SU1049490A1 - (3ar,9as,9bs)-6,6,9a-trimethyltransperhydronaphth(2,2-b)-furan as scent component of perfumery composition - Google Patents

(3ar,9as,9bs)-6,6,9a-trimethyltransperhydronaphth(2,2-b)-furan as scent component of perfumery composition Download PDF

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SU1049490A1
SU1049490A1 SU823440237A SU3440237A SU1049490A1 SU 1049490 A1 SU1049490 A1 SU 1049490A1 SU 823440237 A SU823440237 A SU 823440237A SU 3440237 A SU3440237 A SU 3440237A SU 1049490 A1 SU1049490 A1 SU 1049490A1
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USSR - Soviet Union
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sub
colspan
furan
composition
trimethyltransperhydronaphth
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SU823440237A
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Russian (ru)
Inventor
Павел Федорович Влад
Лариса Владиславовна Прокопышина
Иван Петрович Драгалин
Михаил Николаевич Колца
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Ордена Трудового Красного Знамени Институт Химии Ан Мсср
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Publication of SU1049490A1 publication Critical patent/SU1049490A1/en

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Abstract

(Зой , ,9Ь5)-6,69 а - Триметип-транс-пергидронафто ,1-р фуран формулы - I О сов качестве душистого компонента парфюмерной композиции.(Zoy, 9b5) -6,69 a — Trimetip-trans-perhydronaphto, 1-p furan of the formula — I As the quality of the fragrant component of the perfume composition.

Description

j;j;

соwith

4four

СОWITH

ОABOUT

Claims (1)

<claim-text><table border="1"> <tbody><tr><td> ЯМР-спектр (СС 64</td><td> , ТМС, 5 ), м.ц.:</td></tr> <tr><td colspan="2"> синглеты по ЗН при 0,83 (Со<sub>а</sub> — &gt;СН* ),</td></tr> <tr><td> 0,90 и 1,1 [С.<sub>о</sub> (СН<sub>5</sub></td><td> )<sub>2</sub>] , мупьтиппет</td></tr> <tr><td> при 3,88 (ЗН, Су -СН<sub>2</sub></td><td> и Сц<sub>а</sub> СН- труп-</td></tr> <tr><td> пы).</td><td> </td></tr> <tr><td colspan="2"> Масс-спектр: го/е 222(М<sup>+</sup>),</td></tr> <tr><td> .Найдено, %: С 80,99]</td><td> ;.Н 11,80</td></tr> <tr><td> С(5 ^26° '</td><td> </td></tr> <tr><td colspan="2"> Вычислено, %: С 81,00; Н 11,81.</td></tr> <tr><td colspan="2"> Пример рецептуры парфюмерной компо-</td></tr> <tr><td> эидии, содержащей (3 а К ,</td><td> 9а5, 9Ъ5)-</td></tr> <tr><td colspan="2"> 6,6,9 -гримегил-гранс-пергидронафго</td></tr> <tr><td> [2,1 -'Ыфуран. В состав</td><td> композиции вхо-</td></tr> <tr><td colspan="2"> цят следующие компоненты, вес, %:</td></tr> <tr><td> Яра-яра</td><td> , 0,3</td></tr> <tr><td> Амилбензоат</td><td> 0,9</td></tr> <tr><td> Композиция" "амбрия"</td><td> 1,0</td></tr> <tr><td> Коричное масло "Д",</td><td> 1,0</td></tr> <tr><td> Пентацеканопид</td><td> 1,0</td></tr> <tr><td> Миристиновая кислота</td><td> 1,5</td></tr> <tr><td> Циннамипиэобутират</td><td> .1,5</td></tr> <tr><td> Геранилизобутират</td><td> 2,0</td></tr> <tr><td> Олеиновая кислота</td><td> 8,0</td></tr> <tr><td> Продукт (ЗаК, 9а5,</td><td> </td></tr> <tr><td> 9Ъ5)-6,6,9&lt;х-триметил.</td><td> -</td></tr> <tr><td> транс-пергидронафто</td><td> </td></tr> <tr><td> £.1 -4/фуран</td><td> 10,0</td></tr> <tr><td> • Амбриаль</td><td> 15,0</td></tr> <tr><td> Диэтилфтапат</td><td> 57,8</td></tr> </tbody></table><claim-text> <table border = "1"> <tbody> <tr> <td> NMR spectrum (SS 64 </ td> <td> , TMS, 5), м .ц.: </ Td> </ tr> <tr> <td colspan = "2"> singlets for OA at 0.83 (Co <sub> a </ sub> - &gt; CH *), </ td> </ tr> <tr> <td> 0.90 and 1.1 [p. <Sub> o </ sub> (CH <sub> 5 </ sub> </ td> <td> ) <sub> 2 </ sub>], mntypept </ td> </ tr> <tr> <td> at 3.88 (GH, Su-CH <sub> 2 </ sub> </ td> <td> and Sc <sub> a </ sub> СН- corpse - </ td> </ tr> <tr> <td> py). </ td> <td> </ td> </ tr> <tr> <td colspan = "2"> Mass spectrum: go / e 222 (M <sup> + </ sup>), </ td> </ tr> <tr> <td> . Found,%: C 80.99] </ td> <td> ; .N 11.80 </ td> </ tr> <tr> <td> C (5 ^ 26 ° '</ td> <td> </ td> </ tr> <tr> <td colspan = "2"> Calculated,%: C 81.00; H 11.81. </ Td> </ tr> <tr> <td colspan = "2"> Sample perfume compounding recipe - </ td> </ tr> <tr> <td> eidia containing (3 a K, </ td> <td> 9a5, 9b5) - </ td> </ tr> <tr> <td colspan = "2"> 6,6,9 -grimegyl-gran-pergidronofgo </ td> </ tr> <tr> <td> [2,1 -'Yfuran. The composition </ td> <td> compositions in - </ td> </ tr> <tr> <td colspan = "2"> The following components are worth weight%: </ td> </ tr> <tr> <td> Yara-Yara </ td> <td> 0.3 </ td> </ tr> <tr> <td> Amilbenzoate </ td> <td> 0.9 </ td> </ tr> <tr> <td> The composition "" Ambria "</ td> <td> 1.0 </ td> </ tr> <tr> <td> Cinnamon oil "D", </ td> <td> 1.0 </ td> </ tr> <tr> <td> Pentacecanopid </ td> <td> 1.0 </ td> </ tr> <tr> <td> Myristic acid </ td> <td> 1.5 </ td> </ tr> <tr> <td> Cinnamiabutyrate </ td> <td> .1,5 </ td> </ tr> <tr> <td> Geranyl isobutyrate </ td> <td> 2.0 </ td> </ tr> <tr> <td> Oleic acid </ td> <td> 8.0 </ td> </ tr> <tr> <td> Product (Zak, 9a5, </ td> <td> </ td> </ tr> <tr> <td> 9b5) -6,6,9 <x-trimethyl. </ Td> <td> - </ td> </ tr> <tr> <td> trans-perhydronaphto </ td> <td> </ td> </ tr> <tr> <td> £ .1-4 / furan </ td> <td> 10.0 </ td> </ tr> <tr> <td> • Ambrial </ td> <td> 15.0 </ td> </ tr> <tr> <td> Diethylphaptate </ td> <td> 57.8 </ td> </ tr> </ tbody> </ table>
SU823440237A 1982-05-18 1982-05-18 (3ar,9as,9bs)-6,6,9a-trimethyltransperhydronaphth(2,2-b)-furan as scent component of perfumery composition SU1049490A1 (en)

