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Organic Low-Molecular-Weight Compounds And Preparation Thereof
(AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts
(AREA)
Abstract
FIELD: organic chemistry. SUBSTANCE: desired compounds having common formula $$$ (where $$$ is Cl, $$$ and $$$ is H, Cl) are prepared by phosgenation of benzenesulfamides having common formula $$$ (where $$$ and $$$ are as mentioned above). The process is carried out in the presence of catalyst and additive which contains isocyanate in the medium of chlorine-containing solvent. Tetramethyl ethylene diamine is used as mentioned above catalyst, phenylisocyanate being used as said additive. EFFECT: increases yield of desired product.
SU3774222/04A1984-07-241984-07-24Method for production of ortho-substituted benzenesulfonyl isocyanates
SU1226809A1
(en)