SG11201802078SA - Extractive workup of a sodium-salt-containing mma-methanol mixture - Google Patents

Extractive workup of a sodium-salt-containing mma-methanol mixture

Info

Publication number
SG11201802078SA
SG11201802078SA SG11201802078SA SG11201802078SA SG11201802078SA SG 11201802078S A SG11201802078S A SG 11201802078SA SG 11201802078S A SG11201802078S A SG 11201802078SA SG 11201802078S A SG11201802078S A SG 11201802078SA SG 11201802078S A SG11201802078S A SG 11201802078SA
Authority
SG
Singapore
Prior art keywords
sodium
salt
methanol mixture
extractive workup
containing mma
Prior art date
Application number
SG11201802078SA
Inventor
Matthias Grömping
Steffen Krill
Alexander Lygin
Milica Lukic
Steffen Finger
Original Assignee
Evonik Roehm Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm Gmbh filed Critical Evonik Roehm Gmbh
Publication of SG11201802078SA publication Critical patent/SG11201802078SA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/39Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C07C67/40Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester by oxidation of primary alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/673Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by change of size of the carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/74Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups combined with dehydration
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/39Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/44Preparation of carboxylic acid esters by oxidation-reduction of aldehydes, e.g. Tishchenko reaction
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/58Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54Acrylic acid esters; Methacrylic acid esters
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials
SG11201802078SA 2015-09-16 2016-09-14 Extractive workup of a sodium-salt-containing mma-methanol mixture SG11201802078SA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP15185434 2015-09-16
PCT/EP2016/071608 WO2017046110A1 (en) 2015-09-16 2016-09-14 Extractive workup of a sodium-salt-containing mma-methanol mixture

Publications (1)

Publication Number Publication Date
SG11201802078SA true SG11201802078SA (en) 2018-04-27

Family

ID=54147087

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201802078SA SG11201802078SA (en) 2015-09-16 2016-09-14 Extractive workup of a sodium-salt-containing mma-methanol mixture

Country Status (13)

Country Link
US (1) US10301251B2 (en)
EP (1) EP3350153B1 (en)
JP (1) JP6884140B2 (en)
KR (1) KR102653600B1 (en)
CN (2) CN112521283B (en)
BR (1) BR112018005076B1 (en)
ES (1) ES2738991T3 (en)
MY (1) MY186435A (en)
RU (1) RU2715436C2 (en)
SA (1) SA518391126B1 (en)
SG (1) SG11201802078SA (en)
TW (1) TWI715627B (en)
WO (1) WO2017046110A1 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201722903A (en) * 2015-12-18 2017-07-01 陶氏全球科技責任有限公司 Process for purification of methyl methacrylate
TW201739730A (en) * 2015-12-18 2017-11-16 陶氏全球科技責任有限公司 Process for purification of methyl methacrylate
KR20200038266A (en) * 2017-08-04 2020-04-10 룀 게엠베하 Concrete fluidity improver and water reducing agent
EP3549961A1 (en) * 2018-04-03 2019-10-09 Evonik Röhm GmbH Concrete flow improver and water reducing agent
EP3450422A1 (en) 2017-08-29 2019-03-06 Evonik Röhm GmbH Method for producing optical moulding compositions
EP3587390A1 (en) 2018-06-26 2020-01-01 Röhm GmbH Method for manufacturing mma in high yields
CN111233667A (en) * 2018-11-29 2020-06-05 中国科学院大连化学物理研究所 Improved method for preparing methyl methacrylate
EP3786148A1 (en) * 2019-08-28 2021-03-03 Röhm GmbH Simplified processing of the reactor output from an oxidative esterification
EP3798206A1 (en) 2019-09-25 2021-03-31 Röhm GmbH Method for producing alkyl methacrylates with improved water and acid guidance
EP3798202A1 (en) 2019-09-25 2021-03-31 Röhm GmbH Method for purifying methyl methacrylate from low boiling point components
EP3945088A1 (en) * 2020-07-30 2022-02-02 Röhm GmbH Process for minimising the loss of activity in reaction steps carried out in circulation
KR20240006654A (en) 2021-05-10 2024-01-15 룀 게엠베하 Additives containing unsaturated esters to reduce and stabilize the yellowness index
US20230150912A1 (en) 2021-11-12 2023-05-18 Röhm Gmbh Process for eliminating interfering by-products in the direct oxidative esterification of methacrolein

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3819685A (en) * 1971-12-06 1974-06-25 Standard Oil Co Preparation of esters from unsaturated aldehydes and alcohols
DE3411384A1 (en) * 1984-03-28 1985-10-10 Basf Ag, 6700 Ludwigshafen METHOD FOR THE EXTRACTION OF WATER-FREE OR MOSTLY WATER-FREE FORMIC ACID BY HYDROLYSIS OF METHYLFORMIAT
JPH0769948A (en) * 1993-09-02 1995-03-14 Kuraray Co Ltd Recovery of methanol
DE19604253A1 (en) * 1996-02-06 1997-08-07 Basf Ag Process for the continuous production of alkyl esters of (meth) acrylic acid
JP3950505B2 (en) * 1996-12-13 2007-08-01 旭化成ケミカルズ株式会社 How to recover lead
SG71815A1 (en) 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
JP3532763B2 (en) 1998-04-22 2004-05-31 旭化成ケミカルズ株式会社 Purification method of methyl methacrylate
JP2001288147A (en) * 2000-04-11 2001-10-16 Mitsubishi Rayon Co Ltd Method for producing methyl methacrylate
JP3672818B2 (en) * 2000-12-26 2005-07-20 三菱レイヨン株式会社 (Meth) acrylic acid ester purification method
AU2002354236A1 (en) 2001-12-21 2003-07-09 Asahi Kasei Chemicals Corporation Oxide catalyst composition
JP3819419B2 (en) * 2006-04-21 2006-09-06 旭化成ケミカルズ株式会社 Method for recovering methacrolein and methanol
CN103833551A (en) * 2012-11-27 2014-06-04 华东理工大学工程设计研究院有限公司 Separation equipment and separation method of methyl methacrylate (MMA)
CN108164417B (en) * 2013-04-19 2021-07-06 罗姆化学有限责任公司 Method for producing methyl methacrylate

Also Published As

Publication number Publication date
SA518391126B1 (en) 2022-01-18
CN112521283A (en) 2021-03-19
BR112018005076A2 (en) 2018-10-02
US10301251B2 (en) 2019-05-28
EP3350153B1 (en) 2019-06-05
MY186435A (en) 2021-07-22
US20180251419A1 (en) 2018-09-06
ES2738991T3 (en) 2020-01-28
BR112018005076B1 (en) 2021-06-29
KR20180053716A (en) 2018-05-23
KR102653600B1 (en) 2024-04-01
JP6884140B2 (en) 2021-06-09
CN108124444B (en) 2021-01-29
JP2018527375A (en) 2018-09-20
TWI715627B (en) 2021-01-11
EP3350153A1 (en) 2018-07-25
RU2715436C2 (en) 2020-02-28
BR112018005076A8 (en) 2018-10-02
RU2018113514A (en) 2019-10-16
CN108124444A (en) 2018-06-05
RU2018113514A3 (en) 2019-11-01
TW201722900A (en) 2017-07-01
CN112521283B (en) 2023-09-01
WO2017046110A1 (en) 2017-03-23

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