающийся тем, что процесс ведут в среде хлороформа.1. A method of producing 2-tert-butylperoxyoxacycloalkanes of the general formula where n = 1, 2, by reacting the corresponding oxacycloalkane with tert-butyl hydroperoxide in the presence of an inorganic chlorine-containing compound, in order to reduce the loss of tert-butyl hydroperoxide and simplify the process, chlorine-containing compounds are used sulfuryl chloride, which is added to a mixture of oxacycloalkane and tert-butyl hydroperoxide at 0-10C, after which the reaction mass is maintained at 18-22C for 0.7-1 h, the process is conducted at a molar ratio of chloride sulphuryl, tert-butyl hydroperoxide and oxacycloalkane 1: (1.4-4) :( 3-12) .2. The method according to p. 1, characterized in that the process is conducted in an environment of chloroform.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU3762096/04A SU1360131A1 (en) | 1984-07-09 | 1984-07-09 | METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES |
Publications (1)
Publication Number | Publication Date |
---|---|
SU1360130A1 true SU1360130A1 (en) | 2002-08-27 |
Family
ID=60533717
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU3762096/04A SU1360131A1 (en) | 1984-07-09 | 1984-07-09 | METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES |
SU3762096/04K SU1360130A1 (en) | 1984-07-09 | 1984-07-09 | Method of producing 2-trit-butyl-peroxio-cycloalkanes |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU3762096/04A SU1360131A1 (en) | 1984-07-09 | 1984-07-09 | METHOD OF OBTAINING 2-TRET-BUTYL-PEROXYOXYCLO-ALKANES |
Country Status (1)
Country | Link |
---|---|
SU (2) | SU1360131A1 (en) |
-
1984
- 1984-07-09 SU SU3762096/04A patent/SU1360131A1/en active
- 1984-07-09 SU SU3762096/04K patent/SU1360130A1/en active
Also Published As
Publication number | Publication date |
---|---|
SU1360131A1 (en) | 2002-08-27 |
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