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SU823440237A SU1049490A1 (en) 1982-05-18 1982-05-18 (3ar,9as,9bs)-6,6,9a-trimethyltransperhydronaphth(2,2-b)-furan as scent component of perfumery composition

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2571661C2 (en) * 2010-03-19 2015-12-20 Бостон Байомедикал, Инк. Novel compounds and compositions for targeting at malignant stem cells
US10377731B2 (en) 2007-09-10 2019-08-13 Boston Biomedical, Inc. Compositions and methods for cancer treatment
US10543189B2 (en) 2013-04-09 2020-01-28 Boston Biomedical, Inc. 2-acetylnaphtho[2,3-b]furan -4,9-dione for use on treating cancer
US10646464B2 (en) 2017-05-17 2020-05-12 Boston Biomedical, Inc. Methods for treating cancer
US11299469B2 (en) 2016-11-29 2022-04-12 Sumitomo Dainippon Pharma Oncology, Inc. Naphthofuran derivatives, preparation, and methods of use thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
1. Авторское свидетепьство СССР № 529166, кп, С 07 D ЗО7/92, 1975. *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10377731B2 (en) 2007-09-10 2019-08-13 Boston Biomedical, Inc. Compositions and methods for cancer treatment
US10851075B2 (en) 2007-09-10 2020-12-01 Sumitomo Dainippon Pharma Oncology, Inc. Stat3 pathway inhibitors and cancer stem cell inhibitors
RU2571661C2 (en) * 2010-03-19 2015-12-20 Бостон Байомедикал, Инк. Novel compounds and compositions for targeting at malignant stem cells
US9381184B2 (en) 2010-03-19 2016-07-05 Boston Biomedical, Inc. Compounds and compositions for targeting cancer stem cells
US10543189B2 (en) 2013-04-09 2020-01-28 Boston Biomedical, Inc. 2-acetylnaphtho[2,3-b]furan -4,9-dione for use on treating cancer
US11299469B2 (en) 2016-11-29 2022-04-12 Sumitomo Dainippon Pharma Oncology, Inc. Naphthofuran derivatives, preparation, and methods of use thereof
US10646464B2 (en) 2017-05-17 2020-05-12 Boston Biomedical, Inc. Methods for treating cancer

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