SG11201406619XA - Process for separating a mixture comprising cyclohexanone and phenol - Google Patents

Process for separating a mixture comprising cyclohexanone and phenol

Info

Publication number
SG11201406619XA
SG11201406619XA SG11201406619XA SG11201406619XA SG11201406619XA SG 11201406619X A SG11201406619X A SG 11201406619XA SG 11201406619X A SG11201406619X A SG 11201406619XA SG 11201406619X A SG11201406619X A SG 11201406619XA SG 11201406619X A SG11201406619X A SG 11201406619XA
Authority
SG
Singapore
Prior art keywords
cyclohexanone
phenol
separating
mixture
Prior art date
Application number
SG11201406619XA
Inventor
Keith H Kuechler
Francisco M Benitez
Krystle J Chavez
Christopher L Becker
John L Heidman Jr
Original Assignee
Exxonmobil Chem Patents Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Exxonmobil Chem Patents Inc filed Critical Exxonmobil Chem Patents Inc
Publication of SG11201406619XA publication Critical patent/SG11201406619XA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385Saturated compounds containing a keto group being part of a ring
    • C07C49/403Saturated compounds containing a keto group being part of a ring of a six-membered ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/74Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C37/80Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40Extractive distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/08Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by decomposition of hydroperoxides, e.g. cumene hydroperoxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/58Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by oxidation reactions introducing directly hydroxy groups on a =CH-group belonging to a six-membered aromatic ring with the aid of molecular oxygen
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/53Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C07C45/83Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by extractive distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
SG11201406619XA 2012-05-02 2013-04-09 Process for separating a mixture comprising cyclohexanone and phenol SG11201406619XA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201261641375P 2012-05-02 2012-05-02
PCT/US2013/035744 WO2013165656A1 (en) 2012-05-02 2013-04-09 Process for separating a mixture comprising cyclohexanone and phenol

Publications (1)

Publication Number Publication Date
SG11201406619XA true SG11201406619XA (en) 2014-11-27

Family

ID=48140186

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201406619XA SG11201406619XA (en) 2012-05-02 2013-04-09 Process for separating a mixture comprising cyclohexanone and phenol

Country Status (5)

Country Link
US (1) US9181165B2 (en)
EP (1) EP2844628A1 (en)
CN (1) CN104284876B (en)
SG (1) SG11201406619XA (en)
WO (1) WO2013165656A1 (en)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2964354B1 (en) 2013-03-04 2018-05-30 ExxonMobil Chemical Patents Inc. System and process for making phenol and/or cyclohexanone
JP5993525B2 (en) 2013-03-04 2016-09-14 エクソンモービル ケミカル パテンツ インコーポレイテッド System and method for producing cyclohexylbenzene
EP2978529A1 (en) 2013-03-25 2016-02-03 ExxonMobil Chemical Patents Inc. Process for making alkylated aromatic compound
SG11201506967PA (en) 2013-03-25 2015-10-29 Exxonmobil Chem Patents Inc Process for making alkylated aromatic compound
EP2981517B1 (en) 2013-04-02 2017-04-19 ExxonMobil Chemical Patents Inc. Process and apparatus for making phenol and/or cyclohexanone
CN105829273B (en) 2013-12-20 2019-05-28 埃克森美孚化学专利公司 The method for preparing phenol and/or cyclohexanone
US20170057895A1 (en) 2013-12-20 2017-03-02 Exxonmobil Chemical Patents Inc. Phenol Composition
CN105899477A (en) 2013-12-20 2016-08-24 埃克森美孚化学专利公司 Cyclohexylbenzene composition
WO2015183384A1 (en) 2014-05-30 2015-12-03 Exxonmobil Chemical Patents Inc. Process and device for removing water and/or oxygen from organic liquid
KR20170027855A (en) 2014-08-15 2017-03-10 엑손모빌 케미칼 패턴츠 인코포레이티드 Process and system for making cyclohexanone
WO2016025217A1 (en) 2014-08-15 2016-02-18 Exxonmobil Chemical Patents Inc. Process and system for making cyclohexanone
US9926254B2 (en) 2014-08-15 2018-03-27 Exxonmobil Chemical Patents Inc. Process and system for making cyclohexanone
US9938220B2 (en) 2014-08-15 2018-04-10 Exxonmobil Chemical Patents Inc. Process and system for making cyclohexanone
WO2016053583A1 (en) 2014-09-30 2016-04-07 Exxonmobil Chemical Patents Inc. Process for making cyclohexanone
US10294178B2 (en) 2015-03-31 2019-05-21 Exxonmobil Chemical Patents Inc. Process for making cyclohexanone and/or phenol
WO2017023429A1 (en) 2015-07-31 2017-02-09 Exxonmobil Chemical Patents Inc. Process for making cyclohexanone
WO2017023430A1 (en) 2015-07-31 2017-02-09 Exxonmobil Chemical Patents Inc. Process for making cyclohexanone
WO2019005276A1 (en) 2017-06-28 2019-01-03 Exxonmobil Chemical Patents Inc. Cyclohexanone-containing products and processes for making the same
WO2019005273A1 (en) 2017-06-28 2019-01-03 Exxonmobil Chemical Patents Inc. Cyclohexanone-containing products and processes for making the same
WO2019005274A1 (en) 2017-06-28 2019-01-03 Exxonmobil Chemical Patents Inc. Processes for making cyclohexanone

