SG11202102770XA - Process for bio-1,3-butanediol purification from a fermentation broth - Google Patents

Process for bio-1,3-butanediol purification from a fermentation broth

Info

Publication number
SG11202102770XA
SG11202102770XA SG11202102770XA SG11202102770XA SG11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA
Authority
SG
Singapore
Prior art keywords
bio
fermentation broth
butanediol
purification
butanediol purification
Prior art date
Application number
SG11202102770XA
Inventor
Mario Baldassarre
Alberto Cesana
Fabrizio Bordes
Original Assignee
Versalis Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Versalis Spa filed Critical Versalis Spa
Publication of SG11202102770XA publication Critical patent/SG11202102770XA/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/363—Anion-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D21/00—Separation of suspended solid particles from liquids by sedimentation
    • B01D21/26—Separation of sediment aided by centrifugal force or centripetal force
    • B01D21/262—Separation of sediment aided by centrifugal force or centripetal force by using a centrifuge
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027—Nanofiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58—Multistep processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00—Ion-exchange processes in general; Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/24—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms by elimination of water
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/12—Alkadienes
    • C07C11/16—Alkadienes with four carbon atoms
    • C07C11/167—1, 3-Butadiene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C07C31/207—1,4-Butanediol; 1,3-Butanediol; 1,2-Butanediol; 2,3-Butanediol
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F36/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
    • C08F36/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
    • C08F36/04—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
    • C08F36/06—Butadiene
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/18—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic polyhydric
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/62—Carboxylic acid esters
    • C12P7/625—Polyesters of hydroxy carboxylic acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B01D2325/0283—Pore size
    • B01D2325/02834—Pore size more than 0.1 and up to 1 µm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/34—Molecular weight or degree of polymerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2523/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
    • C07C2523/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of rare earths

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Zoology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Microbiology (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
SG11202102770XA 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth SG11202102770XA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IT201800008820 2018-09-21
PCT/EP2019/075123 WO2020058381A1 (en) 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth

Publications (1)

Publication Number Publication Date
SG11202102770XA true SG11202102770XA (en) 2021-04-29

Family

ID=64607119

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11202102770XA SG11202102770XA (en) 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth

Country Status (18)

Country Link
US (1) US20210380512A1 (en)
EP (1) EP3853197B1 (en)
JP (1) JP7390369B2 (en)
KR (1) KR20210068049A (en)
CN (1) CN113166008B (en)
AU (1) AU2019344574B2 (en)
BR (1) BR112021005183B1 (en)
CA (1) CA3113477A1 (en)
CL (1) CL2021000700A1 (en)
DK (1) DK3853197T3 (en)
EA (1) EA202190811A1 (en)
FI (1) FI3853197T3 (en)
IL (1) IL281601B2 (en)
MX (1) MX2021003364A (en)
PL (1) PL3853197T3 (en)
PT (1) PT3853197T (en)
SG (1) SG11202102770XA (en)
WO (1) WO2020058381A1 (en)

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1908620A1 (en) 1969-02-21 1970-09-03 Basf Ag Modified polyolefin waxes
JPS6165834A (en) * 1984-09-07 1986-04-04 Daicel Chem Ind Ltd Purification of 1,3-butylene glycol
US6361983B1 (en) 1999-09-30 2002-03-26 E. I. Du Pont De Nemours And Company Process for the isolation of 1,3-propanediol from fermentation broth
CA2522928C (en) 2003-05-06 2013-09-24 E.I. Du Pont De Nemours And Company Purification of biologically-produced 1,3-propanediol
WO2010127319A2 (en) 2009-04-30 2010-11-04 Genomatica, Inc. Organisms for the production of 1,3-butanediol
WO2010141780A1 (en) 2009-06-04 2010-12-09 Genomatica, Inc. Process of separating components of a fermentation broth
AU2012273177A1 (en) 2011-06-22 2013-05-02 Genomatica, Inc. Microorganisms for producing 1,3-butanediol and methods related thereto
MX348612B (en) * 2011-08-19 2017-06-21 Genomatica Inc Microorganisms and methods for producing 2,4-pentadienoate, butadiene, propylene, 1,3-butanediol and related alcohols.
EP2753699A4 (en) 2011-09-08 2015-08-19 Genomatica Inc Eukaryotic organisms and methods for producing 1,3-butanediol
CN103987852B (en) 2011-10-14 2017-02-15 东丽株式会社 Process for producing 2,3-butanediol
JP2014176567A (en) 2013-03-15 2014-09-25 Makita Corp Cleaner
BR112015021885B1 (en) * 2013-03-15 2021-08-17 Genomatica, Inc PROCESS FOR PURIFICATION OF 1,4-BUTANEDIOL (1,4-BDO)
US20140275465A1 (en) 2013-03-15 2014-09-18 Genomatica, Inc. Process and systems for obtaining 1,4-butanediol from fermentation broths
TR201904615T4 (en) 2013-04-12 2019-05-21 Toray Industries Process for producing 1,4-butanediol.
CN105793429B (en) * 2013-11-22 2019-12-06 东丽株式会社 Method for producing 2,3-butanediol
HUE059279T2 (en) 2014-05-16 2022-11-28 Versalis Spa Process for the production of alkenols and use thereof for the production of 1,3-butadiene
CN107074677B (en) * 2014-12-12 2021-03-09 维尔萨利斯股份公司 Process for producing 1, 3-butadiene from 1, 3-butanediol
CN107108398B (en) 2015-02-23 2023-10-10 维尔萨利斯股份公司 For oxygen-containing compounds is dehydrated by a method of
PL3262023T3 (en) 2015-02-23 2021-07-05 Versalis S.P.A. Process for the production of dienes
IT201600105178A1 (en) * 2016-10-19 2018-04-19 Versalis Spa Process for the production of dienes
JP2020512351A (en) * 2017-03-31 2020-04-23 ジェノマティカ， インコーポレイテッド Process and system for obtaining 1,3-butanediol from fermentation broth

Also Published As

Publication number Publication date
DK3853197T3 (en) 2024-02-12
EP3853197A1 (en) 2021-07-28
IL281601B1 (en) 2023-11-01
EA202190811A1 (en) 2021-06-17
WO2020058381A1 (en) 2020-03-26
BR112021005183B1 (en) 2024-03-12
CN113166008B (en) 2024-02-06
PL3853197T3 (en) 2024-05-20
KR20210068049A (en) 2021-06-08
CA3113477A1 (en) 2020-03-26
IL281601B2 (en) 2024-03-01
FI3853197T3 (en) 2024-03-01
EP3853197B1 (en) 2024-01-24
PT3853197T (en) 2024-02-22
JP7390369B2 (en) 2023-12-01
CN113166008A (en) 2021-07-23
AU2019344574B2 (en) 2024-01-25
US20210380512A1 (en) 2021-12-09
BR112021005183A2 (en) 2021-06-29
JP2022502364A (en) 2022-01-11
MX2021003364A (en) 2021-08-16
AU2019344574A1 (en) 2021-04-29
CL2021000700A1 (en) 2021-10-08
IL281601A (en) 2021-05-31

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