SU1209627A1 - Soldering glass compound - Google Patents

Soldering glass compound Download PDF

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Publication number
SU1209627A1
SU1209627A1 SU843783573A SU3783573A SU1209627A1 SU 1209627 A1 SU1209627 A1 SU 1209627A1 SU 843783573 A SU843783573 A SU 843783573A SU 3783573 A SU3783573 A SU 3783573A SU 1209627 A1 SU1209627 A1 SU 1209627A1
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SU
USSR - Soviet Union
Prior art keywords
glass
lead
soldering
glass compound
soldering glass
Prior art date
Application number
SU843783573A
Other languages
Russian (ru)
Inventor
Виктор Борисович Калинин
Александр Юрьевич Шашков
Владимир Николаевич Сигаев
Галина Борисовна Княжер
Регина Антоновна Журавлева
Павел Иванович Литвинов
Яков Лазаревич Рыжик
Малхаз Александрович Мелива
Original Assignee
Предприятие П/Я Х-5382
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Предприятие П/Я Х-5382 filed Critical Предприятие П/Я Х-5382
Priority to SU843783573A priority Critical patent/SU1209627A1/en
Application granted granted Critical
Publication of SU1209627A1 publication Critical patent/SU1209627A1/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/24Fusion seal compositions being frit compositions having non-frit additions, i.e. for use as seals between dissimilar materials, e.g. glass and metal; Glass solders

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Description

1 one

Изобретение относитс  к составам материалов, в частности к составу низкотемпературной припоечной стек- локомпозиции, котора  может быть использована в электронной технике дл  герметизации интегральных схем в металлических корпусах, изготовленных из сплавов на основе меди , алгсмини , а также дл  спаивани  деталей ультрапрецизион- ньгх резисторов.The invention relates to the composition of materials, in particular, to the composition of low-temperature solder glass composition, which can be used in electronic engineering for sealing integrated circuits in metal housings made of copper-based alloys, as well as for soldering parts of ultra-precision resistors.

Свинцовый сурик15 t--Moлибдaт аммони 12 ,1 850Red lead t 15 - Ammonium molibdat 12, 1 850

Свинцовый сурик35 Red lead35

п--Молибдат аммо-28,3 950 ни p - Ammo molybdate-28.3 950

Свинцовый сурик20Red lead20

ft -Молибдат аммони 16 ,2ft-Ammonium molybdate 16, 2

В качестве легкоплавкого стекла может быть вз то некристаллизующеес  свинцовоборатное стекло с ТКЛР (110-115) 10 К и температурой разм гчени  340-380 с. Одним из примеров стекла с указанными свойствами  вл етс  стекло следующего состо- ва, мас.%: РЬО 83-85; ВгОз12-15; AliOjO,1-1,0; SiCti,0,1-1,5;Zn.OO,1-2,0.As a low-melting glass, noncrystallizing lead borate glass with TCLE (110–115) 10 K and a softening temperature of 340–380 s can be used. One example of glass with the indicated properties is glass of the following state, wt.%: PHO 83-85; VgOz12-15; AliOjO, 1-1.0; SiCti, 0.1-1.5; Zn.OO, 1-2.0.

Стеклокомпозиц ионный припоечньй материал с ТКЛР получают путем смешивани  порошков легкоплавкого стекла и кристгшлического молибдата свинца.The glass composite ion solder material with TCLE is produced by mixing powders of low-melting glass and crystalline lead molybdate.

Составы предлагаемой стеклокомпо- зиции приведены в табл. 2, а ихThe compositions of the proposed glass composition are given in Table. 2, and their

свойства - в табл. 3.properties - in the table. 3

Таблица2Table 2

096272096272

Цель изобретени  - повышение КТР и снижение температуры спаивани .The purpose of the invention is to increase the CTE and decrease the temperature of soldering.

Порошок кристаллического молибдена свинца (РЬИоО;,) получают смешиванием свинцового сурика и ц,- Молиб- дата аммони  1(НН(;)Мо|Ог(, 4 . Смесь тщательно гомогенизируют и отжигают при 800-1000°С в течение 1-6 ч до получени  необходимого гра- 0 нулометрического состава. Примеры получени  PbMoOi, приведены в табл.1.Lead crystalline molybdenum powder (PHYOO ;,) is obtained by mixing lead red lead and c, - Ammonium Molybdate 1 (HH (;) Mo | Og (, 4. The mixture is thoroughly homogenized and annealed at 800–1000 ° С for 1–6 to obtain the required grain size composition. Examples of the preparation of PbMoOi are given in Table 1.

Т а б л и ц а 1Table 1

10001000

3,53.5

СвойстваProperties

ТаблицаЗ Составы Table H

Температура спаивани , с 490 470 450 450 Врем  выдержки при спаивании ,Soldering temperature, from 490 470 450 450 Soaking time at soldering,

минmin

Способность к кристаллизацииCrystallisability

20 1520 15

1515

1515

Не кристаллизуетс Does not crystallize

ТКЛР, .10- К TEC, .10- K

145 139 125 120145 139 125 120

Предлагаема  стеклокомпозици  дает возможность получени  прочных термостойких спаев деталей из ситал- лов, стекла, металлов и сплавов с высоким ТКЛР.The proposed glass composition makes it possible to obtain durable heat-resistant junctions of parts made of sital glass, glass, metals, and alloys with high thermal expansion coefficient.

Claims (1)

ПРИПОЕЧНАЯ СТЕКЛОКОМПОЗИЦИЯ, включающая легкоплавкое стекло и соль свинца, отличающаяся тем, что, с целью повышения КТР и снижения температуры спаивания, она содержит в качестве соли свинца молибдат свинца при следующем соотношении компонентов, мас.%:SOLDER GLASS COMPOSITION, including low-melting glass and lead salt, characterized in that, in order to increase the CTE and lower the soldering temperature, it contains lead molybdate as the lead salt in the following ratio of components, wt.%: Легкоплавкое стекло 50-90 Молибдат свинца . 10-50Fusible glass 50-90 Lead molybdate. 10-50
SU843783573A 1984-08-23 1984-08-23 Soldering glass compound SU1209627A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU843783573A SU1209627A1 (en) 1984-08-23 1984-08-23 Soldering glass compound

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU843783573A SU1209627A1 (en) 1984-08-23 1984-08-23 Soldering glass compound

Publications (1)

Publication Number Publication Date
SU1209627A1 true SU1209627A1 (en) 1986-02-07

Family

ID=21135827

Family Applications (1)

Application Number Title Priority Date Filing Date
SU843783573A SU1209627A1 (en) 1984-08-23 1984-08-23 Soldering glass compound

Country Status (1)

Country Link
SU (1) SU1209627A1 (en)

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Патент US № 3964920, :кл. 106-53, опублик. 1976. Патент US № 4115132, кл. 106-53, опублик. 1978. *

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