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US2265939A (en) * 1940-05-03 1941-12-09 Du Pont Azeotropic distillation
US4230638A (en) 1979-05-04 1980-10-28 Phillips Petroleum Company Separation of cyclohexylbenzene from a cyclohexylbenzene-cyclohexanone-phenol admixture
JPS5814411B2 (en) 1979-11-02 1983-03-18 三井化学株式会社 Purification method of phenols
DE3117135A1 (en) 1981-04-30 1982-11-18 Bayer Ag, 5090 Leverkusen CRYSTALLINE ALUMOSILICATE, METHOD FOR THE PRODUCTION THEREOF AND THE USE THEREOF FOR CATALYTICALLY CONVERTING METHANOL AND / OR DIMETHYL ETHER IN HYDROCARBONS
US4826667A (en) 1986-01-29 1989-05-02 Chevron Research Company Zeolite SSZ-25
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US5236575A (en) 1991-06-19 1993-08-17 Mobil Oil Corp. Synthetic porous crystalline mcm-49, its synthesis and use
JP3265659B2 (en) 1992-06-05 2002-03-11 住友化学工業株式会社 Phenol purification method
US5362697A (en) 1993-04-26 1994-11-08 Mobil Oil Corp. Synthetic layered MCM-56, its synthesis and use
ES2124154B1 (en) 1995-11-08 1999-12-01 Univ Politecnica De Valencia C PREPARATION METHOD AND CATALYTIC PROPERTIES OF A MICROPOROUS SOLID WITH HIGH EXTERNAL SURFACE.
ES2105982B1 (en) 1995-11-23 1998-07-01 Consejo Superior Investigacion ZEOLITE ITQ-1
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US6049018A (en) 1999-01-21 2000-04-11 Mobil Corporation Synthetic porous crystalline MCM-68, its synthesis and use
DE10015874A1 (en) 2000-03-30 2001-10-11 Creavis Tech & Innovation Gmbh Process for the preparation of aromatic alcohols, especially phenol
US6756030B1 (en) 2003-03-21 2004-06-29 Uop Llc Crystalline aluminosilicate zeolitic composition: UZM-8
CN101687784B (en) 2007-08-22 2014-11-12 埃克森美孚化学专利公司 Oxidation of hydrocarbons
WO2009058527A1 (en) 2007-10-31 2009-05-07 Exxonmobil Chemical Patents Inc. Oxidation of hydrocarbons
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JP5444327B2 (en) * 2008-04-25 2014-03-19 エクソンモービル・ケミカル・パテンツ・インク Process for producing phenol and / or cyclohexanone
US9115060B2 (en) 2011-10-07 2015-08-25 Exxonmobil Chemical Patents Inc. Process for producing phenol

Also Published As

Publication number Publication date
US20150094495A1 (en) 2015-04-02
WO2013165656A1 (en) 2013-11-07
CN104284876A (en) 2015-01-14
EP2844628A1 (en) 2015-03-11
US9181165B2 (en) 2015-11-10
CN104284876B (en) 2017-03-08

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